CN103613979A - Ink cleaning agent and preparation method thereof - Google Patents
Ink cleaning agent and preparation method thereof Download PDFInfo
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- CN103613979A CN103613979A CN201310515034.XA CN201310515034A CN103613979A CN 103613979 A CN103613979 A CN 103613979A CN 201310515034 A CN201310515034 A CN 201310515034A CN 103613979 A CN103613979 A CN 103613979A
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- sodium
- ink
- auxiliary agent
- acid
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- 238000002360 preparation method Methods 0.000 title claims description 7
- 239000012459 cleaning agent Substances 0.000 title abstract description 7
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims abstract description 21
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 21
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims abstract description 14
- VKYKSIONXSXAKP-UHFFFAOYSA-N hexamethylenetetramine Chemical compound C1N(C2)CN3CN1CN2C3 VKYKSIONXSXAKP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- -1 polyoxyethylene octylphenol Polymers 0.000 claims abstract description 8
- ICLYJLBTOGPLMC-KVVVOXFISA-N (z)-octadec-9-enoate;tris(2-hydroxyethyl)azanium Chemical compound OCCN(CCO)CCO.CCCCCCCC\C=C/CCCCCCCC(O)=O ICLYJLBTOGPLMC-KVVVOXFISA-N 0.000 claims abstract description 7
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 7
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 claims abstract description 7
- 235000010299 hexamethylene tetramine Nutrition 0.000 claims abstract description 7
- 239000004312 hexamethylene tetramine Substances 0.000 claims abstract description 7
- 235000006408 oxalic acid Nutrition 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 239000011734 sodium Substances 0.000 claims abstract description 7
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 7
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims abstract description 7
- 235000010234 sodium benzoate Nutrition 0.000 claims abstract description 7
- 239000004299 sodium benzoate Substances 0.000 claims abstract description 7
- 229940048109 sodium methyl cocoyl taurate Drugs 0.000 claims abstract description 7
- 229940048842 sodium xylenesulfonate Drugs 0.000 claims abstract description 7
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims abstract description 7
- 229940117013 triethanolamine oleate Drugs 0.000 claims abstract description 7
- QUCDWLYKDRVKMI-UHFFFAOYSA-M sodium;3,4-dimethylbenzenesulfonate Chemical compound [Na+].CC1=CC=C(S([O-])(=O)=O)C=C1C QUCDWLYKDRVKMI-UHFFFAOYSA-M 0.000 claims abstract description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
- 239000003599 detergent Substances 0.000 claims description 11
- 238000002156 mixing Methods 0.000 claims description 11
- 238000003756 stirring Methods 0.000 claims description 11
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims description 6
- XDLMVUHYZWKMMD-UHFFFAOYSA-N 3-trimethoxysilylpropyl 2-methylprop-2-enoate Chemical compound CO[Si](OC)(OC)CCCOC(=O)C(C)=C XDLMVUHYZWKMMD-UHFFFAOYSA-N 0.000 claims description 6
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 6
- 239000003153 chemical reaction reagent Substances 0.000 claims description 6
- 230000008878 coupling Effects 0.000 claims description 6
- 238000010168 coupling process Methods 0.000 claims description 6
- 238000005859 coupling reaction Methods 0.000 claims description 6
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims description 6
- WBHHMMIMDMUBKC-QJWNTBNXSA-N ricinoleic acid Chemical compound CCCCCC[C@@H](O)C\C=C/CCCCCCCC(O)=O WBHHMMIMDMUBKC-QJWNTBNXSA-N 0.000 claims description 6
- 229960003656 ricinoleic acid Drugs 0.000 claims description 6
- FEUQNCSVHBHROZ-UHFFFAOYSA-N ricinoleic acid Natural products CCCCCCC(O[Si](C)(C)C)CC=CCCCCCCCC(=O)OC FEUQNCSVHBHROZ-UHFFFAOYSA-N 0.000 claims description 6
- 229910000077 silane Inorganic materials 0.000 claims description 6
- 229920002545 silicone oil Polymers 0.000 claims description 6
- KDVYCTOWXSLNNI-UHFFFAOYSA-N 4-t-Butylbenzoic acid Chemical compound CC(C)(C)C1=CC=C(C(O)=O)C=C1 KDVYCTOWXSLNNI-UHFFFAOYSA-N 0.000 claims description 3
- 229940075507 glyceryl monostearate Drugs 0.000 claims description 3
- 239000003112 inhibitor Substances 0.000 claims description 3
- 239000001788 mono and diglycerides of fatty acids Substances 0.000 claims description 3
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 claims description 3
- 230000003647 oxidation Effects 0.000 claims description 3
- 238000007254 oxidation reaction Methods 0.000 claims description 3
- 229960003885 sodium benzoate Drugs 0.000 claims description 3
- 238000010792 warming Methods 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 2
- 238000007639 printing Methods 0.000 abstract description 13
- 230000000694 effects Effects 0.000 abstract description 4
- 238000000034 method Methods 0.000 abstract description 4
- 230000006378 damage Effects 0.000 abstract description 2
- 239000002360 explosive Substances 0.000 abstract description 2
- 231100000331 toxic Toxicity 0.000 abstract description 2
- 230000002588 toxic effect Effects 0.000 abstract description 2
- 229940043237 diethanolamine Drugs 0.000 abstract 1
- 229940008099 dimethicone Drugs 0.000 abstract 1
- 235000013870 dimethyl polysiloxane Nutrition 0.000 abstract 1
- 239000004205 dimethyl polysiloxane Substances 0.000 abstract 1
- 239000003344 environmental pollutant Substances 0.000 abstract 1
- 229960004011 methenamine Drugs 0.000 abstract 1
- 239000002574 poison Substances 0.000 abstract 1
- 231100000614 poison Toxicity 0.000 abstract 1
- 231100000719 pollutant Toxicity 0.000 abstract 1
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 abstract 1
- 239000000344 soap Substances 0.000 abstract 1
- 239000003350 kerosene Substances 0.000 description 8
- 238000004140 cleaning Methods 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- 229910000831 Steel Inorganic materials 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 230000000254 damaging effect Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 230000002110 toxicologic effect Effects 0.000 description 1
- 231100000027 toxicology Toxicity 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
Landscapes
- Detergent Compositions (AREA)
Abstract
The invention discloses an ink cleaning agent, which is characterized by comprising the following raw materials by weight: 20-30 parts of polyoxyethylene octylphenol ether, 5-8 parts of sodium sulfonate, 1-2 parts of diethanol amine, 1-2 parts of oxalic acid, 5-7 parts of sodium benzoate, 2-4 parts of sodium methyl cocoyl taurate, 1-2 parts of sodium xylene sulfonate, 2-3 parts of dimethicone, 1-2 parts of hexamethylene tetramine, 1-2 parts of citric acid, 1-2 parts of triethanolamine oleate soap, 4-5 parts of an auxiliary agent and 100-110 parts of water. The auxiliary agent added in the invention improves the process performances of the cleaning agent, reduces the toxic and side effect and pollution to the environment. The ink cleaning agent provided by the invention has the advanategs of good ability to dissolve and dilute ink, high pollutant removal efficiency, no poison, no pollution, no inflammable or explosive property, little damage effect on roller of a printing machine, convenience for usage and low cost.
Description
Technical field
The present invention relates to print cleaning technique field, particularly a kind of detergent for ink and preparation method thereof.
Background technology
Printing equipment needs the dirts such as routine cleaning greasy dirt and ink marks in process of production.When changing ink kind or print job need the ink on ink roller to clean up after completing, and softening drum, silk screen, press plate and type matrix on printing press can be infected with ink in printing process, for keeping the standard state of printing press and the quality of printed matter also to tackle printing machinery, clean.
Existing detergent for ink is mainly divided into two large classes: a class is vapour, kerosene, and another kind of is the special-purpose novel printing ink cleaning agent of printing.
Gasoline and kerosene are a kind of wide spectrum organism solvents, and proportion is little, and evaporation rate is fast, cheap.In the existing printing house of China, major part is also cleaned ink with gasoline and kerosene.As detergent for ink, there are a lot of shortcomings in gasoline and kerosene: the one, and safety problem, vapour oil flash only has twenties degree, if the ventilation equipment in printing factory building is bad, is easy to the situation of causing danger; The 2nd, pollution problem, gasoline and kerosene, as a kind of organic solvent, have certain toxicity, if Long Term Contact must cause destruction to a certain degree to the healthy of workman and environment around.Novel printing ink cleaning agent is compared with kerosene with gasoline, and cleaning performance is good, and safety performance is high, and little to the pollution hazard of human body and environment.Novel printing ink cleaning agent normally consists of solvent, tensio-active agent, auxiliary agent, water.At present conventional solvent is still from non-renewable solvent oil, and such as kerosene, smell is large, and degradation property is poor, and environment is still existed to certain threat.
Summary of the invention
The object of this invention is to provide a kind of detergent for ink and preparation method thereof.
In order to realize object of the present invention, the present invention passes through following scheme implementation:
A detergent for ink, is made by the raw material of following weight part: polyoxyethylene octylphenol ether 20-30, sodium sulfonate 5-8, diethanolamine 1-2, oxalic acid 1-2, Sodium Benzoate 5-7, sodium methyl cocoyl taurate 2-4, sodium xylene sulfonate 1-2, dimethyl silicone oil 2-3, hexamethylenetetramine 1-2, citric acid 1-2, triethanolamine oleate 1-2, auxiliary agent 4-5, water 100-110;
Described auxiliary agent is made by the raw material of following weight part: Silane coupling reagent KH-570 2-3, ricinolic acid 2-3, tea-polyphenol 2-3, glyceryl monostearate 4-5, neopentyl glycol 2-3, p-tert-butyl benzoic acid 3-4, oxidation inhibitor 1035 1-2, ethanol 15-18; Preparation method mixes Silane coupling reagent KH-570, ricinolic acid, ethanol, is heated to 60-70 ℃, stirs after 20-30 minute, then adds other remaining component, is warming up to 80-85 ℃, stirs 30-40 minutes, obtains.
A kind of detergent for ink of the present invention, by following concrete steps, made:
(1) at room temperature sodium sulfonate, diethanolamine, oxalic acid, sodium xylene sulfonate, dimethyl silicone oil, hexamethylenetetramine, citric acid are added in mixing kettle, add in mixing kettle after the water of half amount is heated to 65-75 ℃, be stirred to completely and dissolve;
(2) polyoxyethylene octylphenol ether, Sodium Benzoate, sodium methyl cocoyl taurate, triethanolamine oleate are added in mixing kettle, add the water of 80-90 ℃ of being heated to of surplus, with the speed of 1300-1400 rev/min, stir 4-6 minute;
(3) finally auxiliary agent and all the other remaining components are added in mixing kettle, stir, naturally cooling.
Excellent effect of the present invention is: the present invention adds auxiliary agent, has improved the processing performance of clean-out system, reduces its toxic side effect and the pollution to environment; The present invention has good dissolved dilution ability to ink, and detersive efficiency is high, and toxicological harmless, pollution-free is nonflammable explosive, and little, easy to use to printing press rubber roll damaging action, cost is low.
Embodiment
Below by specific examples, the present invention is described in detail.
A detergent for ink, by following weight part (kilogram) raw material make: polyoxyethylene octylphenol ether 20, sodium sulfonate 5, diethanolamine 1, oxalic acid 1, Sodium Benzoate 5, sodium methyl cocoyl taurate 2, sodium xylene sulfonate 1, dimethyl silicone oil 2, hexamethylenetetramine 1, citric acid 1, triethanolamine oleate 1, auxiliary agent 4, water 100;
Described auxiliary agent by following weight part (kilogram) raw material make: Silane coupling reagent KH-570 3, ricinolic acid 2, tea-polyphenol 2, glyceryl monostearate 4, neopentyl glycol 2, p-tert-butyl benzoic acid 4, oxidation inhibitor 1,035 1, ethanol 15; Preparation method mixes Silane coupling reagent KH-570, ricinolic acid, ethanol, is heated to 60-70 ℃, stirs after 20-30 minute, then adds other remaining component, is warming up to 80-85 ℃, stirs 30-40 minutes, obtains.
A kind of detergent for ink of the present invention, by following concrete steps, made:
(1) at room temperature sodium sulfonate, diethanolamine, oxalic acid, sodium xylene sulfonate, dimethyl silicone oil, hexamethylenetetramine, citric acid are added in mixing kettle, add in mixing kettle after the water of half amount is heated to 65-75 ℃, be stirred to completely and dissolve;
(2) polyoxyethylene octylphenol ether, Sodium Benzoate, sodium methyl cocoyl taurate, triethanolamine oleate are added in mixing kettle, add the water of 80-90 ℃ of being heated to of surplus, with the speed of 1300-1400 rev/min, stir 4-6 minute;
Ink is applied on the stainless steel metal thin slice of certain mass, under state of nature, dries, steel disc is placed in to the beaker that fills clean-out system, at 25 ℃, soak after 5 minutes, more at the uniform velocity vibrate 5 minutes, obtaining cleaning soil removal efficiency is 92.5%, and cleansing power is good.With this clean-out system with gasoline, kerosene, compare, rubber cloth increases the service life 2 years, ink roller can increase the service life 3 years.
Claims (2)
1. a detergent for ink, it is characterized in that, by the raw material of following weight part, made: polyoxyethylene octylphenol ether 20-30, sodium sulfonate 5-8, diethanolamine 1-2, oxalic acid 1-2, Sodium Benzoate 5-7, sodium methyl cocoyl taurate 2-4, sodium xylene sulfonate 1-2, dimethyl silicone oil 2-3, hexamethylenetetramine 1-2, citric acid 1-2, triethanolamine oleate 1-2, auxiliary agent 4-5, water 100-110;
Described auxiliary agent is made by the raw material of following weight part: Silane coupling reagent KH-570 2-3, ricinolic acid 2-3, tea-polyphenol 2-3, glyceryl monostearate 4-5, neopentyl glycol 2-3, p-tert-butyl benzoic acid 3-4, oxidation inhibitor 1035 1-2, ethanol 15-18; Preparation method mixes Silane coupling reagent KH-570, ricinolic acid, ethanol, is heated to 60-70 ℃, stirs after 20-30 minute, then adds other remaining component, is warming up to 80-85 ℃, stirs 30-40 minutes, obtains.
2. a kind of detergent for ink according to claim 1, is characterized in that, by following concrete steps, is made:
(1) at room temperature sodium sulfonate, diethanolamine, oxalic acid, sodium xylene sulfonate, dimethyl silicone oil, hexamethylenetetramine, citric acid are added in mixing kettle, add in mixing kettle after the water of half amount is heated to 65-75 ℃, be stirred to completely and dissolve;
(2) polyoxyethylene octylphenol ether, Sodium Benzoate, sodium methyl cocoyl taurate, triethanolamine oleate are added in mixing kettle, add the water of 80-90 ℃ of being heated to of surplus, with the speed of 1300-1400 rev/min, stir 4-6 minute;
(3) finally auxiliary agent and all the other remaining components are added in mixing kettle, stir, naturally cooling.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310515034.XA CN103613979B (en) | 2013-10-28 | A kind of detergent for ink and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310515034.XA CN103613979B (en) | 2013-10-28 | A kind of detergent for ink and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103613979A true CN103613979A (en) | 2014-03-05 |
| CN103613979B CN103613979B (en) | 2016-11-30 |
Family
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106833106A (en) * | 2017-03-21 | 2017-06-13 | 南宁东印时代广告有限公司 | Printing ink washing agent |
| CN110804501A (en) * | 2019-11-15 | 2020-02-18 | 南京魄力倍清洁科技有限公司 | Efficient environment-friendly color tracing acidic cleaning agent |
| CN112322396A (en) * | 2020-12-01 | 2021-02-05 | 李帅谕 | Barrel cleaning agent special for preventing foaming |
| CN113234345A (en) * | 2021-05-26 | 2021-08-10 | 中山市富日印刷材料有限公司 | Environment-friendly efficient cleaning agent and preparation method thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101434764A (en) * | 2007-11-15 | 2009-05-20 | 中国石油化工股份有限公司 | Printing ink cleaning agent |
| CN101492579A (en) * | 2008-01-24 | 2009-07-29 | 中山火炬职业技术学院 | Printing ink cleaning agent |
| CN101638532A (en) * | 2009-08-29 | 2010-02-03 | 茂名学院 | Water-solubility printing ink washing agent |
| CN101684211A (en) * | 2008-09-28 | 2010-03-31 | 魏发灿 | Environment protection type energy-saving detergent for ink |
| CN102408773A (en) * | 2011-09-26 | 2012-04-11 | 深圳市创明电池技术有限公司 | PVC film ink cleaning agent and preparation method thereof |
| CN102888140A (en) * | 2011-07-20 | 2013-01-23 | 深圳市裕同印刷股份有限公司 | Formula and preparation process of environment-friendly printing ink cleaning agent |
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101434764A (en) * | 2007-11-15 | 2009-05-20 | 中国石油化工股份有限公司 | Printing ink cleaning agent |
| CN101492579A (en) * | 2008-01-24 | 2009-07-29 | 中山火炬职业技术学院 | Printing ink cleaning agent |
| CN101684211A (en) * | 2008-09-28 | 2010-03-31 | 魏发灿 | Environment protection type energy-saving detergent for ink |
| CN101638532A (en) * | 2009-08-29 | 2010-02-03 | 茂名学院 | Water-solubility printing ink washing agent |
| CN102888140A (en) * | 2011-07-20 | 2013-01-23 | 深圳市裕同印刷股份有限公司 | Formula and preparation process of environment-friendly printing ink cleaning agent |
| CN102408773A (en) * | 2011-09-26 | 2012-04-11 | 深圳市创明电池技术有限公司 | PVC film ink cleaning agent and preparation method thereof |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106833106A (en) * | 2017-03-21 | 2017-06-13 | 南宁东印时代广告有限公司 | Printing ink washing agent |
| CN110804501A (en) * | 2019-11-15 | 2020-02-18 | 南京魄力倍清洁科技有限公司 | Efficient environment-friendly color tracing acidic cleaning agent |
| CN112322396A (en) * | 2020-12-01 | 2021-02-05 | 李帅谕 | Barrel cleaning agent special for preventing foaming |
| CN113234345A (en) * | 2021-05-26 | 2021-08-10 | 中山市富日印刷材料有限公司 | Environment-friendly efficient cleaning agent and preparation method thereof |
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Inventor after: Pan Jianli Inventor before: Song Yuchun |
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Effective date of registration: 20161008 Address after: The river town of Luojiang District of Quanzhou City, Fujian province 362013 new village to mill No. 4 Applicant after: Pan Jianli Address before: 233000 No. 404 South Daqing Road, hi tech Zone, Anhui, Bengbu Applicant before: Anhui Topusen Battery Co., Ltd. |
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Effective date of registration: 20170331 Address after: 523625 Dongguan, Guangdong Zhangmutou town, Luo Luo community New Town Plaza, No. 246 Patentee after: Dongguan Huasheng cleaning agent technology Co., Ltd. Address before: The river town of Luojiang District of Quanzhou City, Fujian province 362013 new village to mill No. 4 Patentee before: Pan Jianli |
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