CN103637975B - A kind of cream frost changing water instantaneously - Google Patents
A kind of cream frost changing water instantaneously Download PDFInfo
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Abstract
A kind of cream frost changing water instantaneously, its formulation ratio is: volatilization silicone oil (DC-345, low sticky silicone oil (DC-200,5cst), stearoyl inulin (Rheopearl? ISK2), polydimethylsiloxane and KSG-210/complex (KSG-210), lauryl PEG-9 polydimethylsiloxanes ethyl dimethione (KF-6038), purified water, butanediol, 1,3-PD (ZEMEA), sodium chloride, sodium citrate, micromolecule hyaluronic acid sodium, 1.2 pentanediols (HYDROLITE5), trehalose (TREHALOSE100), water/sodium lactate/gluconic acid sodium salt complex (PURASAL? MOISTXS), tocopherol acetas (Vitamin? E? Acetate), Fucus Vesiculosus extract (OLEPHYCOL? FV), Glycyrrhiza glabra L. extracting solution (Liquorice? LC), bisabolol, phenoxyethanol, essence, water/propylene glycol/Methylisothiazolinone/methyl hydroxybenzoate/propyl hydroxybenzoate/compound preservative (MICROCARE_MTP), this cream frost is water-in-oil system, and it is good that Water-In-Oil cream frost has moistness, and closure is good, and moisture retention is lasting.Also have the feature of oil-in-water cream frost concurrently, smear salubrious, and occur the globule instantaneously, the sensation kept the skin wet continually is provided to user.
Description
Technical field
The present invention relates to a kind of the cream frost and the preparation technology thereof that change water instantaneously.
Background technology
Cream frost is of a great variety on the market, and increasing consumer payes attention to lasting moisture retention and uses sensation.Traditional Water-In-Oil cream frost moistness and persistency better, but skinfeel sticks greasy; Or technology controlling and process is bad, there is low temperature unsure state.Some Water-In-Oil, in order to improve sticky sense and smear salubrious sense, adds ethanol.And increasing consumer wishes to use nonalcoholic product.The invention provides a kind of cream frost changing water instantaneously, soft, slim and graceful skinfeel, smears middle moment globule and generates, to the sensation of consumer's moisturizing continually.
Summary of the invention
The object of the invention is: provide one stable clearly to have the cream frost formula and preparation technology thereof of changing water as silk instantaneously, make product change the exquisite ability of water instantaneously and stability is taken into account.
The present invention is such realization: a kind of cream frost changing water instantaneously, and the percentage by weight of its formulation ratio is:
A oil phase:
Volatilization silicone oil (DC-345) 7.00%-10.00%,
Low sticky silicone oil (DC-200,5cst) 1.50%-3.00%,
Stearoyl inulin (RheopearlISK2) 0.20%-0.80%,
Polydimethylsiloxane and KSG-210/complex (KSG-210) 2.50%-3.50%,
Lauryl PEG-9 polydimethylsiloxanes ethyl dimethione (KF-6038): 0.10%-0.20%;
B aqueous phase
Purified water 53.35%-72.84%, butanediol 10.00%-15.00%,
1,3-PD (ZEMEA) 2.00%-5.00%, sodium chloride 1.20%-1.50%,
Sodium citrate 0.15%-0.20%, micromolecule hyaluronic acid sodium 0.01%-0.10%,
1.2 pentanediols (HYDROLITE5) 0.50%-2.00%;
C phase
Trehalose (TREHALOSE100) 1.00%-2.00%,
Water/sodium lactate/gluconic acid sodium salt complex (PURASALMOISTXS) 0.50%-2.00%,
Tocopherol acetas (VitaminEAcetate) 0.01%-0.05%,
Fucus Vesiculosus extract (OLEPHYCOLFV) 0.01%-0.10%,
Glycyrrhiza glabra L. extracting solution (LiquoriceLC) 0.01%-0.10%,
Bisabolol 0.01%-0.10%,
Phenoxyethanol 0.10%-0.50%, essence 0.20%-0.30%,
Water/propylene glycol/Methylisothiazolinone/methyl hydroxybenzoate/propyl hydroxybenzoate compound preservative (MICROCARE_MTP) 0.16%-0.20%,
Each raw material weight percentage ratio sum is 100% above.
Described a kind of cream frost changing water instantaneously, its preparation method according to the following steps:
(1) prepare oil phase will to volatilize silicone oil (DC-345), low sticky silicone oil (DC-200,5cst), polydimethylsiloxane and KSG-210/complex (KSG-210) and lauryl PEG-9 polydimethylsiloxanes ethyl dimethione (KF-6038) are added in the vacuum emulsification cylinder of, it is good for flooding homogenizing head with oil phase, emulsion tank is heated to 80 DEG C, open homogenizing, until formed without uniform particles viscous pasty state.Again stearoyl inulin is added, after dissolving, continue homogenizing, formed uniform without granule thick liquid, for subsequent use;
Prepare aqueous phase first by purified water suction aqueous phase cylinder, be heated to 75-80 DEG C, then will with butanediol scattered hyaluronate sodium in advance, add in aqueous phase cylinder, finally add 1 successively, ammediol (ZEMEA), sodium chloride, sodium citrate and 1.2 pentanediols (HYDROLITE5), be stirred to complete dissolved state;
(2) by main emulsion tank design temperature 80 DEG C.Scattered oil phase raw material is proceeded in main emulsion tank, opens and stir 20-30r/min; By aqueous phase cylinder raw material by the main emulsion tank of the slow suction of strainer valve, slowly form uniform emulsion;
(4) when Aqueous Phase Raw Material suction 1/3, suction aqueous phase is stopped; Emulsion tank stops stirring, and opens low speed homogenizing 800-1000/min, makes to expect the more evenly fine and smooth of body dispersion in emulsion tank; After homogenizing 2-3 minute, stop homogenizing, continue to open and stir 25-35r/min;
Continue slow suction aqueous phase cylinder raw material, until form uniform emulsion.Be incubated after 30 minutes, open cooling water temperature.
(5) when temperature is reduced to about 35 DEG C, add with good trehalose, water/sodium lactate/gluconic acid sodium salt complex (PURASALMOISTXS), tocopherol acetas (VitaminEAcetate), Fucus Vesiculosus extract (OLEPHYCOLFV), Glycyrrhiza glabra L. extracting solution (LiquoriceLC), bisabolol, phenoxyethanol, essence and the water/propylene glycol/Methylisothiazolinone/methyl hydroxybenzoate/propyl hydroxybenzoate compound preservative (MICROCARE_MTP) of water dissolution, continue to be stirred to the homogeneous latex emulsion state without globule granule;
(6) evacuation, proceeds in large container by material body; Leave standstill 24 hours, use external high speed agitator, according to the state of material body, different stirrings is set and hastens, of short duration high-speed stirred 2-5 minute, form the mastic of stable light;
(7) censorship, the qualified rear fill of indices.
This system is Water-In-Oil water outlet system, in order to the effect changing water instantaneously can be reached, and oil phase material rate < 20%, generally based on ring-type volatilization silicone oil, so both can provide the smooth skinfeel of silicone oil, again because the volatilization of silicone oil, make its product glutinous not greasy, water outlet is very fast.But volatilization silicone oil is polarity oils and fats, is difficult to mix with other oils and fatss or oil phase thickeners, makes product be difficult to stablize or occur the state of granule.So allow the enhancing of oil phase dissolubility and thickening be the white stable key of this type of cream.Present invention uses a kind of cyclic silicone oils thickening agent-stearoyl inulin, oil phase is based on silicone oil and the low sticky silicone oil of volatilizing.This thickening agent can be dissolved in volatilization silicone oil and thickening volatilization silicone oil, thus the dissolubility denseness of oil phase is increased, finally makes the stability of product greatly promote, and give the sense of touch of product softness.Primary emulsion raw material KSG-210 is a kind of silicon body of hydrophilic modifying.Have unique spacial framework, controlled moisture stores delivery systme, destroys hydrogen chain active force by electrolyte, and moisture in space is isolated, and moisture release is continuously, naturally controlled, and has the submissive sense of silkiness.Co-emulsifier is KF-6038, compared with common silicone oil emulsification agent, adds organosilyl side chain and alkyl branches, emulsifying product stability is improved greatly, has smooth silk-like handle.In aqueous phase, add butanediol and 1.3-propylene glycol, both can improve moisturizing degree, the low-temperature stability of product can be increased again.Add trehalose, the low-temperature stability of aquatic products can be assisted out and extend the shelf life of product.Coordinate other active component as micromolecular hyaluronic acid, Fucus Vesiculosus extraction, Radix Glycyrrhizae extraction, tocopherol acetas etc., reach deeply preserving moisture, resist environmental stimuli, prevent skin to be oxidized, antidotal effect.Integral formula is that moisture retention is good based on changing outlet capacity brilliance instantaneously, and skinfeel is slim and graceful, because be the system of silicone oil water conservation, can add wetting agent and the active matter of electrolytes in system, as sodium lactate, and sodium gluconate etc.And this is according to the feature of formula, formulate special production technology.Before emulsifying, first by oil phase material dissolution thickening homogenizing, be dispersed into fine and smooth viscous pasty state.This step is the key determining that mastic is fine and smooth and stable.In emulsification, then first suction 1/3 aqueous phase opens low speed homogenizing, makes mastic finer and smoother uniform and stable, then continues all the other aqueous phases of 2/3 of slow suction and enter emulsion tank emulsifying.After discharging, leave standstill and within 24 hours, use the of short duration rapid stirring of external stirrer to stiff light mastic again.Closely cooperating by composition and engineering, makes mastic fine and smooth graceful, smear both can instantaneousization water, has again lasting moisture retention and stability concurrently.This cream frost is water-in-oil system, and it is good that Water-In-Oil cream frost has moistness, and closure is good, and moisture retention is lasting.Also have the feature of oil-in-water cream frost concurrently, smear salubrious, and occur the globule instantaneously, the sensation kept the skin wet continually is provided to user.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described
Embodiment 1
A kind of cream frost changing water instantaneously, the percentage by weight of its formula:
A oil phase:
Volatilization silicone oil (DC-345) 8.50%, low sticky silicone oil (DC-200,5cst) 2.50%,
Stearoyl inulin (RheopearlISK2) 0.50%,
Polydimethylsiloxane and KSG-210 complex (KSG-210) 3.00%,
Lauryl PEG-9 polydimethylsiloxanes ethyl dimethione (KF-6038) 0.15%;
B aqueous phase
Purified water 62.72%, butanediol 12.00%,
1,3-PD (ZEMEA) 4.00%, sodium chloride 1.30%
Sodium citrate 0.16%, micromolecule hyaluronic acid sodium 0.06%,
1.2 pentanediols (HYDROLITE5) 1.50%;
C phase
Trehalose (TREHALOSE100) 1.50%,
Water/sodium lactate/gluconic acid sodium salt complex (PURASALMOISTXS) 1.5%,
Tocopherol acetas (VitaminEAcetate) 0.03%
Fucus Vesiculosus extract (OLEPHYCOLFV) 0.05%,
Glycyrrhiza glabra L. extracting solution (LiquoriceLC) 0.05%,
Bisabolol 0.10%, phenoxyethanol 0.05%,
Essence 0.25%
Water/propylene glycol/Methylisothiazolinone/methyl hydroxybenzoate/propyl hydroxybenzoate compound preservative (MICROCARE_MTP) 0.18%.
Its preparation method is according to the following steps:
(1) prepare oil phase will to volatilize silicone oil (DC-345), low sticky silicone oil (DC-200,5cst), polydimethylsiloxane and KSG-210/complex (KSG-210) and lauryl PEG-9 polydimethylsiloxanes ethyl dimethione (KF-6038) are added in the vacuum emulsification cylinder of, it is good for flooding homogenizing head with oil phase, emulsion tank is heated to 80 DEG C, open homogenizing, until formed without uniform particles viscous pasty state.Again stearoyl inulin is added, after dissolving, continue homogenizing, formed uniform without granule thick liquid, for subsequent use;
Prepare aqueous phase first by purified water suction aqueous phase cylinder, be heated to 75-80 DEG C, then will with butanediol scattered hyaluronate sodium in advance, add in aqueous phase cylinder, finally add 1 successively, ammediol (ZEMEA), sodium chloride, sodium citrate and 1.2 pentanediols (HYDROLITE5), be stirred to complete dissolved state;
(2) by main emulsion tank design temperature 80 DEG C.Scattered oil phase raw material is proceeded in main emulsion tank, opens and stir 20-30r/min; By aqueous phase cylinder raw material by the main emulsion tank of the slow suction of strainer valve, slowly form uniform emulsion;
(4) when Aqueous Phase Raw Material suction 1/3, suction aqueous phase is stopped; Emulsion tank stops stirring, and opens low speed homogenizing 800-1000/min, makes to expect the more evenly fine and smooth of body dispersion in emulsion tank; After homogenizing 2-3 minute, stop homogenizing, continue to open and stir 25-35r/min;
Continue slow suction aqueous phase cylinder raw material, until form uniform emulsion.Be incubated after 30 minutes, open cooling water temperature.
(5) when temperature is reduced to about 35 DEG C, add with good trehalose, water/sodium lactate/gluconic acid sodium salt complex (PURASALMOISTXS), tocopherol acetas (VitaminEAcetate), Fucus Vesiculosus extract (OLEPHYCOLFV), Glycyrrhiza glabra L. extracting solution (LiquoriceLC), bisabolol, phenoxyethanol, essence and the water/propylene glycol/Methylisothiazolinone/methyl hydroxybenzoate/propyl hydroxybenzoate compound preservative (MICROCARE_MTP) of water dissolution, continue to be stirred to the homogeneous latex emulsion state without globule granule;
(6) evacuation, proceeds in large container by material body; Leave standstill 24 hours, use external high speed agitator, according to the state of material body, different stirrings is set and hastens, of short duration high-speed stirred 2-5 minute, form the mastic of stable light;
(7) censorship, the qualified rear fill of indices.
The present embodiment 1: a kind of parameters changing the cream frost of water instantaneously:
Mastic outward appearance: milky uniform and smooth mastic
Abnormal smells from the patient: consistent with essence standard specimen abnormal smells from the patient
Heat-resisting: 45 DEG C, 4 months stable testing
Cold-resistant :-15 ~-5 DEG C, 4 months low-temperature stabilizations
Smear sense: spread upon on skin, change water instantaneously, submissive as silk.
Embodiment 2
One changes water cream frost instantaneously, and the percentage by weight of its formula is:
Volatilization silicone oil (DC-345) 10.00%,
Low sticky silicone oil (DC-200,5cst) 3.00%,
Stearoyl inulin (RheopearlISK2) 0.80%,
Polydimethylsiloxane and KSG-210 complex (KSG-210) 3.50%,
Lauryl PEG-9 polydimethylsiloxanes ethyl dimethione (KF-6038) 0.20%;
B aqueous phase:
Purified water 53.35%, butanediol 15.00%,
1,3-PD (ZEMEA) 5.00%, sodium chloride 1.50%,
Sodium citrate 0.20%, micromolecule hyaluronic acid sodium 0.10%,
1.2 pentanediols (HYDROLITE5) 2.00%;
C low temperature adds phase
Trehalose (TREHALOSE100) 2.00%,
Water/sodium lactate/gluconic acid sodium salt complex (PURASALMOISTXS) 2.00%,
Tocopherol acetas (VitaminEAcetate) 0.05%
Fucus Vesiculosus extract (OLEPHYCOLFV) 0.10%,
Glycyrrhiza glabra L. extracting solution (LiquoriceLC) 0.10%,
Bisabolol 0.10%, phenoxyethanol 0.50%,
Essence 0.30%,
Water/propylene glycol/Methylisothiazolinone/methyl hydroxybenzoate/propyl hydroxybenzoate compound preservative (MICROCARE_MTP) 0.20%.
The present embodiment 2: one changes water cream frost parameters instantaneously:
Mastic outward appearance: milky uniform and smooth mastic
Abnormal smells from the patient: consistent with essence standard specimen abnormal smells from the patient
Heat-resisting: 45 DEG C, 4 months stable testing
Cold-resistant :-15 ~-5 DEG C, 4 months low-temperature stabilizations
Smear sense: spread upon on skin, change water instantaneously, submissive as silk.
Embodiment 3
One changes water cream frost instantaneously, and the percentage by weight of its formula is:
Volatilization silicone oil (DC-345) 7.00%,
Low sticky silicone oil (DC-200,5cst) 1.50%,
Stearoyl inulin (RheopearlISK2) 0.20%,
Polydimethylsiloxane and KSG-210 complex (KSG-210) 2.50%,
Lauryl PEG-9 polydimethylsiloxanes ethyl dimethione (KF-6038) 0.10%;
B aqueous phase:
Purified water 72.84%, butanediol 10.00%,
1,3-PD (ZEMEA) 2.00%, sodium chloride 1.20%,
Sodium citrate 0.15%, micromolecule hyaluronic acid sodium 0.01%,
1.2 pentanediols (HYDROLITE5) 0.50%;
C low temperature adds phase
Trehalose (TREHALOSE100) 1.00%,
Water/sodium lactate/gluconic acid sodium salt complex (PURASALMOISTXS) 0.50%,
Tocopherol acetas (VitaminEAcetate) 0.01%
Fucus Vesiculosus extract (OLEPHYCOLFV) 0.01%,
Glycyrrhiza glabra L. extracting solution (LiquoriceLC) 0.01%,
Bisabolol 0.01%, phenoxyethanol 0.1%,
Essence 0.20%,
Water/propylene glycol/Methylisothiazolinone/methyl hydroxybenzoate/propyl hydroxybenzoate compound preservative (MICROCARE_MTP) 0.16%.
The present embodiment 3: one changes water cream frost parameters instantaneously:
Mastic outward appearance: milky uniform and smooth mastic
Abnormal smells from the patient: consistent with essence standard specimen abnormal smells from the patient
Heat-resisting: 45 DEG C, 4 months stable testing
Cold-resistant :-15 ~-5 DEG C, 4 months low-temperature stabilizations
Smear sense: spread upon on skin, change water instantaneously, submissive as silk.
The cream frost changing water instantaneously of the present invention has the following advantages:
1, spread upon on skin and change water instantaneously, form fine and closely woven droplet at skin surface, to the sensation of consumer's moisturizing continually.Soft, skinfeel is slim and graceful as silk.
2, water-in-oil system, what have Water-In-Oil cream frost has feature, and closure is good, moistness, and moisture retention is more lasting.There is again the slim and graceful skinfeel of oil-in-water cream frost, smooth as silk.
3, good stability, can add containing electrolytical active component.
Raw materials for production table:
Claims (1)
1. change the cream frost of water instantaneously for one kind, it is characterized in that: the percentage by weight of its formulation ratio is:
A oil phase:
Volatilization silicone oil 7.00%-10.00%,
Low sticky silicone oil 1.50%-3.00%,
Stearoyl inulin 0.20%-0.80%,
Polydimethylsiloxane and KSG-210/complex 2.50%-3.50%,
Lauryl PEG-9 polydimethylsiloxanes ethyl dimethione: 0.10%-0.20%;
B aqueous phase
Purified water 53.35%-72.84%, butanediol 10.00%-15.00%,
1,3-PD 2.00%-5.00%, sodium chloride 1.20%-1.50%,
Sodium citrate 0.15%-0.20%, micromolecule hyaluronic acid sodium 0.01%-0.10%,
1.2 pentanediol 0.50%-2.00%;
C phase
Trehalose 1.00%-2.00%,
Water/sodium lactate/gluconic acid sodium salt complex 0.50%-2.00%,
Tocopherol acetas 0.01%-0.05%,
Fucus Vesiculosus extract 0.01%-0.10%,
Glycyrrhiza glabra L. extracting solution 0.01%-0.10%,
Bisabolol 0.01%-0.10%,
Phenoxyethanol 0.10%-0.50%, essence 0.20%-0.30%,
Water/propylene glycol/Methylisothiazolinone/methyl hydroxybenzoate/propyl hydroxybenzoate compound preservative 0.16%-0.20%,
Each raw material weight percentage ratio sum is 100% above;
Its preparation method is according to the following steps:
(1) preparing oil phase is added in a vacuum emulsification cylinder by volatilization silicone oil, low sticky silicone oil, polydimethylsiloxane and KSG-210/complex and lauryl PEG-9 polydimethylsiloxanes ethyl dimethione, oil phase floods homogenizing head, emulsion tank is heated to 80 DEG C, open homogenizing, until formed without uniform particles viscous pasty state; Again stearoyl inulin is added, after dissolving, continue homogenizing, formed uniform without granule thick liquid, for subsequent use;
Prepare aqueous phase first by purified water suction aqueous phase cylinder, be heated to 75-80 DEG C, then with butanediol scattered hyaluronate sodium in advance, add in aqueous phase cylinder, finally add 1,3-PD, sodium chloride, sodium citrate and 1.2 pentanediols successively, be stirred to complete dissolved state;
(2) by main emulsion tank design temperature 80 DEG C, scattered oil phase raw material is proceeded in main emulsion tank, open and stir 20-30r/min; By aqueous phase cylinder raw material by the main emulsion tank of the slow suction of strainer valve, slowly form uniform emulsion;
(3) when Aqueous Phase Raw Material suction 1/3, suction aqueous phase is stopped; Emulsion tank stops stirring, and opens low speed homogenizing 800-1000r/min, makes to expect the more evenly fine and smooth of body dispersion in emulsion tank; After homogenizing 2-3 minute, stop homogenizing, continue to open and stir 25-35r/min;
Continue slow suction aqueous phase cylinder raw material, until form uniform emulsion; Be incubated after 30 minutes, open cooling water temperature;
(4) when temperature is reduced to 35 DEG C, add with water-soluble trehalose, water/sodium lactate/gluconic acid sodium salt complex, tocopherol acetas, Fucus Vesiculosus extract, Glycyrrhiza glabra L. extracting solution, bisabolol, phenoxyethanol, essence and water/propylene glycol/Methylisothiazolinone/methyl hydroxybenzoate/propyl hydroxybenzoate compound preservative, continue to be stirred to the homogeneous latex emulsion state without globule granule;
(5) evacuation, proceeds in large container by material body; Leave standstill 24 hours, use external high speed agitator, according to the state of material body, different mixing speeds is set, of short duration high-speed stirred 2-5 minute, form the mastic of stable light;
(6) censorship, the qualified rear fill of indices;
Described volatilization silicone oil is volatilization silicone oil DC-345, and described low sticky silicone oil is low sticky silicone oil DC-200,5cst;
Described polydimethylsiloxane and KSG-210/complex are polydimethylsiloxane and KSG-210 complex KSG-210;
Described lauryl PEG-9 polydimethylsiloxanes ethyl dimethione is lauryl PEG-9 polydimethylsiloxanes ethyl dimethione KF-6038.
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| CN104188817A (en) * | 2014-08-28 | 2014-12-10 | 广州芭薇化妆品有限公司 | Water cream with wrinkle-removing effect and preparation method thereof |
| CN106137918A (en) * | 2016-08-17 | 2016-11-23 | 诺斯贝尔化妆品股份有限公司 | A kind of moment milk skin whitener |
| CN106726713A (en) * | 2016-12-14 | 2017-05-31 | 诺斯贝尔化妆品股份有限公司 | A kind of translucent moisturizing cream |
| CN107536718A (en) * | 2017-09-29 | 2018-01-05 | 广东馨柯生命科学有限公司 | A kind of long-acting slow-release whitening snow defrosting and preparation method thereof |
| CN109330927A (en) * | 2018-11-02 | 2019-02-15 | 广州丽彦妆生物科技有限公司 | One kind, which is moistened, repairs plain face frost and preparation method thereof |
| CN109330903A (en) * | 2018-11-29 | 2019-02-15 | 四川省中医药科学院 | A kind of clean oil packet water aqua type preparation method and applications |
| CN112143583A (en) * | 2020-10-10 | 2020-12-29 | 苏州特密达新材料有限公司 | Semi-aqueous cleaning agent containing nano silver |
| CN114767606B (en) * | 2022-05-06 | 2024-01-30 | 广东博然堂生物科技有限公司 | Crystal dew capable of instantly dissolving water and preparation method thereof |
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| CN1809335A (en) * | 2003-06-19 | 2006-07-26 | 宝洁公司 | Polyol-in-silicone emulsions |
| CN102670478A (en) * | 2012-04-20 | 2012-09-19 | 诺斯贝尔(中山)无纺日化有限公司 | Multi-effect restoring skin cream |
| CN103402488A (en) * | 2011-02-07 | 2013-11-20 | 株式会社资生堂 | Sunscreen cosmetic |
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| JPS615005A (en) * | 1984-06-19 | 1986-01-10 | Yoshitomi Pharmaceut Ind Ltd | Humectant |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1809335A (en) * | 2003-06-19 | 2006-07-26 | 宝洁公司 | Polyol-in-silicone emulsions |
| CN103402488A (en) * | 2011-02-07 | 2013-11-20 | 株式会社资生堂 | Sunscreen cosmetic |
| CN102670478A (en) * | 2012-04-20 | 2012-09-19 | 诺斯贝尔(中山)无纺日化有限公司 | Multi-effect restoring skin cream |
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