CN103609714A - Production method for plant-based milk powder - Google Patents

Production method for plant-based milk powder Download PDF

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Publication number
CN103609714A
CN103609714A CN201310638400.0A CN201310638400A CN103609714A CN 103609714 A CN103609714 A CN 103609714A CN 201310638400 A CN201310638400 A CN 201310638400A CN 103609714 A CN103609714 A CN 103609714A
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milk powder
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CN103609714B (en
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李柱平
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Xie Junjie
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BEIJING JINGGUANGHE BIOTECHNOLOGY Co Ltd
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Abstract

The invention relates to the production method for plant-based milk powder. According to the method, grain processed byproducts or whole grain seeds serve as raw materials. The method comprises the following steps: performing pretreatment on edible parts of plants, removing stench from the plants, depolymerizing plant globulin subunits, performing physical fracture on long peptide chains of plant globulin, binding small protein molecules with non-polar groups, performing ionization treatment on protein, and emulsifying to obtain the plant-based milk powder. By the method, an out-dated grain processing mode is changed; the utilization rate of grains is greatly improved; a whole ecological industry chain is created; moreover, the product, namely plant-based milk or plant-based milk powder, produced by the method is similar to animal milk.

Description

A kind of production method of plant base milk powder
Technical field
The production method that the present invention relates to a kind of plant base milk powder, belongs to food processing field.
Background technology
The product such as current existing soymilk, cereal are with milk, still rest on the primary stage, to adding the element of cereal in the simple physical processing of soybean or milk, can not solve the problem of further processing of grains and comprehensive utilization completely, in grain processing, can produce some byproducts, in many byproducts, contain abundant nutritional labeling, these valuable resources are not well utilized, and in these byproducts, often contain more vitamin, mineral matter and the plant function factor.Byproduct after grain fine finishining is because the problems such as coarse, stench taste, structure indefinite form are used as feed mostly, and part byproduct deep processing degree is also very limited, and this has just caused great waste; Make the food after processing, nutritive value is had a greatly reduced quality.
Summary of the invention
In order significantly to improve grain utilization rate, present inventor has carried out a large amount of explorations and innovation in grain processing different aspects, a kind of production method of plant base milk powder is provided, really accomplish to get rid of the weed and keep the flower of the leek, make grain processing reduce the generation of byproduct as far as possible, nutritious composition is remained completely, changed the backward pattern of grain processing, greatly improve the utilization rate of grain, createed a complete ecological industrial chain
And the product that this method is produced shows with the form of class animal milk---plant base breast or plant base milk powder.
The technical scheme that the present invention solves the problems of the technologies described above is as follows: a kind of production method of plant base milk powder, comprising:
1) pre-treatment of plant edible part: take cereal processed side product or whole grain cereal seed is raw material, in above-mentioned raw materials, all contain abundant cereal crude protein, add water agitation grinding more than 30 minutes, the amount ratio of raw material and water is greater than 1:7, obtain the juice that contains cereal crude protein, again the juice that contains cereal crude protein is carried out to ultra-fine grinding, make particle diameter > 80 orders of raw material;
2) the stench taste of removal plant: rare alcohol buffer solution is joined to 1), in the juice after pulverizing, 30 ℃ are stirred 10~170 minutes, and the rare alcohol buffer solution of centrifugal removal obtains dry, adds the deionized water and stirring of 2~5 times of dry biomass even, obtains slurries;
3) in the slurries that the depolymerization of phytogloibulin subunit: to 2) obtain, add depolymerization liquid, 30~40 ℃ of insulated and stirred 5~40 minutes, it is 3~6.6 rear washing 2~3 times that deionized water regulates pH, is filtered dry standbyly, obtains material 1;
4) physical rupture of the long peptide chain of phytogloibulin: add water adjusting concentration to 10% in material 1, then add sodium acid carbonate adjust pH to 7.8~8.2, agitating heating, pumps into material 1 in high speed shear tank and carry out high speed shear, obtains material 2;
5) combination of small protein molecule and non-polar group: material 2 temperature are increased to 75 ℃, add organic carbonate and catalyst, stir insulation 15 minutes, obtain material 3;
6) protein ionize process: by material 3 Vacuum Concentrations to protein content 35%~45%, add sylvite or sodium salt, the addition of described sylvite or sodium salt accounts for 0.04%~0.08% of material 3 quality, at 30~40 ℃, stirs 10~80 minutes, obtains colloidal material 4;
7) emulsification treatment: according to required product specification, by adding wall material, adjust protein content in colloidal material 4, after homogeneous, sterilizing, become plant base emulsion, solid concentration is 30%~40%, plant base emulsion is the stable suspension liquid that the mixture of cereal various nutrients forms by self-emulsifying, plant base emulsion is spray dried to powdery lower than 160 ℃, obtains plant base milk powder.
On the basis of technique scheme, the present invention can also do following improvement.
Further, 1) in, described cereal processed side product is one or more the mixture in gluten, potato starch parting liquid, wheat embryo, dregs of beans, rice bran, maize germ, wheat, rice, soybean.
Further, 2) in, described rare alcohol buffer solution is (0.1~5) by mass ratio: (0.1~10): (0.01~0.5): the bamboo charcoal particle of (0.01~0.03), ethanol, NaOH and ferrate form.
The beneficial effect that adopts above-mentioned further scheme is to add rare alcohol buffer solution can eliminate little molecule aldehyde and the ketone relevant to the stench taste of plant.
Further, 3) in, described depolymerization liquid is (0.1~3) by mass ratio: (0.01~0.5): the fumaric acid of (0.01~0.2), sulphite and cysteine form.
The beneficial effect that adopts above-mentioned further scheme is with fumaric acid, sulphite and cysteine, to destroy the hydrogen bond of peptide interchain, makes peptide chain not in polymerization, reaches the effect of phytogloibulin matter subunit depolymerization.
Further, 4) in, described in be heated with stirring to 70~75 ℃;
The beneficial effect that adopts above-mentioned further scheme is in the time of 70~75 ℃, and peptide chain is opened and is wire;
Further, 4) in, the condition of described high speed shear: rotating speed is 1430~1500 revs/min, shear gap is 1~5 micron, at 70~75 ℃ of down cuts, stirs 20 minutes;
Further, 5) in, described organic carbonate is that carbon number is one or more the mixture in 8~26 aliphatic acid, the addition of described organic carbonate accounts for 0.1~0.8% of material 2 quality.
Further, 5) in, described catalyst is metaphosphoric acid salt, the addition of described catalyst accounts for 0.05%~0.3% of material 2 quality.
Further, 6) in, described sylvite is potassium citrate or potassium chloride, described sodium salt is sodium acid carbonate or sodium acetate;
Further, 7) in, described wall material is one or more mixture in dextrin, beta-schardinger dextrin-, converted starch;
The invention has the beneficial effects as follows:
The feature of the product utilization plants such as existing vegetable protein beverage itself is processed, and as coconut milk, soymilk, peanut milk etc., these products lack versatility, can not be as the raw material of industry as milk.Personal characteristics (mainly referring to local flavor aspect) how to remove plant itself retains its general character (nutrition aspect), and finally to form structure be great advantage of the present invention with stable components, the relative cheap bulk raw material of cost.We can produce same composition, constitutionally stable product with different vegetable raw materials; As ox, eat different feeds and only can extrude (this is milk and the milk powder prerequisite of doing the raw material of industry) milk.
Compared with prior art, the inventive method can be converted into plant edible part " milk ", also find no at present identical technology, and the present invention be take food processing byproducts as primary raw material (add and also can independently carry out production and processing man-hour at use raw grain), in process, reduced to greatest extent the personal characteristics of each Plants itself, the function of simulated animal mammary gland, by the even proportioning of Different Nutrition composition emulsification completely, directly produce milk or milk, finally make plant base breast or plant base milk powder.
The present invention has realized the preliminary industrialization phase that machinery is given milk.For the productive manpower, the mechanization of milk are laid a good foundation.
The specific embodiment
Below principle of the present invention and feature are described, example, only for explaining the present invention, is not intended to limit scope of the present invention.
Implementation column 1
1) by the 1:2:7 mixing in mass ratio of wheat, rice, soybean (raw grain), obtain maslin, add water agitation grinding 50 minutes, the amount ratio of maslin and water is 1:8, obtain the juice that contains cereal crude protein, again the juice that contains cereal crude protein is carried out to ultra-fine grinding, make particle diameter > 80 orders of raw material;
2) rare alcohol buffer solution being joined to 1) in juice after pulverizing, 30 ℃ are stirred 70 minutes, and the rare alcohol buffer solution of centrifugal removal obtains dry, adds the deionized water and stirring of 2 dry biomass even, obtains slurries; The bamboo charcoal particle that rare alcohol buffer solution is 2:1:0.02:0.02 by mass ratio, ethanol, solid sodium hydroxide and the solid potassium ferrate of 95% concentration form, and the addition of rare alcohol buffer solution is 1) in 3 times of cereal mixture quality.
3) to 2) add depolymerization liquid in the slurries that obtain, 30 ℃ of insulated and stirred 40 minutes, it is 5.6 rear washing 2 times that deionized water regulates pH, is filtered dry standbyly, obtains material 1; The fumaric acid that depolymerization liquid is 0.3:0.01:0.01 by mass ratio, sulphite and cysteine form, and the addition of depolymerization liquid is 1) in 3 times of cereal mixture quality.
4) in material 1, add water adjusting concentration to 10%, then add sodium acid carbonate adjust pH to 7.8, be heated with stirring to 70 ℃, material 1 is pumped in high speed shear tank and carries out high speed shear, and rotating speed is 1430 revs/min, and shear gap is 1 micron, at 70 ℃ of down cuts, stir 20 minutes, obtain material 2;
5) material 2 temperature are increased to 75 ℃, add 12 carbon fatty acids and sodium metaphosphate, the addition of 12 carbon fatty acids accounts for 0.1% of material 2 quality, and the addition of sodium metaphosphate accounts for 0.1% of material 2 quality, stirs insulation 15 minutes, obtains material 3;
6) by material 3 Vacuum Concentrations to protein content 35%~45%, add natrium citricum, addition accounts for 0.05%, 30 ℃ of material 3 quality and stirs 40 minutes, obtains colloidal material 4;
7) add wall material (dextrin: beta-schardinger dextrin-: the mass ratio=1:2:1 of converted starch) adjust protein content to 25% in colloidal material 4, after homogeneous, sterilizing, become plant base emulsion, solid concentration is 30%~40%, 150 ℃ of plant base emulsions are spray dried to powdery, obtain plant base milk powder.
Embodiment 2
1) by the 4:2:4 mixing in mass ratio of wheat embryo, corn, dregs of beans (food processing byproducts), obtain maslin, add water agitation grinding 50 minutes, the amount ratio of maslin and water is 1:8, obtain the juice that contains cereal crude protein, again the juice that contains cereal crude protein is carried out to ultra-fine grinding, make particle diameter > 80 orders of raw material;
2) rare alcohol buffer solution being joined to 1) in juice after pulverizing, 30 ℃ are stirred 70 minutes, and the rare alcohol buffer solution of centrifugal removal obtains dry, adds the deionized water and stirring of 3 times of dry biomass even, obtains slurries; The bamboo charcoal particle that rare alcohol buffer solution is 1:0.5:0.01:0.01 by mass ratio, 95% ethanol, solid sodium hydroxide and solid potassium ferrate form, and the addition of rare alcohol buffer solution is 1) in 3 times of cereal mixture quality.
3) to 2) add depolymerization liquid in the slurries that obtain, 30 ℃ of insulated and stirred 40 minutes, it is 5.6 rear washing 2 times that deionized water regulates pH, is filtered dry standbyly, obtains material 1; The fumaric acid that depolymerization liquid is 5:0.2:0.2 by mass ratio, sulphite and cysteine form, and the addition of depolymerization liquid is 1) in 3 times of cereal mixture quality.
4) in material 1, add water adjusting concentration to 10%, then add sodium acid carbonate adjust pH to 7.8, be heated with stirring to 75 ℃, material 1 is pumped in high speed shear tank and carries out high speed shear, and rotating speed is 1500 revs/min, and shear gap is 5 microns, at 75 ℃ of down cuts, stir 20 minutes, obtain material 2;
5) material 2 temperature are increased to 75 ℃, add 12 carbon fatty acids and sodium metaphosphate, the addition of 12 carbon fatty acids accounts for 0.1% of material 2 quality, and the addition of sodium metaphosphate accounts for 0.12% of material 2 quality, stirs insulation 15 minutes, obtains material 3;
6) by material 3 Vacuum Concentrations to protein content 35%~45%, add natrium citricum, addition accounts for 0.06%, 30 ℃ of material 3 quality and stirs 40 minutes, obtains colloidal material 4;
7) add wall material (dextrin: beta-schardinger dextrin-: the mass ratio=1:2:1 of converted starch) adjust protein content to 28% in colloidal material 4, after homogeneous, sterilizing, become plant base emulsion, solid concentration is 30%~40%, 150 ℃ of plant base emulsions are spray dried to powdery, obtain plant base milk powder.
Implementation column 3
1) Potato protein concentrate mud is added to water agitation grinding 50 minutes, the amount ratio of raw material and water is 1:8, obtains the juice that contains cereal crude protein, then the juice that contains cereal crude protein is carried out to ultra-fine grinding, makes particle diameter > 80 orders of raw material;
2) rare alcohol buffer solution being joined to 1) in juice after pulverizing, 30 ℃ are stirred 60 minutes, and the rare alcohol buffer solution of centrifugal removal obtains dry, adds the deionized water and stirring of 4 times of dry biomass even, obtains slurries; The bamboo charcoal particle that rare alcohol buffer solution is 1:0.5:0.01:0.01 by mass ratio, 95% ethanol, solid sodium hydroxide and solid potassium ferrate form, and the addition of rare alcohol buffer solution is 1) 3 times of Potato protein concentrate shale amount.
3) to 2) add depolymerization liquid in the slurries that obtain, 30 ℃ of insulated and stirred 40 minutes, it is 5.6 rear washing 2 times that deionized water regulates pH, is filtered dry standbyly, obtains material 1; The fumaric acid that depolymerization liquid is 3:0.1:0.1 by mass ratio, sulphite and cysteine form, and the addition of depolymerization liquid is 1) in 3 times of Potato protein concentrate shale amount.
4) in material 1, add water adjusting concentration to 10%, then add sodium acid carbonate adjust pH to 7.8, be heated with stirring to 70 ℃, material 1 is pumped in high speed shear tank and carries out high speed shear, and rotating speed is 1430 revs/min, and shear gap is 1 micron, at 70 ℃ of down cuts, stir 20 minutes, obtain material 2;
5) material 2 temperature are increased to 75 ℃, add 12 carbon fatty acids and sodium metaphosphate, the addition of 12 carbon fatty acids accounts for 0.1% of material 2 quality, and the addition of sodium metaphosphate accounts for 0.06% of material 2 quality, stirs insulation 15 minutes, obtains material 3;
6) by material 3 Vacuum Concentrations to protein content 35%~45%, add natrium citricum, addition accounts for 0.05%, 30 ℃ of material 3 quality and stirs 40 minutes, obtains colloidal material 4;
7) add wall material (dextrin: beta-schardinger dextrin-: the mass ratio=1:2:1 of converted starch) adjust protein content to 18% in colloidal material 4, after homogeneous, sterilizing, become plant base emulsion, solid concentration is 30%~40%, 150 ℃ of plant base emulsions are spray dried to powdery, obtain plant base milk powder.
Nutritional labeling to the plant base milk powder of the embodiment of the present application 1~3 preparation is measured, and result is as following table:
Table 1
Project Embodiment 1 Embodiment 2 Embodiment 3
Protein 25.4% 28.2% 18.6%
Fat 21% 18% 23%
Dietary fiber 3.2% 2.6% 4.1%
Moisture≤ 5% 4.8% 4.7%
The foregoing is only preferred embodiment of the present invention, in order to limit the present invention, within the spirit and principles in the present invention not all, any modification of doing, be equal to replacement, improvement etc., within all should being included in protection scope of the present invention.

Claims (8)

1. a production method for plant base milk powder, is characterized in that, comprising:
1) pre-treatment of plant edible part: take cereal processed side product or whole grain cereal seed is raw material, add water agitation grinding more than 30 minutes, the amount ratio of raw material and water is greater than 1:7, obtain the juice that contains cereal crude protein, again the juice that contains cereal crude protein is carried out to ultra-fine grinding, make particle diameter > 80 orders of raw material;
2) the stench taste of removal plant: rare alcohol buffer solution is joined to 1), in the juice after pulverizing, 30 ℃ are stirred 10~170 minutes, and the rare alcohol buffer solution of centrifugal removal obtains dry, adds the deionized water and stirring of 2~5 times of dry biomass even, obtains slurries;
3) in the slurries that the depolymerization of phytogloibulin subunit: to 2) obtain, add depolymerization liquid, 30~40 ℃ of insulated and stirred 5~40 minutes, deionized water regulates the rear washing in pH to 3~6.6 2~3 times, is filtered dry standbyly, obtains material 1;
4) physical rupture of the long peptide chain of phytogloibulin: add water adjusting concentration to 10% in material 1, then add sodium acid carbonate to regulate pH value to 7.8~8.2, be heated with stirring to 70~75 ℃, material 1 is pumped in high speed shear tank and carries out high speed shear, obtain material 2;
5) combination of small protein molecule and non-polar group: material 2 temperature are increased to 75 ℃, add organic carbonate and catalyst, stir insulation 15 minutes, obtain material 3;
6) protein ionize process: by material 3 Vacuum Concentrations to protein content 35%~45%, add sylvite or sodium salt, the addition of described sylvite or sodium salt accounts for 0.04%~0.08% of material 3 quality, at 30~40 ℃, stirs 10~80 minutes, obtains colloidal material 4;
7) emulsification treatment: by adding wall material to adjust protein content in colloidal material 4, become plant base emulsion after homogeneous, sterilizing, solid concentration is 30%~40%, and plant base emulsion is spray dried to powdery lower than 160 ℃, obtains plant base milk powder.
2. production method according to claim 1, it is characterized in that, 1) in, described cereal processed side product is one or more the mixture in gluten, potato starch parting liquid, wheat embryo, wheat, dregs of beans, rice bran, rice, soybean, maize germ, Potato protein concentrate mud.
3. production method according to claim 1, it is characterized in that, 2) in, described rare alcohol buffer solution is (0.1~5) by mass ratio: (0.1~10): (0.01~0.5): the bamboo charcoal particle of (0.01~0.03), ethanol, NaOH and ferrate form.
4. production method according to claim 1, is characterized in that, 3) in, described depolymerization liquid is (0.1~3) by mass ratio: (0.01~0.5): the fumaric acid of (0.01~0.2), sulphite and cysteine form.
5. production method according to claim 1, is characterized in that, 4) in, the condition of described high speed shear: rotating speed is 1430~1500 revs/min, shear gap is 1~5 micron, at 70~75 ℃ of down cuts, stirs 20 minutes.
6. production method according to claim 1, is characterized in that, 5) in, described organic carbonate is that carbon number is one or more the mixture in 8~26 aliphatic acid, the addition of described organic carbonate accounts for 0.1~0.8% of material 2 quality; Described catalyst is metaphosphoric acid salt, and the addition of described catalyst accounts for 0.05%~0.3% of material 2 quality.
7. production method according to claim 1, is characterized in that, 6) in, described sylvite is potassium citrate or potassium chloride, described sodium salt is sodium acid carbonate or sodium acetate.
8. production method according to claim 1, is characterized in that, 7) in, described wall material is one or more mixture in dextrin, beta-schardinger dextrin-, converted starch.
CN201310638400.0A 2013-12-02 2013-12-02 Production method for plant-based milk powder Expired - Fee Related CN103609714B (en)

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