CN103641454A - High-voltage ceramic material and preparation method thereof - Google Patents
High-voltage ceramic material and preparation method thereof Download PDFInfo
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- CN103641454A CN103641454A CN201310618484.1A CN201310618484A CN103641454A CN 103641454 A CN103641454 A CN 103641454A CN 201310618484 A CN201310618484 A CN 201310618484A CN 103641454 A CN103641454 A CN 103641454A
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Abstract
The invention relates to the technical field of ceramic materials, particularly a high-voltage ceramic material which is characterized by comprising the following components in percentage by weight: 45-76 parts of industrial waste, 16-20 parts of plasticizer, 0.5-3 parts of lubricant, 0.8-8 parts of modifier, 6-11 parts of kieselguhr, 1.2-6 parts of reinforcing fiber, 72-82 parts of alumina and 18-23 parts of zirconia. By fully utilizing the industrial waste as the raw material and adding proper parts of plasticizer, lubricant, modifier, kieselguhr and reinforcing fiber, the obtained ceramic material is nontoxic and harmless, can reutilize the resources, is environment-friendly, and is suitable for application to domestic ceramics, architectural ceramics or the like.
Description
Technical field
The present invention relates to technical field of ceramic material, more specifically, relate to a kind of higfh-tension ceramics material and preparation method thereof.
Background technology
Along with the transformation to sludge treatment thinking both at home and abroad, now progressively unification comes on the technical thought of sludge anhydration burning.For the solid waste forming after sludge incineration, how incineration residue should be disposed, always the state in arguement.The outlet of the flyash meanwhile, various large, medium and small heat power plants being produced is never effectively solved.The waste garrulous material sheet of all kinds of pot banks, the fertilizer of Bricks and Tiles Plant is arbitrarily piled abstention, topples over environment is done great damage.
Meanwhile, along with improving constantly of people's living standard, the consciousness of environment and health progressively strengthens, and green material and environmentfriendly products will be paid close attention to by people day by day.Healthy, long-lived, the comfortable highest goal that has become modern's pursuit.Antibacterial, health care, environment-protecting product arise at the historic moment, and obtain and develop rapidly.And no matter ceramic is as domestic ceramics or as building ceramics such as household, decorations, all closely bound up with daily life, so people also have higher requirement to the health care function of all kinds of ceramics.
Summary of the invention
The present invention is at least one defect overcoming described in above-mentioned prior art, and a kind of higfh-tension ceramics material that utilizes trade waste to manufacture is provided.
For solving the problems of the technologies described above, the technical solution used in the present invention is:
A kind of higfh-tension ceramics material is provided, comprises by weight percentage following component: 45 ~ 76 parts of trade wastes, 16 ~ 20 parts, softening agent, 0.5 ~ 3 part of lubricant, 0.8 ~ 8 part of properties-correcting agent, 6 ~ 11 parts, diatomite, 1.2 ~ 6 parts of fortifying fibres,, 72 ~ 82 parts, aluminum oxide, 18 ~ 23 parts of zirconium whites.
Further, also comprise 0.3 ~ 3 part of mica powder, 2 ~ 3 parts of fire retardants.
Preferably, comprise by weight percentage following component: 61 parts of trade wastes, 18 parts, softening agent, 2 parts of lubricants, 5 parts of properties-correcting agent, 8 parts, diatomite, 3 parts of fortifying fibres, 1 part of mica powder and 2 parts of fire retardants, 75 parts, aluminum oxide, 20 parts of zirconium whites.
Alternatively, described industrial waste is useless mud, waste ceramic fragment or incineration residue.
Alternatively, described properties-correcting agent is silicon carbide or silicon oxide.
Alternatively, described fortifying fibre is Natvosol, ceramic fiber or sapphire whisker.
Preferably, described softening agent is nontoxicity softening agent.
The present invention also provides a kind of preparation method of as above-mentioned arbitrary higfh-tension ceramics material, comprises the following steps:
S1. distinguish the following component of ball milling by weight: 45 ~ 76 parts of trade wastes, 16 ~ 20 parts, softening agent, 0.5 ~ 3 part of lubricant, 0.8 ~ 8 part of properties-correcting agent, 6 ~ 11 parts, diatomite, 1.2 ~ 6 parts of fortifying fibres, 72 ~ 82 parts, aluminum oxide, 18 ~ 23 parts of zirconium whites;
S2. by after said components mix and blend, add 0.3 ~ 3 part of mica powder and 2 ~ 3 parts of fire retardants and make slurry;
S3. by described slurry sinter molding.
Wherein, described Ball-milling Time is 26 ~ 30 hours, and churning time is 10 ~ 20 minutes; Sintering time is 3 ~ 5 hours, and sintering temperature is 1100 ~ 1250 ℃.
Compared with prior art, the invention has the beneficial effects as follows:
Higfh-tension ceramics material of the present invention makes full use of trade waste as raw material, and add softening agent, lubricant, properties-correcting agent, diatomite and the fortifying fibre of suitable umber, the stupalith obtaining is nontoxic, when resource can reuse, the stupalith environmental protection obtaining, is suitable for the application of domestic ceramics or building ceramic etc.
Embodiment
Below in conjunction with embodiment, the present invention is further illustrated.
Embodiment 1
Choose 61 parts, useless mud, 18 parts, nontoxicity softening agent, 2 parts of lubricants, 5 parts, silicon carbide, 8 parts, diatomite, 3 parts of Natvosols, 72 parts, aluminum oxide, 18 parts of zirconium whites; Broken mixing, ball milling 26 hours mix and blend 15 minutes; Adding 2 parts of 1 part of mica powder and fire retardants continues mix and blend and makes slurry; By slurry sintering 4 hours under the environment of 1200 ℃.
The stupalith finished product making after tested, without damaging phenomenon, tasteless, nontoxic, high pressure resistant.
Embodiment 2
Choose 45 parts of waste ceramic fragments, 20 parts, nontoxicity softening agent, 3 parts of lubricants, 8 parts, silicon carbide, 11 parts, diatomite and 6 parts of Natvosols, 75 parts, aluminum oxide, 20 parts of zirconium whites; Broken mixing, ball milling 26 hours mix and blend 20 minutes; Add 3 parts of 0.3 part of mica powder and fire retardants, surplus is that rare earth oxide or other inevitable impurity continue mix and blend and makes slurry; By slurry sintering 4 hours under the environment of 1100 ℃.
The stupalith finished product making after tested, without damaging phenomenon, tasteless, nontoxic, high pressure resistant.
Embodiment 3
Choose 76 parts, useless mud, 16 parts, softening agent, 0.5 part of lubricant, 0.8 part, silicon carbide, 6 parts, diatomite and 1.2 parts of ceramic fibers, 73 parts, aluminum oxide, 21 parts of zirconium whites; Broken mixing, ball milling 30 hours mix and blend 10 minutes; Add 3 parts of 3 parts of mica powders and fire retardants, surplus is that rare earth oxide or other inevitable impurity continue mix and blend and makes slurry; By slurry sintering 3 hours under the environment of 1100 ℃.
The stupalith finished product making after tested, without damaging phenomenon, tasteless, nontoxic, high pressure resistant.
Embodiment 4
Choose 55 parts of waste ceramic fragments, 18 parts, nontoxicity softening agent, 1 part of lubricant, 6 parts of silicon oxide, 10 parts, diatomite and 3 parts of ceramic fibers, 80 parts, aluminum oxide, 22 parts of zirconium whites; Broken mixing, ball milling 28 hours mix and blend 18 minutes; Add 2 parts of 1 part of mica powder and fire retardants, surplus is that rare earth oxide or other inevitable impurity continue mix and blend and makes slurry; By slurry sintering 4 hours under the environment of 1250 ℃.
The stupalith finished product making after tested, without damaging phenomenon, tasteless, nontoxic, high pressure resistant.
Embodiment 5
Choose 2 parts of 69 parts of incineration residues, 16 parts, softening agent, 0.5 part of lubricant, 5 parts of silicon oxide, 6 parts, diatomite and sapphire whiskers; Broken mixing, ball milling 28 hours mix and blend 18 minutes; Add 1 part of mica powder and 2 parts of fire retardants, 82 parts, aluminum oxide, 23 parts of zirconium whites, surplus is that rare earth oxide or other inevitable impurity continue mix and blend and makes slurry; By slurry sintering 5 hours under the environment of 1250 ℃.
The stupalith finished product making after tested, without damaging phenomenon, tasteless, nontoxic, high pressure resistant.
Embodiment 6
Choose 50 parts of incineration residues, 20 parts, softening agent, 3 parts of lubricants, 7 parts of silicon oxide, 8 parts, diatomite and 6 parts of sapphire whiskers, 82 parts, aluminum oxide, 23 parts of zirconium whites; Broken mixing, ball milling 30 hours mix and blend 10 minutes; Add 2 parts of 1 part of mica powder and fire retardants, surplus is that rare earth oxide or other inevitable impurity continue mix and blend and makes slurry; By slurry sintering 3 hours under the environment of 1200 ℃.
The stupalith finished product making after tested, without damaging phenomenon, tasteless, nontoxic, high pressure resistant.
Obviously, the above embodiment of the present invention is only for example of the present invention is clearly described, and is not the restriction to embodiments of the present invention.For those of ordinary skill in the field, can also make other changes in different forms on the basis of the above description.Here exhaustive without also giving all embodiments.All any modifications of doing within the spirit and principles in the present invention, be equal to and replace and improvement etc., within all should being included in the protection domain of the claims in the present invention.
Claims (9)
1. a higfh-tension ceramics material, it is characterized in that, comprise by weight percentage following component: 45 ~ 76 parts of trade wastes, 16 ~ 20 parts, softening agent, 0.5 ~ 3 part of lubricant, 0.8 ~ 8 part of properties-correcting agent, 6 ~ 11 parts, diatomite and 1.2 ~ 6 parts of fortifying fibres, 72 ~ 82 parts, aluminum oxide, 18 ~ 23 parts of zirconium whites.
2. higfh-tension ceramics material according to claim 1, is characterized in that, also comprises 0.3 ~ 3 part of mica powder, 2 ~ 3 parts of fire retardants.
3. higfh-tension ceramics material according to claim 2, it is characterized in that, comprise by weight percentage following component: 61 parts of trade wastes, 18 parts, softening agent, 2 parts of lubricants, 5 parts of properties-correcting agent, 8 parts, diatomite, 3 parts of fortifying fibres, 1 part of mica powder, 2 parts of fire retardants, 75 parts, aluminum oxide, 20 parts of zirconium whites.
4. according to the higfh-tension ceramics material described in claims 1 to 3 any one, it is characterized in that, described industrial waste is useless mud, waste ceramic fragment or incineration residue.
5. according to the higfh-tension ceramics material described in claims 1 to 3 any one, it is characterized in that, described properties-correcting agent is silicon carbide or silicon oxide.
6. according to the higfh-tension ceramics material described in claims 1 to 3 any one, it is characterized in that, described fortifying fibre is Natvosol, ceramic fiber or sapphire whisker.
7. a preparation method for higfh-tension ceramics material as described in claim 1 to 6 any one, is characterized in that, comprises the following steps:
Difference is the following component of ball milling by weight: 45 ~ 76 parts of trade wastes, 16 ~ 20 parts, softening agent, 0.5 ~ 3 part of lubricant, 0.8 ~ 8 part of properties-correcting agent, 6 ~ 11 parts, diatomite, 1.2 ~ 6 parts of fortifying fibres, 72 ~ 82 parts, aluminum oxide, 18 ~ 23 parts of zirconium whites;
By after said components mix and blend, add 0.3 ~ 3 part of mica powder and 2 ~ 3 parts of fire retardants and make slurry;
By described slurry sinter molding.
8. preparation method according to claim 7, is characterized in that, described Ball-milling Time is 26 ~ 30 hours, and churning time is 10 ~ 20 minutes.
9. preparation method according to claim 7, is characterized in that, described sintering time is 3 ~ 5 hours, and sintering temperature is 1100 ~ 1250 ℃.
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| CN201310618484.1A CN103641454A (en) | 2013-11-29 | 2013-11-29 | High-voltage ceramic material and preparation method thereof |
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| CN201310618484.1A CN103641454A (en) | 2013-11-29 | 2013-11-29 | High-voltage ceramic material and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104909724A (en) * | 2015-06-03 | 2015-09-16 | 苏州靖羽新材料有限公司 | High-strength anti-fracture ceramic material and preparation method thereof |
| CN106145895A (en) * | 2016-07-07 | 2016-11-23 | 安徽省德邦瓷业有限公司 | A kind of pottery waste material recycling technique |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1579991A (en) * | 2003-08-08 | 2005-02-16 | 江苏艺兴紫砂陶股份有限公司 | Light, heat-insulating, sound-proofing environmentally-friendly ceramic product and its manufacture process |
| CN101580615A (en) * | 2009-02-13 | 2009-11-18 | 章建华 | Formulation of environment-friendly ceramic polymer composite material and preparation thereof |
| CN102898123A (en) * | 2012-09-04 | 2013-01-30 | 青岛保利康新材料有限公司 | Environment protection type ceramic material |
-
2013
- 2013-11-29 CN CN201310618484.1A patent/CN103641454A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1579991A (en) * | 2003-08-08 | 2005-02-16 | 江苏艺兴紫砂陶股份有限公司 | Light, heat-insulating, sound-proofing environmentally-friendly ceramic product and its manufacture process |
| CN101580615A (en) * | 2009-02-13 | 2009-11-18 | 章建华 | Formulation of environment-friendly ceramic polymer composite material and preparation thereof |
| CN102898123A (en) * | 2012-09-04 | 2013-01-30 | 青岛保利康新材料有限公司 | Environment protection type ceramic material |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104909724A (en) * | 2015-06-03 | 2015-09-16 | 苏州靖羽新材料有限公司 | High-strength anti-fracture ceramic material and preparation method thereof |
| CN106145895A (en) * | 2016-07-07 | 2016-11-23 | 安徽省德邦瓷业有限公司 | A kind of pottery waste material recycling technique |
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Application publication date: 20140319 |