CN103585029B - Powder baths applies some make up - Google Patents
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- CN103585029B CN103585029B CN201210286973.7A CN201210286973A CN103585029B CN 103585029 B CN103585029 B CN 103585029B CN 201210286973 A CN201210286973 A CN 201210286973A CN 103585029 B CN103585029 B CN 103585029B
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Abstract
Even if the powder baths that the present invention plays with providing the function-stable that a kind of long-term storage also can allow magnesium hydride applies some make up.Become the powder baths containing magnesium hydride and moisture absorption composition to apply some make up.Preferably magnesium hydride is turned to its mean diameter by microgranule is 10～120 μm.Additionally, at least one powder more preferably contained in Pericarpium Citri Reticulatae (Pericarpium Citri junoris), Fructus Capsici, Korean Ginseng, Rhizoma Zingiberis Recens, Radix Angelicae Sinensis and Chinese mugwort.
Description
Technical field
The present invention relates to a kind of powder baths containing magnesium hydride apply some make up.
Background technology
Magnesium hydride is that gap between the metallic atom of magnesium keeps hydrogen and the compound that formed, according to the reaction of following formula (1)
Formula, magnesium hydride and water reaction, thus discharge hydrogen and decompose.
MgH2+2H2O→Mg(OH)2+2H2…(1)
The method manufacturing magnesium hydride has multiple, such as according to the method disclosed in following patent documentation 1 and patent documentation 2,
Magnesium hydride can be manufactured efficiently.
If making magnesium hydride react with water, then during gaseous hydrogen is dissolved in this water, oxidation-reduction potential (ORP) is mobile to reduction
Side, becomes the function water (hydrogeneous water) with oxidation resistance.This water is preventing skin aging, minimizing oxidative stress, is preventing into
People is sick, maintained by defying age the field widely such as healthy has to be applied.
The hydrogeneous water with this function is used as skincare product and has attempted.Such as, following patent document 3 discloses that
A kind of method of the effect that skincare product or domestic water are given suppression or prevention skin aging (aging), the feature of the method
Be, to directly the contact skincare product of skin or domestic water, oxidation-reduction potential ORP=0.80-0.047pH with
Under, give identical with the ORP of skin, or its following reproducibility.Additionally, the following one hydrogen that Patent Document 4 discloses is sent out
Raw agent, this hydrogenite is to embed alkaline earth metal hydride etc. in the water soluble compounds such as Polyethylene Glycol, xylitol, trehalose
The powder of hydride and make, and describe and use it for astringent and bath shampoo.
Patent documentation
Patent documentation 1: No. 4083786 publications of Japanese Patent No.
Patent documentation 2: No. 4425990 publications of Japanese Patent No.
Patent documentation 3: Japanese Unexamined Patent Publication 2000-119161 publication
Patent documentation 4: No. 4384227 publications of Japanese Patent No.
Summary of the invention
Invent problem to be solved
But, because magnesium hydride can react with water, so dampness etc. can make magnesium hydride decompose lentamente, exist and be difficult to make hydrogen
The function-stable ground changing magnesium plays such problem.
Even if it is an object of the invention to provide a kind of long-term preservation also can make the powder that plays of function-stable ground of magnesium hydride
End bath applies some make up.
Solve the means needed for problem
For achieving the above object, present inventor has performed in-depth study, result completes following invention.
That is, the powder baths of the present invention applies some make up and is characterised by containing magnesium hydride and moisture absorption composition.
Powder baths according to the present invention applies some make up, and its moisture absorption composition removes the moisture to contact with magnesium hydride, institute
To be prevented from the situation causing magnesium hydride to decompose lentamente due to factors such as dampnesss, even if preserving for a long time, hydrogenation also can be made
The function-stable ground of magnesium plays.
Preferably: in the powder baths of the present invention applies some make up, above-mentioned magnesium hydride is turned to its mean diameter by microgranule and is
10-120μm。
Accordingly, magnesium hydride is compared with other alkaline earth metal hydrides, and the reaction with water is slow, but, pass through micronized
Making its surface area increase, so promoting reaction even without acid etc., containing with water, hot water or aqueous cosmetics precursor etc.
Water substance also can produce suitable hydrogen when coordinating.It addition, the harsh feeling of magnesium hydride also has improvement when using.
Preferably: the powder baths of the present invention applies some make up and is prepared to water quantities less than 10%.
Hereby it is possible to suppress the intrinsic moisture applied some make up due to powder baths and the situation making magnesium hydride decompose.Such as,
As bath article, sometimes use the inorganic salts such as sulfate, sodium, carbonate, but, according to combination difference, and if existing and have water
Point then can lump, maybe can produce gas etc. and rotten such shortcoming occur as a result, use the present invention can suppress these shortcomings.
Preferably: in the powder baths of the present invention applies some make up possibly together with selected from Pericarpium Citri Reticulatae (Pericarpium Citri junoris), Fructus Capsici, Korean Ginseng,
At least one powder in Rhizoma Zingiberis Recens, Radix Angelicae Sinensis and Chinese mugwort.
Accordingly, can expect that the effect of the blood circulation promoting produced by them is carried with the hydrogeneous water produced by magnesium hydride
The synergism of the effect of the blood circulation promoting come.
The powder baths of the present invention apply some make up in can also containing selected from sodium sulfate, sodium chloride, potassium chloride, magnesium sulfate and
The powder of at least one inorganic salt in Alumen.Further, it is also possible to containing selected from sodium bicarbonate, sodium carbonate and sodium sesquicarbonate
In the powder of at least one carbonate.
Preferably: the powder baths of the present invention apply some make up containing 0.005～5 weight %, selected from silicic acid anhydride, silicic acid
Aluminum, aluminium oxide, potassium oxide, sodium oxide, magnesium oxide, iron sesquioxide, calcium oxide and the rock association thing containing these compositions
In at least one powder.Furthermore it is preferred that the above-mentioned moisture absorption composition containing 1-99 weight %.
Invention effect
Powder baths according to the present invention applies some make up, and its moisture absorption composition removes the moisture to contact with magnesium hydride, because of
This is prevented from the situation making magnesium hydride decompose lentamente due to factors such as dampnesss, even if preserving for a long time, also can make magnesium hydride
Function-stable ground plays.
Detailed description of the invention
It is a kind of cosmetics containing magnesium hydride that the powder baths of the present invention applies some make up, for water, hot water or containing aquation
The hydrous matters such as cosmetic precursor coordinate and produce function water (hydrogeneous water).Magnesium hydride reacts with water according to the reaction equation of following formula (1),
Thus discharge hydrogen while decomposing.
MgH2+2H2O→Mg(OH)2+2H2…(1)
Magnesium hydride used in the present invention, is not particularly limited for its acquisition pattern, such as according to patent the 4083786th
Number publication and No. 4425990 method disclosed in publication of patent can manufacture effectively.
Specifically, as disclosed in No. 4083786 publication of patent, the raw material powder using magnesium as main component
Body is pre-stored in being sealed in the hydrogen atmosphere sealed in container, is maintained at by the pressure of the hydrogen atmosphere in this sealing container
While authorized pressure, by the temperature of the hydrogen atmosphere in this sealing container regulation the 1st during in maintain following temperature
Degree, this temperature is on the profile of equilibrium carrying out chemical combination and generating between the reaction of magnesium hydride and back reaction than elemental magnesium and hydrogen molecule
The temperature corresponding with above-mentioned authorized pressure high and and this temperature between temperature difference temperature within setting, thus, remove
Remove the tunicle of above-mentioned raw materials powder surface, it follows that be not to return to room temperature, but by the hydrogen atmosphere in this sealing container
Temperature during the 2nd of regulation in maintain following temperature and keep, this temperature be than on the above-mentioned profile of equilibrium with above-mentioned
The temperature that authorized pressure is corresponding low and and this temperature between temperature difference temperature within setting, thus, by above-mentioned raw materials
Powder body manufactures magnesium hydride.According to the method, can effectively manufacture the magnesium hydride that hydrogenation ratio is high.Additionally, such as patent
As disclosed in No. 4425990 publications, it is also possible to without powder material, but make multi-disc using magnesium as main component
Thin slice is piled up and through compressor obtained by overcompression so that it is react with hydrogen in hydrogen atmosphere.According to the method, use with magnesium
Thin slice for main component manufactures, and therefore likely causes the method that the powder material of dust explosion carries out manufacturing with use
Compare, the magnesium hydride that hydrogenation ratio is high can be manufactured safer and more effectively.
It should be noted that hydrogenation ratio refers to relative to according to MgH2Molecular weight 26 and Mg molecular weight 24 can be inhaled ideally
The percentage rate of the hydrogen amount stayed, when manufacturing magnesium hydride, measures the quality before and after hydrogen occlusion, and obtains according to following formula (2).
The magnesium hydride obtained according to said method etc., generally its hydrogenation ratio are about 70-100%, more preferably 90-
About 100%, higher than other hydrogen occlusion alloy, the deterioration for chemical is also stable, transporting, supply, the operation of storage etc.
Property aspect, process also be easier, be the most excellent hydrogen occlusion body.But, because having the reactivity with water, so existing
The problem decomposed lentamente due to reasons such as dampnesss during long-term preservation.
Therefore, the powder baths of the present invention applies some make up, containing above-mentioned magnesium hydride, and containing moisture absorption composition.As
Moisture absorption composition, containing having the material of effect absorbing moisture, such as can enumerate containing silicon dioxide, sodium sulfate,
Magnesium sulfate, copper sulfate, calcium chloride, magnesium chloride, aluminium oxide, phosphorus pentoxide, kieselguhr, zeolite etc..Particularly preferably use dioxy
SiClx, sodium sulfate.
Powder baths for the present invention applies some make up, and the preferably mean diameter of magnesium hydride is 10～120 μm, and more preferably 20
～80 μm.If mean diameter is relatively big, surface area reduces, and result exists the trend reduced with the hydrogen generation speed in the reaction of water,
Additionally, there are the trend of the harsh feeling remaining magnesium hydride.If mean diameter is too small, then electrostatic is caused to increase due to micronized
Add and wettability reduce, thus exist when coordinating with the hydrous matter such as water, hot water or aqueous cosmetics precursor, float on the surface and
It is difficult to make the molten tendency depositing hydrogen amount increase.Specifically, in the tank of 40 DEG C of the depth of water about 20 centimetres, with the ratio of 2.5 milligrams
When adding above-mentioned magnesium hydride in every 1 liter of water, the molten hydrogen amount of depositing after 30 minutes is more than 0.01mmol/L, more preferably
More than 0.03mmol/L, and preferably become non-rising particle diameter.It should be noted that as the mean diameter obtaining magnesium hydride
Assay method, the method that particle size values is estimated in the parsing of the diffraction maximum shape by being observed by powder X-ray diffraction device
It is simple, is preferably used.Micronized utilizes well-known method to carry out, and limits its device, method etc. the most especially
System.Such as can be with jet pulverizer or the super micron mill etc. of gases at high pressure.It addition, can be used on as simple and easy method
Mortar carries out pulverizing etc..
Powder baths for the present invention applies some make up, and is preferably prepared to water quantities and is less than 10%, is more preferably prepared as water
Component is less than 7.5%, is most preferably prepared as less than 5%.The mensuration of water quantities, such as, can be carried out in the following manner.That is,
5 grams of the sample accurately weighed up is put into evaporating dish, after being dried 3 hours in the blast type temperature chamber be held in 105 DEG C, again surveys
The quality of this sample fixed, and calculate according to following formula (3).
It should be noted that when coordinating the volatile ingredients such as ethanol in the powder baths of the present invention in applying some make up, based on
The decrement caused because of its volatilization is modified by the value of the use level of this volatile ingredient, is worth as upper obtained by thus
State water quantities.
The powder baths of the present invention applies some make up and preferably comprises the above-mentioned magnesium hydride of 0.005～10 weight %, more preferably contains
0.01～5 weight %.Furthermore it is preferred that the above-mentioned moisture absorption composition containing 1～99 weight %, more preferably contain 1～80 weight %,
Most preferably 10～60 weight %.Additionally, it is preferred that the particle diameter of this moisture absorption composition is the particle diameter same degree with magnesium hydride.
Specifically, preferably mean diameter is 10～120 μm, more preferably 20～80 μm.
Powder baths for the present invention applies some make up, it is intended that give and the hydrogeneous water institute utilizing magnesium hydride to produce
The synergistic action effect of the effect of the blood circulation promoting caused, it is also possible to containing selected from Pericarpium Citri Reticulatae (Pericarpium Citri junoris), Fructus Capsici, Korean Ginseng,
At least one powder in Rhizoma Zingiberis Recens, Radix Angelicae Sinensis and Chinese mugwort.In such a situation it is preferred to use the water quantities material less than 10%
Or thus prepared material, more preferably uses the water quantities material less than 7.5% or thus prepared material,
The most preferably with material less than 5% or thus prepared material.Furthermore it is preferred that be that to pulverize be the powder of below 1000 μm
End.
During the powder baths of the present invention applies some make up, in addition to above-mentioned basis, can suitably coordinate well-known
Additive or other compositions.Such as, the alcohols of ethanol etc., nonionic surfactant, polysaccharide, low molecule saccharide, natural
Oils and fats, emulsifying agent, spice etc..
It addition, the powder baths for the present invention applies some make up, it is necessary to take into account stability, and in view of the water in cosmetics
Component, the most suitably can coordinate on the basis of combinations of the above thing inorganic salts, inorganic acids, organic acid, oils,
The compositions such as binding agent class, polyalcohols, wetting agent, plant powder and crude drug class (extract, powder).
Specifically, the shower cosmetics of the present invention can comprise following component:
1) inorganic salts
Boric acid, Borax, magnesium sulfate, sodium sulfide, Potassium monosulfide., sodium nitrate, calcium nitrate, ammonium sulfate, sodium thiosulfate, phosphoric acid hydrogen
Calcium, potassium chloride, ammonium chloride, sodium phosphate, sodium dithionite, Calcium hyposulfite, sulfur, carbamide, sodium sesquicarbonate and Alumen etc..
2) inorganic acids
Silicic acid and boric acid etc..
3) organic acid
Benzoic acid, citric acid, fumaric acid, tartaric acid, malic acid and salicylic acid etc..
4) oils
Olive oil, soybean oil, almond oil, Oleum Ricini, Oleum Cocois, Petiolus Trachycarpi oil, turtle oil, rice oil, Jojoba oil, ermine oil,
Egg oil, squalane, American Avocado Tree oil, lanoline, liquid paraffin, white vaseline, DHA and EPA etc..
5) binding agent class
Sodium carboxymethyl cellulose, methylcellulose, sodium salt, casein, pectin, starch, sodium alginate, polyvinyl alcohol, poly-
Vinylpyrrolidone, locust bean gum, carrageenin, agar, carbomer and glucose manna carbohydrate gum etc..
6) polyalcohols, wetting agent
Glycerol, propylene glycol, sorbitol, Polyethylene Glycol, 1,3 butylene glycol, vitamin C and derivant thereof, hydrolyzed-silk, collagen,
Chrondroitin and protein complexes, glycyrrhizin and derivant thereof etc..
7) perfumery
Oleum lavandula angustifolia, Flos Jasmini Sambac oil, attar of roses, Fructus Citri Limoniae oil, orange oil, Oleum menthae, thyme oil, oil of Rhizoma Acori Graminei, Oleum Anisi Stellati, day
This Cortex Cryptomeriae Fortunei Radicis oil, Japanese Thuja oil, Cedrus deoclar (Roxb.) G. Don oil, Oleum Rosae Rugosae, eucalyptus oil, Camphora, mentha piperita oil, oleum menthae viridis, citronellol, Fructus Citri tangerinae
Oil, PiceameyeriRehd. Et Wils., citronellol etc. are natural and synthetic perfume etc..
8) plant powder and crude drug class (extract, powder)
Fericarpium Citri Limoniae, Sargassum, spirulina, chlorophyll, Dunaliella salina, Cedrus deoclar (Roxb.) G. Don, Japanese Thuja, Testa oryzae, Rhizoma Acori Graminei, Rhizoma Zingiberis Recens, Radix Glycyrrhizae,
PiceameyeriRehd. Et Wils., Herba Menthae, Cortex cinnamomi japonici (Ramulus Cinnamomi), Fructus Mume, Herba Houttuyniae, Folium Persicae, Flos Matricariae chamomillae, Aloe, jasmine, Rosehips, lavandula angustifolia, Fructus psidii guajavae immaturus, Radix Scutellariae, Chinese holly
The ground product of Qi, Ganoderma, Ramulus Sambuci Williamsii, angelica keiskei koidzumi, Radix Et Caulis Acanthopanacis Senticosi, Fructus Arctii, Radix Glycyrrhizae, Flos Carthami, Herba Erodii, Rhizoma Zingiberis Recens, Fructus Capsici etc. and water thereof
Dissolubility or oil-soluble extracting solution.
And then, the powder baths for the present invention applies some make up, and in addition to those specified above, can also contain in right amount as required
There are antibacterial, surfactant, vitamins, aminoacid and pharmaceuticals, medicine part outer article and tar system color used for cosmetic
Element etc..
The powder baths of the present invention applies some make up and can use with any concentration.Generally, relative in bathtub 150～
220 liters of hot water, the usage amount that bath applies some make up is generally about 25g～30g.It addition, containing Ore in bath applies some make up
In the case of, during balneation, in water, ore concentrations is usually 1ppb～20,000ppm.Therefore, apply some make up can for the powder baths of the present invention
To use as follows, such as, the concentration of the compositions with silicon dioxide as main component is made to reach when balneation
The concentration of 1ppb～20,000ppm (2 weight %).Such as, the bath for the present invention applies some make up, as shown in the Examples, permissible
Used containing the bath of the 250mg compositions 25g that applies some make up by mixing in 180L hot water.
Powder baths for the present invention applies some make up, be preferably prepared to utilize aluminum packaging, polyethylene packaging, paper wrapper or
Sealed inert gas etc. completely cuts off dampness and packaged state is supplied to user.Additionally, it is preferred that be prepared as in use from bag
After dress takes out, coordinate with the aqueous such as water, hot water or aqueous cosmetics precursor and used as cosmetics.Need explanation
, in the present invention, aqueous cosmetics precursor refers to: be prepared as containing for carrying out the water that reacts, and and the present invention with magnesium hydride
Powder baths apply some make up combination, thus the material of the cosmetics needed for being formed.
As the cosmetics that apply some make up of powder baths of the application present invention, whole body, half body, foot, arm can be enumerated and use
Bath apply some make up or bath shampoo etc..Such as, as bath shampoo, it is preferably prepared to the water for bathing relative to 1L and adds magnesium hydride
0.5～125mg, more preferably add magnesium hydride 2.5～50mg, thus use.
[embodiment]
Hereinafter illustrate and the present invention is illustrated, but the scope of the present invention is not limited to these examples.
<manufacturing example 1>
Utilizing the method disclosed in No. 4425990 publications of Japanese Patent No., (hydrogenation ratio is 90-to the magnesium hydride of preparation bulk
95%), with pulverizer, its coarse powder is broken to about 0.1mm, then is ground into micropowder with jet pulverizer.Utilize X-ray powder
The parsing of diffraction instrument, show that the particle diameter of obtained magnesium hydride is 60 μm.
<test example 1>
As described below, to the molten change depositing hydrogen amount used when manufacturing the magnesium hydride obtained in example 1 and add in hot water
It is measured.
That is, at tank (horizontal 60 cm x indulge deep 40 centimetres of 30 cm x) the inner hot water putting into tap water of tropical fish
50L (depth of water 20 centimetres), is maintained at 40 DEG C with heater by water temperature and is set to bath pattern.It is added above-mentioned magnesium hydride
0.125 gram, stir 2 times back and forth with the plastic ruler of 50 centimeter length.Then make water not flow and stand, and measure from putting into magnesium hydride
Molten after starting 0,15,30,60,120,180 minutes deposits hydrogen concentration.When measuring, use and molten deposit hydrogen meter [Micro-sensor
Multi-Meter (H2 sensor)]) (UNISENSE company system), its electrode is inserted in the hot water in tank always, sees
Survey the measured value of each hour.It should be noted that need not take a breath especially in indoor, but come with configured air-conditioning
Carry out the management of temperature humidity.8 tests are carried out altogether at different date and times.
Table 1 illustrates the result of the test of 8 times altogether.
[table 1]
| mmol/L | 0 minute | 15 minutes | 30 minutes | 60 minutes | 120 minutes | 180 minutes |
| Test 1 | 0.00 | 0.02 | 0.03 | 0.04 | 0.04 | 0.05 |
| Test 2 | 0.00 | 0.02 | 0.04 | 0.06 | 0.06 | 0.06 |
| Test 3 | 0.00 | 0.04 | 0.04 | 0.04 | 0.06 | 0.07 |
| Test 4 | 0.00 | 0.03 | 0.04 | 0.04 | 0.06 | 0.06 |
| Test 5 | 0.00 | 0.06 | 0.09 | 0.07 | 0.08 | 0.09 |
| Test 6 | 0.01 | 0.04 | 0.05 | 0.06 | 0.07 | 0.08 |
| Test 7 | 0.01 | 0.05 | 0.06 | 0.06 | 0.09 | 0.09 |
| Test 8 | 0.01 | 0.03 | 0.04 | 0.05 | 0.07 | 0.10 |
| Averagely | 0.004 | 0.036 | 0.049 | 0.053 | 0.066 | 0.075 |
Its result, starts molten hydrogen amount of depositing between 0-15 minute from input magnesium hydride and increases to average about 0.036mmol/L,
Elapsing then as the time, molten hydrogen amount of depositing increases lentamente.
<embodiment 1>(bath shampoo)
The formula using magnesium hydride the according to the form below 2 obtained in manufacturing example 1 manufactures bath shampoo, carries out according to a conventional method
Aluminum is packed.
[table 2]
| Components Name | Use level (quality %) |
| Magnesium hydride | 2.0 |
| Sodium sulfate | To 100 |
| Sodium chloride | 20.0 |
| Sodium bicarbonate | 20.0 |
| Calcium carbonate | 2.0 |
| Maltose alcohol | 2.0 |
| Pericarpium Citri junoris extract | 0.1 |
| Hydrolytic collagen | 0.1 |
| Glycine | 0.5 |
| Silicon dioxide | 0.1 |
| 2-Sulfosuccinic acid ethylhexyl sodium | 0.1 |
| Polysorbate80 | 0.05 |
| Glycerol | 0.05 |
| Ethanol | 1.0 |
| Spice | 1.0 |
From aluminum is packed, take out this bath shampoo 25 grams, put in the hot water of 200L and use, to skin when result is had a bath
Sense of touch is fine, does not the most stimulate, and after having a bath, skin radiance and moist feeling (moisture retention), have the effect of good beauty treatment skin
Really.It addition, heat insulation effect (warming) is the most fine.
<test example 2>
The formula using magnesium hydride according to the form below 3 epimere obtained in manufacturing example 1 manufactures powder baths and applies some make up, and presses
Conventional method has carried out aluminum packaging.
[table 3]
The powder baths obtained is applied some make up and has carried out storage stability test.Specifically, after to preserving 4 days at 60 DEG C
In aluminum packaging the dilatancy of air whether good, preserve 6 months at 40 DEG C after powder flowbility is the best, preserve 6 at 40 DEG C
After individual month, powder is formed with or without lump, by ◎: the best, and zero: good, △: slightly worse, ×: these 4 grades of difference are evaluated.
Its result, as shown in table 3 hypomere, is being coordinated the embodiment 2 of sodium sulfate and is joining by 50 weight % by 98 weight %
Having closed in the embodiment 3～6 of sodium sulfate, all of evaluation result all obtains extraordinary bin stability.It addition, with by 98 matter
Amount % has coordinated the comparative example 1 of sodium bicarbonate to compare, and 50 mass % of this sodium bicarbonate are replaced as sodium sulfate 50 weight %
The bin stability of embodiment 7 is more preferable.It addition, compared with the comparative example 2 having coordinated sodium carbonate by 98 mass %, by this sodium carbonate
The bin stability of the 50 mass % embodiment 8 that is replaced as sodium sulfate 50 weight % more preferable.It addition, coordinate with by 98 mass %
The comparative example 3 of calcium carbonate is compared, and 50 mass % of this calcium carbonate are replaced as the storage of the embodiment 9 of sodium sulfate 50 weight %
Stability is more preferable.It addition, compared with the comparative example 4 having coordinated sodium sesquicarbonate by 98 mass %, by the 50 of this sodium sesquicarbonate
The bin stability of the embodiment 10 that quality % is replaced as sodium sulfate 50 weight % is more preferable.
It may thus be appreciated that: utilize sodium sulfate can improve the bin stability that the powder baths containing magnesium hydride applies some make up.
<test example 3>
The epimere formula using magnesium hydride the according to the form below 4 obtained in manufacturing example 1 manufactures powder baths and applies some make up, by often
Rule method aluminum is packed.
[table 4]
The moisture content amount (dried decrement) applied some make up obtained powder baths according to a conventional method is determined.Tool
For body, after being dried 3 hours in the blast type temperature chamber be maintained at 105 DEG C, calculate according to following formula (3).
Additionally, carried out the storage stability test as above-mentioned test example 2.Specifically, preserve 4 days at 60 DEG C
Air expansion in rear aluminum packaging whether good, preserve 6 months at 40 DEG C after the mobility of powder the best, by ◎: non-
Chang Hao, zero: good, △: slightly worse, ×: these 4 grades of difference are evaluated.
Result is as shown in table 4 hypomere, and in embodiment 11, moisture content amount is 3.5%, and bin stability is the best.Additionally, with reality
The formula executing example 11 is close, and water quantities is that the bin stability of the embodiment 12 of 10% is the best.In contrast to this, with embodiment
11, the formula of 12 close to but moisture content amount be 11.2% comparative example 5,6 in, find aluminum packaging in air expansion and also powder
Mobility also degenerate.On the other hand, in the embodiment 13～16 of the fit system according to other, moisture content amount is modulated to
2.8～about 4.8%, bin stability is the best or good.
It may thus be appreciated that: by moisture content amount is modulated to below setting, it is possible to improve the powder baths containing magnesium hydride
The bin stability of cosmetic.
Claims (6)
1. a powder baths applies some make up, it is characterised in that containing magnesium hydride and moisture absorption composition, and according to making water quantities not surpass
The mode of 10% crossed is prepared,
Described magnesium hydride is to be micronized into the magnesium hydride that its mean diameter is 10～120 μm,
Described moisture absorption composition be selected from silicon dioxide, sodium sulfate, magnesium sulfate, copper sulfate, calcium chloride, magnesium chloride, aluminium oxide, five
Aoxidize in two phosphorus, kieselguhr, zeolite is one kind or two or more.
Powder baths the most according to claim 1 applies some make up, its possibly together with in sodium chloride, potassium chloride and Alumen extremely
The powder of few a kind of inorganic salt.
Powder baths the most according to claim 1 and 2 applies some make up, and it is possibly together with selected from sodium bicarbonate, sodium carbonate and sesquialter
The powder of at least one carbonate in sodium carbonate.
Powder baths the most according to claim 1 and 2 applies some make up, its possibly together with selected from Pericarpium Citri Reticulatae, Fructus Capsici, Korean Ginseng, Rhizoma Zingiberis Recens,
At least one powder in Radix Angelicae Sinensis and Chinese mugwort.
Powder baths the most according to claim 1 and 2 applies some make up, its contain 0.005～5 weight % selected from silicic acid anhydride,
Aluminium silicate, aluminium oxide, potassium oxide, sodium oxide, magnesium oxide, iron sesquioxide, calcium oxide and the rock group containing these compositions
At least one powder in compound.
Powder baths the most according to claim 1 and 2 applies some make up, and it contains the described moisture absorption composition of 1-99 weight %.
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| CN109223938A (en) * | 2018-11-15 | 2019-01-18 | 河南忠澜艾健康科技有限公司 | A kind of motherwort wormwood bathing health packet and preparation method thereof |
| CN112456438A (en) * | 2020-11-30 | 2021-03-09 | 杭州粟源科技有限公司 | Mixture capable of generating hydrogen for human body and carrier thereof |
| CN115414266A (en) * | 2021-05-16 | 2022-12-02 | 石家庄天旭环保科技有限公司 | Diatom ooze bath powder |
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| CN101304943A (en) * | 2005-11-10 | 2008-11-12 | 株式会社黑罗麦托 | Hydrogen generating agent and use thereof |
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| JP3481260B2 (en) * | 1991-07-04 | 2003-12-22 | 株式会社ツムラ | Bath agent |
| JP2009046370A (en) * | 2007-08-22 | 2009-03-05 | Aquafairy Kk | Hydrogen generating device and hydrogen generating method |
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