CN103626799B - 一种复合肌醇六磷酸糖醇酯螯合剂的制备 - Google Patents
一种复合肌醇六磷酸糖醇酯螯合剂的制备 Download PDFInfo
- Publication number
- CN103626799B CN103626799B CN201310632853.2A CN201310632853A CN103626799B CN 103626799 B CN103626799 B CN 103626799B CN 201310632853 A CN201310632853 A CN 201310632853A CN 103626799 B CN103626799 B CN 103626799B
- Authority
- CN
- China
- Prior art keywords
- sugar alcohol
- phytic acid
- alcohol ester
- composite
- sequestrant
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- -1 phytic acid sugar alcohol sugar alcohol ester Chemical class 0.000 title claims abstract description 23
- IMQLKJBTEOYOSI-UHFFFAOYSA-N Phytic acid Natural products OP(O)(=O)OC1C(OP(O)(O)=O)C(OP(O)(O)=O)C(OP(O)(O)=O)C(OP(O)(O)=O)C1OP(O)(O)=O IMQLKJBTEOYOSI-UHFFFAOYSA-N 0.000 title claims abstract description 20
- 229940068041 phytic acid Drugs 0.000 title claims abstract description 20
- 235000002949 phytic acid Nutrition 0.000 title claims abstract description 20
- 239000000467 phytic acid Substances 0.000 title claims abstract description 20
- 239000002131 composite material Substances 0.000 title claims abstract description 17
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 239000003352 sequestering agent Substances 0.000 title claims abstract description 9
- 239000002253 acid Substances 0.000 claims abstract description 6
- 150000005846 sugar alcohols Chemical class 0.000 claims abstract description 6
- 238000003756 stirring Methods 0.000 claims description 26
- 239000013078 crystal Substances 0.000 claims description 5
- 238000002425 crystallisation Methods 0.000 claims description 5
- 230000008025 crystallization Effects 0.000 claims description 5
- 239000005457 ice water Substances 0.000 claims description 5
- 238000001953 recrystallisation Methods 0.000 claims description 5
- 235000000346 sugar Nutrition 0.000 claims description 4
- 241000220324 Pyrus Species 0.000 claims description 3
- 239000003153 chemical reaction reagent Substances 0.000 claims description 3
- 235000021017 pears Nutrition 0.000 claims description 3
- FBPFZTCFMRRESA-FBXFSONDSA-N Allitol Chemical compound OC[C@H](O)[C@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-FBXFSONDSA-N 0.000 claims description 2
- PHSPJQZRQAJPPF-UHFFFAOYSA-N N-alpha-Methylhistamine Chemical compound CNCCC1=CN=CN1 PHSPJQZRQAJPPF-UHFFFAOYSA-N 0.000 claims description 2
- 125000001246 bromo group Chemical group Br* 0.000 claims description 2
- FYSNRJHAOHDILO-UHFFFAOYSA-N thionyl chloride Chemical compound ClS(Cl)=O FYSNRJHAOHDILO-UHFFFAOYSA-N 0.000 claims 2
- FBPFZTCFMRRESA-KAZBKCHUSA-N D-altritol Chemical compound OC[C@@H](O)[C@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KAZBKCHUSA-N 0.000 claims 1
- 125000001309 chloro group Chemical group Cl* 0.000 claims 1
- 229960003827 isosorbide mononitrate Drugs 0.000 claims 1
- YWXYYJSYQOXTPL-SLPGGIOYSA-N isosorbide mononitrate Chemical compound [O-][N+](=O)O[C@@H]1CO[C@@H]2[C@@H](O)CO[C@@H]21 YWXYYJSYQOXTPL-SLPGGIOYSA-N 0.000 claims 1
- UHZYTMXLRWXGPK-UHFFFAOYSA-N phosphorus pentachloride Chemical compound ClP(Cl)(Cl)(Cl)Cl UHZYTMXLRWXGPK-UHFFFAOYSA-N 0.000 claims 1
- 239000011573 trace mineral Substances 0.000 abstract description 9
- 235000013619 trace mineral Nutrition 0.000 abstract description 9
- 150000002148 esters Chemical class 0.000 abstract description 5
- 239000007788 liquid Substances 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 239000013543 active substance Substances 0.000 abstract 1
- 229910052728 basic metal Inorganic materials 0.000 abstract 1
- 150000003818 basic metals Chemical class 0.000 abstract 1
- 239000003446 ligand Substances 0.000 abstract 1
- 150000003624 transition metals Chemical group 0.000 abstract 1
- 239000003337 fertilizer Substances 0.000 description 8
- 241000196324 Embryophyta Species 0.000 description 6
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 3
- 238000012423 maintenance Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 235000010755 mineral Nutrition 0.000 description 3
- 239000011707 mineral Substances 0.000 description 3
- 239000011259 mixed solution Substances 0.000 description 3
- 239000002689 soil Substances 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 2
- 210000000481 breast Anatomy 0.000 description 2
- 150000001720 carbohydrates Chemical class 0.000 description 2
- 235000014633 carbohydrates Nutrition 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 229910052748 manganese Inorganic materials 0.000 description 2
- 239000011572 manganese Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 210000000056 organ Anatomy 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 239000013589 supplement Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000012190 activator Substances 0.000 description 1
- 244000245420 ail Species 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000003042 antagnostic effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000003115 biocidal effect Effects 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 230000009920 chelation Effects 0.000 description 1
- 238000005056 compaction Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000011790 ferrous sulphate Substances 0.000 description 1
- 235000003891 ferrous sulphate Nutrition 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 235000004611 garlic Nutrition 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 229910017053 inorganic salt Inorganic materials 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 description 1
- 229910000359 iron(II) sulfate Inorganic materials 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- SQQMAOCOWKFBNP-UHFFFAOYSA-L manganese(II) sulfate Chemical compound [Mn+2].[O-]S([O-])(=O)=O SQQMAOCOWKFBNP-UHFFFAOYSA-L 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000002366 mineral element Substances 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 230000026961 phloem transport Effects 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- FAIAAWCVCHQXDN-UHFFFAOYSA-N phosphorus trichloride Chemical compound ClP(Cl)Cl FAIAAWCVCHQXDN-UHFFFAOYSA-N 0.000 description 1
- 230000008635 plant growth Effects 0.000 description 1
- 229940072033 potash Drugs 0.000 description 1
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 1
- 235000015320 potassium carbonate Nutrition 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000006479 redox reaction Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 150000003839 salts Chemical group 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 description 1
- 229960001763 zinc sulfate Drugs 0.000 description 1
- 229910000368 zinc sulfate Inorganic materials 0.000 description 1
Landscapes
- Saccharide Compounds (AREA)
Abstract
Description
Claims (3)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310632853.2A CN103626799B (zh) | 2013-12-03 | 2013-12-03 | 一种复合肌醇六磷酸糖醇酯螯合剂的制备 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310632853.2A CN103626799B (zh) | 2013-12-03 | 2013-12-03 | 一种复合肌醇六磷酸糖醇酯螯合剂的制备 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN103626799A CN103626799A (zh) | 2014-03-12 |
CN103626799B true CN103626799B (zh) | 2016-02-24 |
Family
ID=50208278
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201310632853.2A Active CN103626799B (zh) | 2013-12-03 | 2013-12-03 | 一种复合肌醇六磷酸糖醇酯螯合剂的制备 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN103626799B (zh) |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS63112993A (ja) * | 1986-10-29 | 1988-05-18 | Dai Ichi Kogyo Seiyaku Co Ltd | 酵素法による糖もしくは糖アルコ−ル脂肪酸エステルの製法 |
CN1037515A (zh) * | 1988-05-14 | 1989-11-29 | 周定华 | 肌醇六磷酸酯的生产工艺 |
CN1167113A (zh) * | 1996-03-27 | 1997-12-10 | 策卡有限公司 | 磷酸烷基酯或磷酸酰基二脱水1,4:3,6-d-葡糖醇酯及其制备方法和应用 |
CN1294128A (zh) * | 2000-10-30 | 2001-05-09 | 李国荣 | 一种植酸的生产工艺方法 |
CN101570485A (zh) * | 2008-04-30 | 2009-11-04 | 上海医药工业研究院 | 一种长链脂肪酸的糖醇酯及其分离提取方法和在抑制芳香化酶活性中的应用 |
-
2013
- 2013-12-03 CN CN201310632853.2A patent/CN103626799B/zh active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS63112993A (ja) * | 1986-10-29 | 1988-05-18 | Dai Ichi Kogyo Seiyaku Co Ltd | 酵素法による糖もしくは糖アルコ−ル脂肪酸エステルの製法 |
CN1037515A (zh) * | 1988-05-14 | 1989-11-29 | 周定华 | 肌醇六磷酸酯的生产工艺 |
CN1167113A (zh) * | 1996-03-27 | 1997-12-10 | 策卡有限公司 | 磷酸烷基酯或磷酸酰基二脱水1,4:3,6-d-葡糖醇酯及其制备方法和应用 |
CN1294128A (zh) * | 2000-10-30 | 2001-05-09 | 李国荣 | 一种植酸的生产工艺方法 |
CN101570485A (zh) * | 2008-04-30 | 2009-11-04 | 上海医药工业研究院 | 一种长链脂肪酸的糖醇酯及其分离提取方法和在抑制芳香化酶活性中的应用 |
Also Published As
Publication number | Publication date |
---|---|
CN103626799A (zh) | 2014-03-12 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN103588576B (zh) | 一种多功能肥料 | |
CN103193537B (zh) | 一种含黄棕腐植酸水溶肥料及其制备方法 | |
CN103145491A (zh) | 一种复合营养液配方及其制备方法 | |
CN104478574A (zh) | 一种含腐植酸浓缩螯合态微量元素肥料的制备方法 | |
CN107353142A (zh) | 一种植物营养液及其制备方法 | |
CN104557238A (zh) | 一种高效生物冲施肥 | |
CN109704876A (zh) | 一种水溶肥料增效组合物及其制备方法和应用 | |
CN104892206B (zh) | 一种高浓缩抗低温液体磷钾肥及其制备方法 | |
CN101381246B (zh) | 水培植物营养液及其生产工艺 | |
CN104177179A (zh) | 一种果树营养注射液及其制备方法 | |
CN104478573A (zh) | 一种用于种植山药的高效化肥 | |
CN102557822B (zh) | 一种用重结晶工艺制备含有机钛的过氧化尿素的方法 | |
CN102249814A (zh) | 一种以腐植酸尿素络合物为基质的液体肥料的制备方法 | |
CN104341245A (zh) | 一种玫瑰专用肥料 | |
CN106380008A (zh) | 一种用于碱性土壤的阻垢剂及其制备方法 | |
CN104788181A (zh) | 一种多元微量元素氨基酸螯合肥的生产方法 | |
CN106699274A (zh) | 一种磷酸硒钾有机液肥制备及使用方法 | |
CN103626799B (zh) | 一种复合肌醇六磷酸糖醇酯螯合剂的制备 | |
CN104892074A (zh) | 一种观赏类花卉专用肥及其制备方法 | |
CN104744093A (zh) | 一种花卉营养液 | |
CN102850101A (zh) | 一种富硒复合肥 | |
CN102557825B (zh) | 一种用微波螯合工艺制备含有机钛的微量元素肥料的方法 | |
CN104513105A (zh) | 一种高吸收率缓解肥 | |
CN107840717A (zh) | 一种复合液体肥 | |
CN103936525A (zh) | 一种提高化肥吸收率的添加剂 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
C41 | Transfer of patent application or patent right or utility model | ||
TR01 | Transfer of patent right |
Effective date of registration: 20161130 Address after: 530007 No. 17, pioneering Road, the Guangxi Zhuang Autonomous Region, Nanning Patentee after: NANNING HARWORLD BIOTECHNOLOGY Co.,Ltd. Address before: 530007 No. 17, pioneering Road, the Guangxi Zhuang Autonomous Region, Nanning Patentee before: Guangxi New Orientation Chemical Industry Co.,Ltd. |
|
EE01 | Entry into force of recordation of patent licensing contract |
Application publication date: 20140312 Assignee: Guangxi Zhongbo Warehousing Co.,Ltd. Assignor: NANNING HARWORLD BIOTECHNOLOGY Co.,Ltd. Contract record no.: X2024980007640 Denomination of invention: Preparation of a composite inositol hexaphosphate sugar ester chelating agent Granted publication date: 20160224 License type: Common License Record date: 20240620 |