CN103553485A - Preparation method of healthful environment-friendly diatomite wall material powder with temperature adjustment function - Google Patents
Preparation method of healthful environment-friendly diatomite wall material powder with temperature adjustment function Download PDFInfo
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- CN103553485A CN103553485A CN201310474410.5A CN201310474410A CN103553485A CN 103553485 A CN103553485 A CN 103553485A CN 201310474410 A CN201310474410 A CN 201310474410A CN 103553485 A CN103553485 A CN 103553485A
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- powder
- temperature adjustment
- wall material
- friendly
- adjustment function
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- 239000000843 powder Substances 0.000 title claims abstract description 56
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title claims abstract description 46
- 239000000463 material Substances 0.000 title claims abstract description 38
- 238000002360 preparation method Methods 0.000 title abstract description 4
- 239000002131 composite material Substances 0.000 claims abstract description 17
- 230000008859 change Effects 0.000 claims abstract description 13
- 235000012211 aluminium silicate Nutrition 0.000 claims abstract description 12
- 239000012074 organic phase Substances 0.000 claims abstract description 11
- 239000005995 Aluminium silicate Substances 0.000 claims abstract description 10
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000010459 dolomite Substances 0.000 claims abstract description 9
- 229910000514 dolomite Inorganic materials 0.000 claims abstract description 9
- 238000004146 energy storage Methods 0.000 claims abstract description 9
- 239000010456 wollastonite Substances 0.000 claims abstract description 8
- 229910052882 wollastonite Inorganic materials 0.000 claims abstract description 8
- 239000004568 cement Substances 0.000 claims abstract description 7
- 239000004816 latex Substances 0.000 claims abstract description 7
- 229920000126 latex Polymers 0.000 claims abstract description 7
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 6
- 230000036541 health Effects 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 14
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 12
- 239000011159 matrix material Substances 0.000 claims description 10
- 229910010413 TiO 2 Inorganic materials 0.000 claims description 9
- 150000001875 compounds Chemical class 0.000 claims description 9
- 239000001913 cellulose Substances 0.000 claims description 6
- 229920002678 cellulose Polymers 0.000 claims description 6
- 239000000377 silicon dioxide Substances 0.000 claims description 6
- 239000012071 phase Substances 0.000 claims description 4
- 238000001354 calcination Methods 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 239000011941 photocatalyst Substances 0.000 claims description 3
- 230000008569 process Effects 0.000 claims description 3
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 2
- PZZYQPZGQPZBDN-UHFFFAOYSA-N aluminium silicate Chemical compound O=[Al]O[Si](=O)O[Al]=O PZZYQPZGQPZBDN-UHFFFAOYSA-N 0.000 claims description 2
- 229910000323 aluminium silicate Inorganic materials 0.000 claims description 2
- 230000004048 modification Effects 0.000 claims description 2
- 238000012986 modification Methods 0.000 claims description 2
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims description 2
- 230000009466 transformation Effects 0.000 claims description 2
- 239000002557 mineral fiber Substances 0.000 abstract description 3
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 229920003086 cellulose ether Polymers 0.000 abstract 1
- 239000002245 particle Substances 0.000 abstract 1
- 239000010453 quartz Substances 0.000 abstract 1
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 6
- 238000013016 damping Methods 0.000 description 5
- 238000010521 absorption reaction Methods 0.000 description 3
- 239000011148 porous material Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 2
- 229930040373 Paraformaldehyde Natural products 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- 229920002866 paraformaldehyde Polymers 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 239000000809 air pollutant Substances 0.000 description 1
- 231100001243 air pollutant Toxicity 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
- 230000015271 coagulation Effects 0.000 description 1
- 238000005345 coagulation Methods 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 239000002075 main ingredient Substances 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 239000002957 persistent organic pollutant Substances 0.000 description 1
- 230000001699 photocatalysis Effects 0.000 description 1
- 238000007146 photocatalysis Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
Abstract
The invention relates to a preparation method of a healthful environment-friendly diatomite wall material powder with temperature adjustment function. The wall material powder comprises the following components by weight: 35%-50% of a diatomite / organic phase change energy storage composite material, 15%-25% of an opoka powder of 200-800 mesh, 10%-20% of calcined kaolin of 600-1250 mesh, 5% of calcined dolomite powder of 200-400 mesh, 5% of white cement, 10% of quartz powder of 40-200 mesh, 0.5%-1.5% of a diatomite filter aid supported nanometer TiO2 composite material, 2%-4% of wollastonite mineral fiber with draw ratio no less than 15 and average particle size less than 15 mum, 0.5%-1.0% of a superfine latex powder and 0.3% of cellulose ether. The healthful environment-friendly diatomite wall material powder with temperature adjustment function has the functions of humidity adjustment, environmental protection and temperature adjustment.
Description
Technical field
The present invention relates to indoor decorating coating or coated material technical field, specifically, is a kind of compound method with the health environment-friendly kieselguhr wall material powder of temperature adjustment function.
Background technology
Kieselguhr wall material has been widely used in indoor wall finishing or has decorated because of its health environment-friendly characteristic and good visual effect.But existing kieselguhr wall material only has damping, adsorbs and remove the function of the gaseous organic pollutants such as indoor formaldehyde, toluene, do not regulate the function of room temp.Suitable room temp is to guarantee one of human comfort degree and healthy important factor, and the main method of guaranteeing at present indoor comfort temperature is that summer air conditioner refrigerating, heating in winter heats up, and need to consume a large amount of energy.
Summary of the invention
The object of this invention is to provide a kind of compound method with the health environment-friendly kieselguhr wall material of temperature adjustment function.
The present invention's the health environment-friendly kieselguhr wall material powder with temperature adjustment function is realized by following technique means.
A health environment-friendly kieselguhr wall material powder for temperature adjustment function, is formed by following component proportion according to weight percentage: diatomite/organic phase change energy storage composite material 35%～50%, 200～800 order opoka powder 15%～25%, 600～1250 order calcined kaolins 10%～20%, 200～400 order calcined dolomite powder 5%, white cement 5%, 40～200 order silica powders 10%, super-cell loaded with nano TiO
2matrix material 0.5%～1.5%, length-to-diameter ratio>=15 and median size are less than wollastonite mine fibres 2%～4%, superfine latex powder 0.5%～1.0%, the ether of cellulose 0.3% of 15 μ m; Above-mentioned each composition weight sum is 100%.
Described diatomite/organic phase change energy storage composite material be a kind of with modification infusorial earth, be the composite powder material that carrier, load organic phases become material, 20～28 ℃ of its transformation temperatures, latent heat of phase change >=75J/g.The preparation method of this phase change composite material is open by invention patent mandate notification number CN 102199416 B.
Described opoka powder is that a kind of main component is unformed SiO
2, the siliceous mineral powder of natural porous that porosity is larger, its pore size distribution range is several nanometers to tens nanometer at zero point (mean pore size is 3～5nm approximately), has the large (60～100m of specific surface area
2more than/g, be diatomaceous 3 times of left and right), the characteristics such as absorption property is strong, stable chemical nature, not only have good moisture absorption and moisture releasing (being damping) function, and PARA FORMALDEHYDE PRILLS(91,95) gas have good absorption capturing ability.Nen River Region, opoka Kuang China northeast reserves are abundant, easily exploit and process, and have the advantages such as cost is lower.
Described calcined kaolin is the inorganic non-metallic powder body material of natural kaolin ore deposit after fine grinding and 1000 ℃ of following calcination process, and main component is pure aluminium silicate.Kaolin has removed wherein water of constitution and the organic matter of 15% contained left and right after calcining, has left a large amount of holes, and specific surface area reaches 5m
2more than/g, there is good damping and adsorption function, and whiteness is up to more than 90%, good weatherability.
Described light dolomite powder is a kind of dolomite mineral product of fine grinding after raw material is calcined under 900 ℃ of left and right of take, and main component is MgO and CaO, belongs to inorganic coagulation material, slowly carbonatization under the effect of moisture in air.
Described super-cell loaded with nano TiO
2matrix material is a kind of take the loaded nano TiO that super-cell is carrier
2composite photocatalyst material, its preparation method is open by invention patent mandate notification number CN102039118 B.Super-cell loaded with nano TiO
2photocatalyst material all has good photocatalysis performance under UV-light and visible ray, under fluorescent lamp, and degraded clearance>=80% of PARA FORMALDEHYDE PRILLS(91,95) in 48 hours.
Described wollastonite mine fibres is that main chemical compositions is the natural mineral fiber of Calucium Silicate powder, and this natural mineral fiber can not only increase the intensity of wall material, and can also produce good vision (tiffany) effect.
The above-mentioned compound method with the health environment-friendly kieselguhr wall material powder of temperature adjustment function, comprises the steps: to take raw material with meter electronics, joins in stirring mixer and stirs in proportion, obtains kieselguhr wall material powder of the present invention.
The paste slurry obtaining after the kieselguhr wall material powder obtaining after above-mentioned each component is stirred and clear water are uniformly mixed according to the weight ratio of 1:0.9～1.5 is the health environment-friendly kieselguhr wall material with temperature adjustment function.This wall material is used for decorating indoor wall, can adopt the form construction of plastering, and the diatom ooze wall material use quantity of every square metre of wall is 1.5～2.5kg, scrapes and smears the decorated wall surface that can form thickness 2～4mm after 2～4 times on wall.
Temperature adjustment function health environment-friendly kieselguhr wall material powder of the present invention be take and had the diatomite phase change composite material of accumulation of energy function and specific surface area is large and pore structure distributes suitable opoka as main ingredient, and by interpolation super-cell loaded with nano TiO
2matrix material, makes it not only have damping and the function of the air pollutant such as indoor formaldehyde, toluene is removed in degraded, and has the function that regulates room temp.This wall material powder is used for fitting up indoor wall, can saves office winter and live chamber heating energy consumption; Can save the power consumption of air conditioner refrigerating summer, is a kind of multi-functional interior walls material or coating that collects damping, environmental protection and temperature adjustment function.
Embodiment
Be below embodiments of the invention.The product that Linjiang City, super-cell loaded with nano TiO2 composite material by adopting Jilin Province health care nanometer matrix material Science and Technology Ltd. wherein produces.
Embodiment 1:
Diatomite/organic phase change energy storage composite material 36kg
325 order opoka powder 24kg
1250 order calcined kaolin 15kg
240 order calcined dolomite powder 5kg
40～200 order silica powder 10kg
White cement 5kg
Super-cell loaded with nano TiO
2matrix material 0.5kg
Length-to-diameter ratio >=15 and median size are less than the wollastonite mine fibres 3.5kg of 15 μ m
Superfine latex powder 0.7kg
Ether of cellulose 0.3kg.
Embodiment 2:
Diatomite/organic phase change energy storage composite material 40kg
500 order opoka powder 20kg
800 order calcined kaolin 15kg
325 order calcined dolomite powder 5kg
40～200 order silica powder 10kg
White cement 5kg
Super-cell loaded with nano TiO
2matrix material 0.7kg
Length-to-diameter ratio >=15 and median size are less than the wollastonite mine fibres 3.2kg of 15 μ m
Superfine latex powder 0.8kg
Ether of cellulose 0.3kg.
Embodiment 3:
Diatomite/organic phase change energy storage composite material 43kg
600 order opoka powder 15kg
1000 order calcined kaolin 17kg
200 order calcined dolomite powder 5kg
40～200 order silica powder 10kg
White cement 5kg
Super-cell loaded with nano TiO
2matrix material 1.0kg
Length-to-diameter ratio >=15 and median size are less than the wollastonite mine fibres 2.8kg of 15 μ m
Superfine latex powder 0.9kg
Ether of cellulose 0.3kg.
Embodiment 4:
Diatomite/organic phase change energy storage composite material 47kg
800 order opoka powder 15kg
600 order calcined kaolin 13kg
280 order calcined dolomite powder 5kg
40～200 order silica powder 10kg
White cement 5kg
Super-cell loaded with nano TiO
2matrix material 1.2kg
Length-to-diameter ratio >=15 and median size are less than the wollastonite mine fibres 2.9kg of 15 μ m
Superfine latex powder 0.6kg
Ether of cellulose 0.3kg.
Constituent materials in above-mentioned four embodiment is added and stirred in dry powder stirring mixer, after the assay was approved, adopt weather-proof dressing, packed can dispatching from the factory.
Claims (5)
1. a compound method with the health environment-friendly kieselguhr wall material powder of temperature adjustment function, it is characterized in that, formulated by following component according to weight percentage: diatomite/organic phase change energy storage composite material 35%～50%, 200～800 order opoka powder 15%～25%, 600～1250 order calcined kaolins 10%～20%, 200～400 order calcined dolomite powder 5%, white cement 5%, 40～200 order silica powders 10%, super-cell loaded with nano TiO
2matrix material 0.5%～1.5%, length-to-diameter ratio>=15 and median size are less than wollastonite mine fibres 2%～4%, superfine latex powder 0.5%～1.0%, the ether of cellulose 0.3% of 15 μ m, and above-mentioned each composition weight sum is 100%.
2. the compound method with the health environment-friendly kieselguhr wall material powder of temperature adjustment function according to claim 1, it is characterized in that described diatomite/organic phase change energy storage composite material be a kind of with modification infusorial earth, be the composite powder material that carrier, load organic phases become material, 20～28 ℃ of its transformation temperatures, latent heat of phase change >=75J/g.
3. the compound method with the health environment-friendly kieselguhr wall material powder of temperature adjustment function according to claim 1, is characterized in that described opoka powder is that a kind of main component is unformed SiO
2, natural porous silicoide that porosity is larger.
4. the compound method with the health environment-friendly kieselguhr wall material powder of temperature adjustment function according to claim 1, it is characterized in that described calcined kaolin is the inorganic non-metallic powder body material of natural kaolin ore deposit after fine grinding and 1000 ℃ of following calcination process, main component is pure aluminium silicate.
5. the compound method with the health environment-friendly kieselguhr wall material powder of temperature adjustment function according to claim 1, is characterized in that described super-cell loaded with nano TiO2 matrix material is a kind of and take the loaded nano TiO that super-cell is carrier
2composite photocatalyst material.
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| CN201310474410.5A CN103553485B (en) | 2013-10-12 | 2013-10-12 | Preparation method of healthful environment-friendly diatomite wall material powder with temperature adjustment function |
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| CN103553485B CN103553485B (en) | 2014-12-17 |
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Cited By (5)
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| CN104449591A (en) * | 2014-12-10 | 2015-03-25 | 西安建筑科技大学 | Nanoscale dibasic fatty acid/SiO2 composite phase change material having temperature-regulating and humidity-regulating properties and preparation method thereof |
| CN105289570A (en) * | 2015-10-21 | 2016-02-03 | 安徽工业大学 | Temperature and humidity regulating composite material having photocatalytic performance and preparation method thereof |
| CN108975789A (en) * | 2018-08-31 | 2018-12-11 | 东莞市爱乐居环保科技有限公司 | A kind of environmental and ecological diatom ooze coating and preparation method thereof |
| CN110372412A (en) * | 2019-08-28 | 2019-10-25 | 邱连旺 | A kind of diatomite functional material and preparation method thereof |
| CN112573891A (en) * | 2020-12-10 | 2021-03-30 | 山东省泥博士新型材料有限公司 | Far infrared health maintenance diatom ooze board and preparation method thereof |
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| CN112573891A (en) * | 2020-12-10 | 2021-03-30 | 山东省泥博士新型材料有限公司 | Far infrared health maintenance diatom ooze board and preparation method thereof |
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| CN103553485B (en) | 2014-12-17 |
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Application publication date: 20140205 Assignee: Changchun Bang Bang diatom New Material Co., Ltd. Assignor: China University of Mining & Technology, Beijing Contract record no.: 2016990000058 Denomination of invention: Preparation method of healthful environment-friendly diatomite wall material powder with temperature adjustment function Granted publication date: 20141217 License type: Exclusive License Record date: 20160302 |
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