CN103613979B - A kind of detergent for ink and preparation method thereof - Google Patents
A kind of detergent for ink and preparation method thereof Download PDFInfo
- Publication number
- CN103613979B CN103613979B CN201310515034.XA CN201310515034A CN103613979B CN 103613979 B CN103613979 B CN 103613979B CN 201310515034 A CN201310515034 A CN 201310515034A CN 103613979 B CN103613979 B CN 103613979B
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- Prior art keywords
- sodium
- ink
- auxiliary agent
- detergent
- acid
- Prior art date
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- 239000003599 detergent Substances 0.000 title claims abstract description 13
- 238000002360 preparation method Methods 0.000 title claims description 7
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 21
- MUBZPKHOEPUJKR-UHFFFAOYSA-N oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims abstract description 21
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- ZBCBWPMODOFKDW-UHFFFAOYSA-N Diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 claims abstract description 7
- UQEAIHBTYFGYIE-UHFFFAOYSA-N Hexamethyldisiloxane Chemical compound C[Si](C)(C)O[Si](C)(C)C UQEAIHBTYFGYIE-UHFFFAOYSA-N 0.000 claims abstract description 7
- VKYKSIONXSXAKP-UHFFFAOYSA-N Hexamethylenetetramine Chemical compound C1N(C2)CN3CN1CN2C3 VKYKSIONXSXAKP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229960004011 Methenamine Drugs 0.000 claims abstract description 7
- 229940048109 SODIUM METHYL COCOYL TAURATE Drugs 0.000 claims abstract description 7
- 229940048842 SODIUM XYLENESULFONATE Drugs 0.000 claims abstract description 7
- WXMKPNITSTVMEF-UHFFFAOYSA-M Sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims abstract description 7
- LSNNMFCWUKXFEE-UHFFFAOYSA-L Sulphite Chemical compound [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 claims abstract description 7
- 229940117013 Triethanolamine oleate Drugs 0.000 claims abstract description 7
- 229940008099 dimethicone Drugs 0.000 claims abstract description 7
- 235000013870 dimethyl polysiloxane Nutrition 0.000 claims abstract description 7
- 239000004205 dimethyl polysiloxane Substances 0.000 claims abstract description 7
- 235000010299 hexamethylene tetramine Nutrition 0.000 claims abstract description 7
- 239000004312 hexamethylene tetramine Substances 0.000 claims abstract description 7
- 235000006408 oxalic acid Nutrition 0.000 claims abstract description 7
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- KEAYESYHFKHZAL-UHFFFAOYSA-N sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000011734 sodium Substances 0.000 claims abstract description 7
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 7
- 235000010234 sodium benzoate Nutrition 0.000 claims abstract description 7
- 239000004299 sodium benzoate Substances 0.000 claims abstract description 7
- 238000002156 mixing Methods 0.000 claims description 14
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 11
- 239000002253 acid Substances 0.000 claims description 6
- 239000004359 castor oil Substances 0.000 claims description 6
- 235000019438 castor oil Nutrition 0.000 claims description 6
- 239000003153 chemical reaction reagent Substances 0.000 claims description 6
- 230000001808 coupling Effects 0.000 claims description 6
- 238000010168 coupling process Methods 0.000 claims description 6
- 238000005859 coupling reaction Methods 0.000 claims description 6
- BLRPTPMANUNPDV-UHFFFAOYSA-N silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 6
- 229910000077 silane Inorganic materials 0.000 claims description 6
- SLCVBVWXLSEKPL-UHFFFAOYSA-N 2,2-dimethylpropane-1,3-diol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 claims description 3
- 229940117969 NEOPENTYL GLYCOL Drugs 0.000 claims description 3
- 229940116315 Oxalic Acid Drugs 0.000 claims description 3
- KDVYCTOWXSLNNI-UHFFFAOYSA-N Para-tert-Butylbenzoic acid Chemical compound CC(C)(C)C1=CC=C(C(O)=O)C=C1 KDVYCTOWXSLNNI-UHFFFAOYSA-N 0.000 claims description 3
- 229960003885 Sodium Benzoate Drugs 0.000 claims description 3
- 230000003078 antioxidant Effects 0.000 claims description 3
- 239000003963 antioxidant agent Substances 0.000 claims description 3
- 229960004106 citric acid Drugs 0.000 claims description 3
- 235000015165 citric acid Nutrition 0.000 claims description 3
- 229940043237 diethanolamine Drugs 0.000 claims description 3
- 239000012467 final product Substances 0.000 claims description 3
- 229940075507 glyceryl monostearate Drugs 0.000 claims description 3
- 239000001788 mono and diglycerides of fatty acids Substances 0.000 claims description 3
- 150000008442 polyphenolic compounds Chemical class 0.000 claims description 3
- 235000013824 polyphenols Nutrition 0.000 claims description 3
- VBICKXHEKHSIBG-UHFFFAOYSA-N rac-1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims description 3
- 238000010792 warming Methods 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 2
- 240000007524 Camellia sinensis var. sinensis Species 0.000 claims 1
- 230000000254 damaging Effects 0.000 abstract description 2
- 238000010790 dilution Methods 0.000 abstract description 2
- 239000002360 explosive Substances 0.000 abstract description 2
- 231100000486 side effect Toxicity 0.000 abstract description 2
- 231100000331 toxic Toxicity 0.000 abstract description 2
- 239000003350 kerosene Substances 0.000 description 8
- 238000007639 printing Methods 0.000 description 8
- 238000004140 cleaning Methods 0.000 description 6
- 239000002904 solvent Substances 0.000 description 4
- 239000012459 cleaning agent Substances 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 241001122767 Theaceae Species 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000035943 smell Effects 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
Abstract
The invention discloses a kind of detergent for ink; it is characterized in that, be prepared by the raw materials in: OPEO 20 30, sodium sulfonate 58, diethanolamine 12, oxalic acid 12, sodium benzoate 57, sodium methyl cocoyl taurate 24, sodium xylene sulfonate 12, dimethicone 23, hexamethylenetetramine 12, citric acid 12, triethanolamine oleate 12, auxiliary agent 45, water 100 110；The present invention adds auxiliary agent, improves the processing performance of abluent, reduces its toxic and side effects and the pollution to environment；The present invention has an excellent dissolved dilution ability to ink, and detersive efficiency is high, nonhazardous, pollution-free, nonflammable explosive, little to printer rubber roll damaging action, easy to use, low cost.
Description
Technical field
The present invention relates to print cleaning technique field, particularly a kind of detergent for ink and preparation method thereof.
Background technology
Printing equipment needs the dirts such as routine cleaning greasy dirt and ink marks in process of production.Change ink kind time or print job complete after need the ink on ink roller to clean up, and softening drum, silk screen, galley and the type matrix on printer can be infected with ink in printing process, the quality of normal condition and leaflet for keeping printer is also tackled printing machinery and is carried out.
Existing detergent for ink is broadly divided into two big classes: a class is vapour, kerosene, and another kind of is to print special novel printing ink cleaning agent.
Gasoline and kerosene are a kind of wide spectrum Organic substance solvents, and proportion is little, and evaporation rate is fast, cheap.In existing printing house of China, major part also uses gasoline and kerosene to clean ink.A lot of shortcoming is there is: one is safety problem, and vapour oil flash only has twenties degree, if the ventilation equipment in printing Factory Building is bad, it is easy to situation of causing danger as detergent for ink, gasoline and kerosene；Two is pollution problem, and gasoline and kerosene, as a kind of organic solvent, have certain toxicity, if Long Term Contact, necessarily the environment to the healthy of workman and surrounding causes a certain degree of destruction.Novel printing ink cleaning agent is compared with gasoline and kerosene, and cleaning performance is good, and security performance is high, and the contamination hazard to human body and environment is little.Novel printing ink cleaning agent is typically to be made up of solvent, surfactant, auxiliary agent, water.The most conventional solvent is still from non-renewable solvent naphtha, such as kerosene, and abnormal smells from the patient is big, and degradability is poor, and environment still suffers from certain threat.
Summary of the invention
It is an object of the invention to provide a kind of detergent for ink and preparation method thereof.
In order to realize the purpose of the present invention, the present invention is implemented by below scheme:
A kind of detergent for ink, is prepared by the raw materials in: OPEO 20-30, sodium sulfonate 5-8, diethanolamine 1-2, oxalic acid 1-2, sodium benzoate 5-7, sodium methyl cocoyl taurate 2-4, sodium xylene sulfonate 1-2, dimethicone 2-3, hexamethylenetetramine 1-2, citric acid 1-2, triethanolamine oleate 1-2, auxiliary agent 4-5, water 100-110；
Described auxiliary agent is prepared by the raw materials in: Silane coupling reagent KH-570 2-3, castor oil acid 2-3, tea polyphenols 2-3, glyceryl monostearate 4-5, neopentyl glycol 2-3, p-tert-butyl benzoic acid 3-4, antioxidant 1035
1-2, ethanol 15-18；Preparation method is by Silane coupling reagent KH-570, castor oil acid, ethanol mixing, is heated to 60-70 DEG C, after stirring 20-30 minute, adds other residual components, be warming up to 80-85 DEG C, stirs 30 40 minutes, to obtain final product.
A kind of detergent for ink of the present invention, is made up of step in detail below:
(1) at room temperature adding in mixing kettle by sodium sulfonate, diethanolamine, oxalic acid, sodium xylene sulfonate, dimethicone, hexamethylenetetramine, citric acid, add in mixing kettle after the water of half amount is heated to 65-75 DEG C, stirring is to being completely dissolved；
(2) OPEO, sodium benzoate, sodium methyl cocoyl taurate, triethanolamine oleate are added in mixing kettle, add the water being heated to 80-90 DEG C of surplus, stir 4-6 minute with the speed of 1300-1400 rev/min；
(3) finally auxiliary agent and remaining residual components are added in mixing kettle, stir, natural cooling.
The excellent effect of the present invention is: the present invention adds auxiliary agent, improves the processing performance of abluent, reduces its toxic and side effects and the pollution to environment；The present invention has an excellent dissolved dilution ability to ink, and detersive efficiency is high, nonhazardous, pollution-free, nonflammable explosive, little to printer rubber roll damaging action, easy to use, low cost.
Detailed description of the invention
Below by instantiation, the present invention is described in detail.
A kind of detergent for ink, is made up of the raw material of following weight portion (kilogram): OPEO 20, sodium sulfonate 5, diethanolamine 1, oxalic acid 1, sodium benzoate 5, sodium methyl cocoyl taurate 2, sodium xylene sulfonate 1, dimethicone 2, hexamethylenetetramine 1, citric acid 1, triethanolamine oleate 1, auxiliary agent 4, water 100；
Described auxiliary agent is made up of the raw material of following weight portion (kilogram): Silane coupling reagent KH-570 3, castor oil acid 2, tea polyphenols 2, glyceryl monostearate 4, neopentyl glycol 2, p-tert-butyl benzoic acid 4, antioxidant 1035
1, ethanol 15；Preparation method is by Silane coupling reagent KH-570, castor oil acid, ethanol mixing, is heated to 60-70 DEG C, after stirring 20-30 minute, adds other residual components, be warming up to 80-85 DEG C, stirs 30 40 minutes, to obtain final product.
A kind of detergent for ink of the present invention, is made up of step in detail below:
(1) at room temperature adding in mixing kettle by sodium sulfonate, diethanolamine, oxalic acid, sodium xylene sulfonate, dimethicone, hexamethylenetetramine, citric acid, add in mixing kettle after the water of half amount is heated to 65-75 DEG C, stirring is to being completely dissolved；
(2) OPEO, sodium benzoate, sodium methyl cocoyl taurate, triethanolamine oleate are added in mixing kettle, add the water being heated to 80-90 DEG C of surplus, stir 4-6 minute with the speed of 1300-1400 rev/min；
Being applied to by ink on the stainless steel metal thin slice of certain mass, dry under naturalness, be placed in by steel disc in the beaker filling abluent, after soaking 5 minutes, more at the uniform velocity vibrate 5 minutes at 25 DEG C, obtaining clean dirt rate is 92.5%, and cleansing power is good.With this abluent with compared with gasoline, kerosene, rubber cloth increases the service life 2 years, and ink roller can increase the service life 3 years.
Claims (2)
1. a detergent for ink; it is characterized in that, be prepared by the raw materials in: OPEO 20-30, sodium sulfonate 5-8, diethanolamine 1-2, oxalic acid 1-2, sodium benzoate 5-7, sodium methyl cocoyl taurate 2-4, sodium xylene sulfonate 1-2, dimethicone 2-3, hexamethylenetetramine 1-2, citric acid 1-2, triethanolamine oleate 1-2, auxiliary agent 4-5, water 100-110；
Described auxiliary agent is prepared by the raw materials in: Silane coupling reagent KH-570 2-3, castor oil acid 2-3, tea polyphenols 2-3, glyceryl monostearate 4-5, neopentyl glycol 2-3, p-tert-butyl benzoic acid 3-4, antioxidant 1035 1-2, ethanol 15-18；Preparation method is by Silane coupling reagent KH-570, castor oil acid, ethanol mixing, is heated to 60-70 DEG C, after stirring 20-30 minute, adds other residual components, be warming up to 80-85 DEG C, stirs 30 40 minutes, to obtain final product.
A kind of detergent for ink, it is characterised in that be made up of step in detail below:
(1) at room temperature adding in mixing kettle by sodium sulfonate, diethanolamine, oxalic acid, sodium xylene sulfonate, dimethicone, hexamethylenetetramine, citric acid, add in mixing kettle after the water of half amount is heated to 65-75 DEG C, stirring is to being completely dissolved；
(2) OPEO, sodium benzoate, sodium methyl cocoyl taurate, triethanolamine oleate are added in mixing kettle, add the water being heated to 80-90 DEG C of surplus, stir 4-6 minute with the speed of 1300-1400 rev/min；
(3) finally auxiliary agent is added in mixing kettle, stir, natural cooling.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310515034.XA CN103613979B (en) | 2013-10-28 | A kind of detergent for ink and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310515034.XA CN103613979B (en) | 2013-10-28 | A kind of detergent for ink and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103613979A CN103613979A (en) | 2014-03-05 |
| CN103613979B true CN103613979B (en) | 2016-11-30 |
Family
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101434764A (en) * | 2007-11-15 | 2009-05-20 | 中国石油化工股份有限公司 | Printing ink cleaning agent |
| CN101492579A (en) * | 2008-01-24 | 2009-07-29 | 中山火炬职业技术学院 | Printing ink cleaning agent |
| CN101638532A (en) * | 2009-08-29 | 2010-02-03 | 茂名学院 | Water-solubility printing ink washing agent |
| CN101684211A (en) * | 2008-09-28 | 2010-03-31 | 魏发灿 | Environment protection type energy-saving detergent for ink |
| CN102408773A (en) * | 2011-09-26 | 2012-04-11 | 深圳市创明电池技术有限公司 | PVC film ink cleaning agent and preparation method thereof |
| CN102888140A (en) * | 2011-07-20 | 2013-01-23 | 深圳市裕同印刷股份有限公司 | Formula and preparation process of environment-friendly printing ink cleaning agent |
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101434764A (en) * | 2007-11-15 | 2009-05-20 | 中国石油化工股份有限公司 | Printing ink cleaning agent |
| CN101492579A (en) * | 2008-01-24 | 2009-07-29 | 中山火炬职业技术学院 | Printing ink cleaning agent |
| CN101684211A (en) * | 2008-09-28 | 2010-03-31 | 魏发灿 | Environment protection type energy-saving detergent for ink |
| CN101638532A (en) * | 2009-08-29 | 2010-02-03 | 茂名学院 | Water-solubility printing ink washing agent |
| CN102888140A (en) * | 2011-07-20 | 2013-01-23 | 深圳市裕同印刷股份有限公司 | Formula and preparation process of environment-friendly printing ink cleaning agent |
| CN102408773A (en) * | 2011-09-26 | 2012-04-11 | 深圳市创明电池技术有限公司 | PVC film ink cleaning agent and preparation method thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| CB03 | Change of inventor or designer information |
Inventor after: Pan Jianli Inventor before: Song Yuchun |
|
| TA01 | Transfer of patent application right |
Effective date of registration: 20161008 Address after: The river town of Luojiang District of Quanzhou City, Fujian province 362013 new village to mill No. 4 Applicant after: Pan Jianli Address before: 233000 No. 404 South Daqing Road, hi tech Zone, Anhui, Bengbu Applicant before: Anhui Topusen Battery Co., Ltd. |
|
| GR01 | Patent grant | ||
| CB03 | Change of inventor or designer information |
Inventor after: Xu Yu Inventor after: Zhang Chaowu Inventor before: Pan Jianli |
|
| TR01 | Transfer of patent right |
Effective date of registration: 20170331 Address after: 523625 Dongguan, Guangdong Zhangmutou town, Luo Luo community New Town Plaza, No. 246 Patentee after: Dongguan Huasheng cleaning agent technology Co., Ltd. Address before: The river town of Luojiang District of Quanzhou City, Fujian province 362013 new village to mill No. 4 Patentee before: Pan Jianli |
|
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20161130 Termination date: 20191028 |