CN103666827B - A kind of Raw wool detergent and preparation method thereof - Google Patents
A kind of Raw wool detergent and preparation method thereof Download PDFInfo
- Publication number
- CN103666827B CN103666827B CN201310610483.2A CN201310610483A CN103666827B CN 103666827 B CN103666827 B CN 103666827B CN 201310610483 A CN201310610483 A CN 201310610483A CN 103666827 B CN103666827 B CN 103666827B
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- China
- Prior art keywords
- parts
- raw wool
- sodium
- wool detergent
- preparation
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- 210000002268 wool Anatomy 0.000 title claims abstract description 40
- 239000003599 detergent Substances 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 33
- RNMDNPCBIKJCQP-UHFFFAOYSA-N 5-nonyl-7-oxabicyclo[4.1.0]hepta-1,3,5-trien-2-ol Chemical compound C(CCCCCCCC)C1=C2C(=C(C=C1)O)O2 RNMDNPCBIKJCQP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000011734 sodium Substances 0.000 claims abstract description 22
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 11
- FLIACVVOZYBSBS-UHFFFAOYSA-N Methyl palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC FLIACVVOZYBSBS-UHFFFAOYSA-N 0.000 claims abstract description 11
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims abstract description 11
- 150000001335 aliphatic alkanes Chemical class 0.000 claims abstract description 11
- JXLHNMVSKXFWAO-UHFFFAOYSA-N azane;7-fluoro-2,1,3-benzoxadiazole-4-sulfonic acid Chemical compound N.OS(=O)(=O)C1=CC=C(F)C2=NON=C12 JXLHNMVSKXFWAO-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000008367 deionised water Substances 0.000 claims abstract description 11
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 11
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical class CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 claims abstract description 11
- -1 polyoxyethylene nonylphenol Polymers 0.000 claims abstract description 11
- 229910052938 sodium sulfate Inorganic materials 0.000 claims abstract description 11
- 235000011152 sodium sulphate Nutrition 0.000 claims abstract description 11
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims abstract description 11
- 239000000463 material Substances 0.000 claims abstract description 7
- 230000008719 thickening Effects 0.000 claims abstract description 7
- MGIYRDNGCNKGJU-UHFFFAOYSA-N isothiazolinone Chemical group O=C1C=CSN1 MGIYRDNGCNKGJU-UHFFFAOYSA-N 0.000 claims description 8
- 238000003756 stirring Methods 0.000 claims description 5
- 239000012467 final product Substances 0.000 claims 1
- 238000005406 washing Methods 0.000 abstract description 5
- 239000012752 auxiliary agent Substances 0.000 abstract description 3
- 239000004753 textile Substances 0.000 abstract description 3
- 230000002070 germicidal effect Effects 0.000 abstract description 2
- 238000009991 scouring Methods 0.000 description 3
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- 241000222122 Candida albicans Species 0.000 description 1
- 241000191967 Staphylococcus aureus Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- ZFXVRMSLJDYJCH-UHFFFAOYSA-N calcium magnesium Chemical compound [Mg].[Ca] ZFXVRMSLJDYJCH-UHFFFAOYSA-N 0.000 description 1
- 229940095731 candida albicans Drugs 0.000 description 1
- 238000002242 deionisation method Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
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- Detergent Compositions (AREA)
Abstract
The present invention relates to a kind of Raw wool detergent and preparation method thereof, belong to technical field of textile auxiliary agent.This Raw wool detergent comprises the following component according to weight parts: ethoxylated dodecyl alcohol 7 ~ 11 parts, Seconary Alkane Sulphonate Sodium 6 ~ 9 parts, Uniphat A60 α-sodium sulfonate 2 ~ 4 parts, 3 ~ 5 parts, polyoxyethylene nonylphenol ether (10) sodium sulfate, citric acid 2 ~ 4 parts, thickening material 0.5 ~ 2 part, 1 ~ 3 part, sterilant, deionized water 100 ~ 120 parts.Raw wool detergent degrease of the present invention is effective, and germicidal action is strong, the raw wool good hand touch after washing, and whiteness is high, and preparation technology is simple, is easy to apply.
Description
Technical field
The invention belongs to technical field of textile auxiliary agent, be specifically related to a kind of Raw wool detergent and preparation method thereof.
Background technology
Raw wool is namely without finished wool, and wool wants first scouring of wool to remove the impurity such as suet, wool perspiration and dust before weaving.Current most of producer uses alkali scouring method to wash raw wool, because its resistance to hard deionization water-based is poor, produce calcium magnesium soap precipitation, greatly have impact on washing woolen handle and whiteness, therefore how to overcome the deficiencies in the prior art, the Raw wool detergent developing a kind of applicable acid scouring of wool method is the problem that current technical field of textile auxiliary agent needs solution badly.
Summary of the invention
The object of the invention is, in order to solve the deficiencies in the prior art, to provide a kind of Raw wool detergent and preparation method thereof, this washing composition degrease is effective, and the raw wool good hand touch after washing, whiteness is high.
The technical solution used in the present invention is as follows:
A kind of Raw wool detergent, comprises the following component according to weight parts: ethoxylated dodecyl alcohol 7 ~ 11 parts, Seconary Alkane Sulphonate Sodium 6 ~ 9 parts, Uniphat A60 α-sodium sulfonate 2 ~ 4 parts, 3 ~ 5 parts, polyoxyethylene nonylphenol ether (10) sodium sulfate, citric acid 2 ~ 4 parts, thickening material 0.5 ~ 2 part, 1 ~ 3 part, sterilant, deionized water 100 ~ 120 parts.
Further preferably described thickening material is Xylo-Mucine.
Further preferably described sterilant is isothiazolinone.
Ethoxylated dodecyl alcohol, Seconary Alkane Sulphonate Sodium, Uniphat A60 α-sodium sulfonate, polyoxyethylene nonylphenol ether (10) sodium sulfate join in deionized water by the preparation method of above-mentioned Raw wool detergent, be stirred to after it mixes, add citric acid and sterilant again, continue stirring 10 ~ 20min, finally add thickening material adjusting viscosity, obtain Raw wool detergent of the present invention.
compared with prior art, its beneficial effect is in the present invention:raw wool detergent degrease of the present invention is effective, and germicidal action is strong, the raw wool good hand touch after washing, and whiteness is high, and preparation technology is simple, is easy to apply.
Specific embodiment
Below in conjunction with embodiment, the present invention is described in further detail.
Embodiment 1
A kind of Raw wool detergent, comprises the following component according to weight parts: ethoxylated dodecyl alcohol 7 parts, Seconary Alkane Sulphonate Sodium 6 parts, Uniphat A60 α-sodium sulfonate 2 parts, 3 parts, polyoxyethylene nonylphenol ether (10) sodium sulfate, citric acid 2 parts, Xylo-Mucine 0.5 part, isothiazolinone 1 part, deionized water 100 parts.
Ethoxylated dodecyl alcohol, Seconary Alkane Sulphonate Sodium, Uniphat A60 α-sodium sulfonate, polyoxyethylene nonylphenol ether (10) sodium sulfate join in deionized water by the preparation method of the present embodiment Raw wool detergent, be stirred to after it mixes, add citric acid and isothiazolinone again, continue to stir 10min, finally add Xylo-Mucine adjusting viscosity, obtain the Raw wool detergent of the present embodiment.
Embodiment 2
A kind of Raw wool detergent, comprises the following component according to weight parts: ethoxylated dodecyl alcohol 11 parts, Seconary Alkane Sulphonate Sodium 9 parts, Uniphat A60 α-sodium sulfonate 4 parts, 5 parts, polyoxyethylene nonylphenol ether (10) sodium sulfate, citric acid 4 parts, Xylo-Mucine 2 parts, isothiazolinone 3 parts, deionized water 120 parts.
Ethoxylated dodecyl alcohol, Seconary Alkane Sulphonate Sodium, Uniphat A60 α-sodium sulfonate, polyoxyethylene nonylphenol ether (10) sodium sulfate join in deionized water by the preparation method of the present embodiment Raw wool detergent, be stirred to after it mixes, add citric acid and isothiazolinone again, continue to stir 20min, finally add Xylo-Mucine adjusting viscosity, obtain the Raw wool detergent of the present embodiment.
Embodiment 3
A kind of Raw wool detergent, comprises the following component according to weight parts: ethoxylated dodecyl alcohol 9 parts, Seconary Alkane Sulphonate Sodium 8 parts, Uniphat A60 α-sodium sulfonate 3 parts, 4 parts, polyoxyethylene nonylphenol ether (10) sodium sulfate, citric acid 3 parts, Xylo-Mucine 1 part, isothiazolinone 2 parts, deionized water 110 parts.
Ethoxylated dodecyl alcohol, Seconary Alkane Sulphonate Sodium, Uniphat A60 α-sodium sulfonate, polyoxyethylene nonylphenol ether (10) sodium sulfate join in deionized water by the preparation method of the present embodiment Raw wool detergent, be stirred to after it mixes, add citric acid and isothiazolinone again, continue to stir 17min, finally add Xylo-Mucine adjusting viscosity, obtain the Raw wool detergent of the present embodiment.
Test the bactericidal property of the Raw wool detergent of embodiment 1 ~ 3, test result is as shown in table 1.
The bactericidal property test result of the Raw wool detergent of table 1 embodiment 1 ~ 3
| Embodiment 1 | Embodiment 2 | Embodiment 3 | |
| Streptococcus aureus | 95% | 98% | 99% |
| Intestinal bacteria | 96% | 99% | 98% |
| Candida albicans | 95% | 97% | 99% |
Meanwhile, after the Raw wool detergent of the present embodiment 1 ~ 3 is diluted 10 times, wash raw wool, after to be dried, test its whiteness and feel, the results are shown in Table shown in 2.
Table 2 test result
| Wool whiteness | With or without coarse feel of hardening | |
| Embodiment 1 | 95.2 | Nothing |
| Embodiment 2 | 96.1 | Nothing |
| Embodiment 3 | 98.3 | Nothing |
Claims (4)
1. a Raw wool detergent, is characterized in that comprising the following component according to weight parts: ethoxylated dodecyl alcohol 7 ~ 11 parts, Seconary Alkane Sulphonate Sodium 6 ~ 9 parts, Uniphat A60 α-sodium sulfonate 2 ~ 4 parts, 3 ~ 5 parts, polyoxyethylene nonylphenol ether (10) sodium sulfate, citric acid 2 ~ 4 parts, thickening material 0.5 ~ 2 part, 1 ~ 3 part, sterilant, deionized water 100 ~ 120 parts.
2. Raw wool detergent according to claim 1, is characterized in that described thickening material is Xylo-Mucine.
3. Raw wool detergent according to claim 1, is characterized in that described sterilant is isothiazolinone.
4. the preparation method of Raw wool detergent according to claim 1, ethoxylated dodecyl alcohol, Seconary Alkane Sulphonate Sodium, Uniphat A60 α-sodium sulfonate, polyoxyethylene nonylphenol ether (10) sodium sulfate is it is characterized in that to join in deionized water, be stirred to after it mixes, add citric acid and sterilant again, continue stirring 10 ~ 20min, finally add thickening material adjusting viscosity, to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310610483.2A CN103666827B (en) | 2013-11-27 | 2013-11-27 | A kind of Raw wool detergent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310610483.2A CN103666827B (en) | 2013-11-27 | 2013-11-27 | A kind of Raw wool detergent and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103666827A CN103666827A (en) | 2014-03-26 |
| CN103666827B true CN103666827B (en) | 2015-09-16 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310610483.2A Expired - Fee Related CN103666827B (en) | 2013-11-27 | 2013-11-27 | A kind of Raw wool detergent and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN103666827B (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104911046A (en) * | 2015-07-03 | 2015-09-16 | 陈明志 | Soft-type clothes detergent |
| CN106758158B (en) * | 2016-12-16 | 2019-03-01 | 吴江市北厍盛源纺织品助剂厂 | A kind of environmental protection weaving refining agent and preparation method thereof for mulberry silk |
| CN106676883A (en) * | 2016-12-23 | 2017-05-17 | 五河县盛源畜牧养殖专业合作社 | Natural impurity remover for raw wool |
| CN116695259B (en) * | 2023-06-20 | 2024-02-23 | 广州达维健健康工程有限公司 | Low-temperature washing method for raw wool |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1069761A (en) * | 1991-08-17 | 1993-03-10 | 王怀栋 | Wool detergent |
| CN1123831A (en) * | 1995-10-06 | 1996-06-05 | 李毅民 | Environment-protecting detergent |
| CN102876489A (en) * | 2012-10-26 | 2013-01-16 | 纳爱斯集团有限公司 | Neutral washing powder and preparation method thereof |
| CN102943002A (en) * | 2012-11-21 | 2013-02-27 | 浙江雀屏纺织化工股份有限公司 | Formula and synthesis process of cashmere environment-friendly swelling agent |
| CN103194322A (en) * | 2013-04-11 | 2013-07-10 | 太仓市隆丝达针织时装有限责任公司 | Special detergent for woolen sweater and preparation method thereof |
-
2013
- 2013-11-27 CN CN201310610483.2A patent/CN103666827B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1069761A (en) * | 1991-08-17 | 1993-03-10 | 王怀栋 | Wool detergent |
| CN1123831A (en) * | 1995-10-06 | 1996-06-05 | 李毅民 | Environment-protecting detergent |
| CN102876489A (en) * | 2012-10-26 | 2013-01-16 | 纳爱斯集团有限公司 | Neutral washing powder and preparation method thereof |
| CN102943002A (en) * | 2012-11-21 | 2013-02-27 | 浙江雀屏纺织化工股份有限公司 | Formula and synthesis process of cashmere environment-friendly swelling agent |
| CN103194322A (en) * | 2013-04-11 | 2013-07-10 | 太仓市隆丝达针织时装有限责任公司 | Special detergent for woolen sweater and preparation method thereof |
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| CN103666827A (en) | 2014-03-26 |
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| ASS | Succession or assignment of patent right |
Owner name: NINGBO JIANGDONG LUNSI ENVIRONMENTAL PROTECTION TE Free format text: FORMER OWNER: JIANGSU ZHONGXIN RESOURCES GROUP CO., LTD. Effective date: 20150820 |
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| C41 | Transfer of patent application or patent right or utility model | ||
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| CB03 | Change of inventor or designer information |
Inventor after: Zhang Guohua Inventor before: Zhu Weiqiang |
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| COR | Change of bibliographic data |
Free format text: CORRECT: INVENTOR; FROM: ZHU WEIQIANG TO: ZHANG GUOHUA |
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Effective date of registration: 20150820 Address after: 315043 Zhejiang province Ningbo City Jiangdong Sangtian Road No. 688 building 651 room 6 Applicant after: NINGBO JIANGDONG LUNSIFU ENVIRONMENTAL PROTECTION TECHNOLOGY CO., LTD. Address before: 226300 Industrial Park, Xianfeng Town, Nantong, Jiangsu, Tongzhou District Applicant before: Jiangsu ZhongXin Resources Group Co., Ltd. |
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| C14 | Grant of patent or utility model | ||
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| C41 | Transfer of patent application or patent right or utility model | ||
| CB03 | Change of inventor or designer information |
Inventor after: Guo Ruiping Inventor before: Zhang Guohua |
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| COR | Change of bibliographic data | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20161116 Address after: Guangdong province Zhongshan City Yongyuan road 528467 Tanzhou Town, No. 4 building third layer A Patentee after: Zhongshan flying industry Co., Ltd. Address before: 315043 Zhejiang province Ningbo City Jiangdong Sangtian Road No. 688 building 651 room 6 Patentee before: NINGBO JIANGDONG LUNSIFU ENVIRONMENTAL PROTECTION TECHNOLOGY CO., LTD. |
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| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150916 Termination date: 20171127 |