CN103528995B - A kind of turbidimetry optical match device, transmissometer, sample bottle localization method, the optical match method of sample bottle identification method and multiple sample bottles - Google Patents
A kind of turbidimetry optical match device, transmissometer, sample bottle localization method, the optical match method of sample bottle identification method and multiple sample bottles Download PDFInfo
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- CN103528995B CN103528995B CN201310470638.7A CN201310470638A CN103528995B CN 103528995 B CN103528995 B CN 103528995B CN 201310470638 A CN201310470638 A CN 201310470638A CN 103528995 B CN103528995 B CN 103528995B
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Abstract
The invention discloses a kind of turbidimetry optical match device, optical match device includes transmissometer sample bottle positioning bottle-cover and the measuring flume being arranged on measuring flume positioning mark block, bottle cap includes lid and the shade stretched out at the top of lid, the top end face of shade is octagon, and it is provided with corresponding orientation number on every side, it is rotatable on end face at the top of lid to be provided with instruction disk, indicate to set azimuth mark on disk;Lid is eight prisms, and the octagon side of lid is the locating surface with measuring flume insert port corresponding matching;Lid bottom end face is provided with the placement positioning port detachably connected with sample bottle bottleneck.The present invention is positioned using sample bottle positioning bottle-cover to sample bottle, it enables sample bottle hanging in measuring flume, sample bottle body is which obviated to contact with the direct of positioner, the accuracy for scratching and staiing, ensure that positioning is reduced, movable instruction disk facilitates the optics pairing of sample bottle.
Description
Technical field
The present invention relates to a kind of optical match device and its optical match method, more particularly to a kind of turbidimetry optics
Optical match method with device, transmissometer, sample bottle localization method, sample bottle identification method and multiple sample bottles.
Background technology
Turbidity is the muddy degree of water, and it is that insoluble substance in water causes what the transparency of water reduced to measure.It is anti-
An index of the physical behavior of natural water and drinking water is reflected, the limpid or muddy degree to represent water is that measurement water quality is good
One of important indicator of good degree.
Current transmissometer mainly uses 7,027 two kinds of detection methods of USEPA methods 180.1 and ISO method;General principle is
On the suspended particulate that a branch of incident ray sent by light source assembly is irradiated in water, particle sends scattered light to surrounding, detection
Device is detected and the scattered light of incident light at an angle of 90.
In Optical System Design, first require by non-water sample scattering approach (such as reflection of condenser and water sample tube wall,
Scattering etc.) reach receive device veiling glare it is as few as possible, be so conducive to reduce device zero point;During measurement, not only to consider
The correctness of cleaning and the sampling of sample bottle, while should ensure that the uniformity of measurement position.
During the turbidimetry of water, the positioning of sample bottle 10 is that influence measures reappearance and the key factor of the degree of accuracy,
The method that current transmissometer is used is that sample bottle 10 is placed in measuring flume 20, makes sample with two steel balls headed on by spring 21 22
Product bottle is adjacent to reach positioning with measurement cell wall, and Fig. 1 is existing transmissometer sample bottle mounting means.
Because the scattered light intensity of turbidimetry is very faint, the cut of sample bottle surface and contamination can influence the standard of measurement
Exactness, and this localization method is easy to scratch and contaminated samples bottle;It is that glassware appearance and size is deposited additionally, due to sample bottle
In larger error, there is larger space between measuring flume, the easy run-off the straight when one side stress influences sample bottle positioning accurate
Degree.
Due to glass sample bottle material and the unevenness made influence, the direction that sample bottle is placed in measuring flume is different
When measured value differ greatly(Fig. 2);In accurate measurement, it is necessary to which one or more sample bottles are carried out with optics pairing, current
Sample bottle pairing is that sample bottle is once rotated about 45 degree by every measurement, is carried out after 8 measurements in the one side note that measured value is minimum
Number pen makees a mark as mark, and such method needs the measurement for repeating 8 times comparatively laborious, in addition, the party
Need to rotate 45 degree of sample bottle when method is measured every time, it cannot be guaranteed that each rotation is all 45 degree in actual operating process,
The error of rotational angle is very big, so as to cause final measuring result error big, unreliable.
The content of the invention
Sample bottle can be accurately positioned the technical problem to be solved in the present invention is to provide one kind, and standard can be reached
True measurement turbidity and a kind of turbidimetry optical match device of purpose of accurate optical match, transmissometer, sample bottle positioning side
The optical match method of method, sample bottle identification method and multiple sample bottles.
To reach above-mentioned purpose, technical scheme is as follows:
A kind of turbidimetry optical match device, the measuring flume and sample bottle of the optical match device and transmissometer match
Close, it is characterised in that the optical match device includes transmissometer sample bottle positioning bottle-cover and the measurement being arranged on measuring flume
Groove positioning mark block, the bottle cap includes lid and the shade stretched out at the top of lid, and the top end face of the shade is
It is provided with octagon, and every side at the top of corresponding orientation number, lid and is rotatably provided with instruction disk, the finger on end face
Show the azimuth mark set on disk with the measuring flume positioning mark block corresponding matching on the orientation number and measuring flume on end face;It is described
Lid generally eight prisms, octagon side and the measuring flume insert port corresponding matching of eight prisms, form and bottle cap are rotated
The locating surface that orientation is positioned, and distribution corresponding with octagonal lid top end face;Set on the lid bottom end face
There is the placement positioning port detachably connected with sample bottle bottleneck;Shade and the end face of measuring flume insert port at the top of the lid are matched somebody with somebody
Close.
In one embodiment of the invention, the placement positioning port is the screw thread mouth being spirally connected with sample bottle bottleneck.
In one embodiment of the invention, the lid of eight prism has 1 degree of taper.
In one embodiment of the invention, the instruction disk is arranged on end face at the top of lid by elastic rotation mechanism
On, and 45 degree are rotated every time.
A kind of transmissometer, it includes measuring flume and sample bottle, and the transmissometer also includes turbid described in Claims 1-4
Transmissometer sample bottle positioning bottle-cover in degree measurement optical match device, the optical match device is determined by placement thereon
Position mouth connects with sample bottle, then is coordinated by its octagon locating surface and measuring flume insert port, assigns into measuring flume and inserts into the mouth,
So that sample bottle is vacantly placed in measuring flume, it is not directly contacted with measuring flume.
In one embodiment of the invention, the bottom of the measuring flume is correspondingly arranged on spacing with sample bottle cooperation
Groove.
A kind of localization method of transmissometer sample bottle, the localization method comprises the following steps:
(1)The bottleneck of sample bottle is placed in the placement positioning port on transmissometer sample bottle positioning bottle-cover, sample is realized
Bottle is fixedly connected with transmissometer sample bottle positioning bottle-cover;
(2)The positioning bottle-cover that placement is connected with sample bottle is coordinated by its octagon locating surface and measuring flume insert port, is made
The orientation number obtained on positioning bottle-cover is corresponding with the measuring flume positioning mark block on measuring flume, is thus positioned;
(3)The positioning bottle-cover for being connected with sample bottle will be disposed to assign into measuring flume to insert into the mouth so that on positioning bottle-cover connect
The sample bottle connect is vacantly placed in measuring flume, is not directly contacted with measuring flume.
A kind of sample bottle identification method, the identification method comprises the following steps:
(1)In the sample bottle that high purity water is added to cleaning, and sample bottle positioning bottle-cover is fixedly connected with sample bottle;
(2)By sample bottle wiped clean, and last layer silicone oil is applied on sample bottle, then by the side on sample bottle positioning bottle-cover
Position number alignment measuring flume positioning mark block, inserts sample bottle in measuring flume after alignment;
(3)Apparatus measures key, record number and reading value are pressed, so measures successively totally 8 times, 8 data is compared
Azimuth mark is turned into the minimum orientation number of reading value more afterwards;
(4)From now on when using the sample bottle, as long as azimuth mark can be obtained by with measuring flume positioning mark block alignment
Accurate reading.
A kind of optical match method of multiple sample bottles, the optical match method comprises the following steps:
(1)The step being first according in claim 8 is identified measurement to first sample bottle, records reading value, and
Azimuth mark is turned into the minimum orientation number of reading value:
(2)Step in by second sample bottle according to claim 8 is identified measurement, and records reading value, directly
To when obtaining reading and first sample bottle least count difference less than ± 0.1NTU, azimuth mark block is turned into the reading corresponding
Orientation number, such second sample bottle and first sample bottle optical match are completed;
(3)Repeat step(2)Optical match is carried out to other sample bottles.
By above-mentioned technical proposal, the beneficial effects of the invention are as follows:
The present invention is positioned to sample bottle using sample bottle positioning bottle-cover, and it is directly contacted with bottleneck, without with
Body is contacted, and is which obviated the scuffing and contamination on sample bottle body surface, is improved the degree of accuracy of measurement;Use Mold Making
Sample bottle positioning bottle-cover there is the very high degree of accuracy, it is ensured that the accuracy of positioning, movable instruction disk facilitates sample bottle
Optics pairing and it is actually used.
Brief description of the drawings
In order to illustrate more clearly about the embodiment of the present invention or technical scheme of the prior art, below will be to embodiment or existing
There is the accompanying drawing used required in technology description to be briefly described, it should be apparent that, drawings in the following description are only this
Some embodiments of invention, for those of ordinary skill in the art, on the premise of not paying creative work, can be with
Other accompanying drawings are obtained according to these accompanying drawings.
Fig. 1 is the scheme of installation of existing sample bottle and measuring flume;
10th, sample bottle 20, measuring flume 21, spring 22, steel ball
Fig. 2 is the top view of inventive samples bottle positioning bottle-cover;
Fig. 3 is the sectional view of inventive samples bottle positioning bottle-cover;
Fig. 4 is the upward view of inventive samples bottle positioning bottle-cover;
Fig. 5 is mounting structure schematic diagram of the present invention;
Fig. 6 is Fig. 5 top view.
Numeral and the corresponding component title represented by letter in figure:
100th, measuring flume 110, measuring flume insert port 120, measuring flume positioning mark block 130, stopper slot 200, sample
Product bottle 210, bottleneck 300, transmissometer sample bottle positioning bottle-cover 310, lid 311, instruction disk 311a, azimuth mark
312nd, locating surface 313, placement positioning port 320, shade.
Embodiment
In order that the technical means, the inventive features, the objects and the advantages of the present invention are easy to understand, tie below
Conjunction is specifically illustrating, and the present invention is expanded on further.
Referring to shown in Fig. 2 to Fig. 6, the invention discloses a kind of turbidimetry optical match device, optical match device with
The measuring flume 100 and sample bottle 200 of transmissometer are engaged, and optical match device includes the He of transmissometer sample bottle positioning bottle-cover 300
It is arranged on the measuring flume positioning mark block 120 on measuring flume;Transmissometer sample bottle positioning bottle-cover 300 includes lid 310 and by covering
The shade 320 stretched out at the top of body, the top end face of shade 320 is to be provided with corresponding orientation number on octagon, and every side
Code, orientation number can be made up of 1 to 8 eight numerals, can also be made up of 8 different letters, and the present invention is by by 1 to 8 eight
Individual numeral composition, this eight numerals are arranged in order clockwise.
It is rotatable on end face at the top of bottle cap lid to be provided with instruction disk 311, indicate to be provided with disk 311 with end face
The azimuth mark 311a of the measuring flume positioning mark corresponding matching of block 120 on orientation number and measuring flume 100, indicates that disk 311 passes through
Elastic rotation mechanism is arranged on the top end face of lid 310, and rotates 45 degree every time;Indicate that disk often rotates 45 °, then azimuth mark
Also 45 ° are rotated.
Generally eight prisms of bottle cap lid 310, the octagon side of eight prisms is corresponding with measuring flume insert port 110 to match somebody with somebody
Close, form the locating surface 312 positioned to bottle cap rotational orientation, and distribution corresponding with octagonal lid top end face,
It is 45 ° that lid 310, which often rotates an orientation, and it can ensure that installation and measurement accuracy;Lid bottom end face is provided with and sample
The placement positioning port 313 that bottle bottleneck detachably connects, present invention placement positioning port 313 is the spiral shell being spirally connected with sample bottle bottleneck 210
Line mouthful, specifically disposes positioning port to use internal thread, and bottleneck uses external screw thread, or placement positioning port to use external screw thread, bottleneck
Using internal thread;Do not limit herein, as long as both can be threaded togather;In addition to screw thread, it can also be adopted
It is detachably connected mode with other well known and is fixed, is not added with repeating herein;Shade 320 and measuring flume insert port at the top of lid
End face coordinate.
The invention also discloses a transmissometer, transmissometer is by measuring flume 100, sample bottle 200 and turbidimetry optics
With device composition, the top of measuring flume 100 is provided with measuring flume insert port 110, and sample bottle 200 is when mounted from measuring flume insert port
Load in 110, the diameter of measuring flume insert port 110 is slightly larger than the width of sample bottle body, the height and width of measuring flume are big
In the length and width of sample bottle, it is easy to sample bottle can be hanging in measuring flume 100 when installing so that sample bottle not with measurement
The inwall of groove 100 is contacted, when solving existing sample bottle positioning, and sample bottle surface is easily scratched or by dirt with positioning means contacts
The problem of dye, it improves the precision of optical match measurement.
Locating surface 312 on bottle cap lid of the present invention and be hermetic seal between the mounting surface of measuring flume insert port, it can subtract
The flowing of few measuring flume inner air and outer air, improves the degree of accuracy of measurement.
It is shown in Figure 6, indicate on end face at the top of the sample bottle positioning bottle-cover lid azimuth mark in disk with it is any one
During individual orientation number alignment, the vertical central axis of the vertical central axis and azimuth mark 311a of measuring flume positioning mark block 120
Point-blank.
The present invention is additionally provided with stopper slot 130 in the bottom of measuring flume 100, and the section of stopper slot 130 is and sample bottle bottom of bottle
The U-shaped structure of matching, stopper slot 130 is located at the underface of mounting groove insert port 110, and its length is equal to the width of sample bottle bottom of bottle
Degree, sample bottle is after installing, and its bottom of bottle sub-fraction is contacted with stopper slot, and stopper slot plays the work for limiting sample bottle position
With stability when improving sample bottle installation and measuring so that sample bottle will not be produced in measurement and rocked, so as to improve
Measurement accuracy.
In order to improve the degree of accuracy of optical match, bottle cap lid of the present invention is not common cylindrical structure, but eight ribs
Column structure, the lid of eight prisms has 1 degree of taper, and it causes lid to be up-small and down-big structure, using the structure just
In the installation of lid;In order to coordinate the structure of bottle cap lid, measuring flume insert port 110 is also configured as matching with bottle cap cover body structure
Octagon structure;Lid can be accurately positioned when being arranged in measuring flume insert port to sample bottle, and be rotated every time equal
45 degree of progress optics pairings can accurately be rotated.
Invention additionally discloses a kind of localization method of transmissometer sample, comprise the following steps that:
(1)The bottleneck of sample bottle is placed in the placement positioning port on transmissometer sample bottle positioning bottle-cover lid, realized
Sample bottle is fixedly connected with transmissometer sample bottle positioning bottle-cover, and the present invention uses threaded connection, sample bottle and transmissometer
Sample bottle positioning bottle-cover is fixed together after being connected through a screw thread.
(2)The positioning bottle-cover for being connected with sample bottle is pacified by its octagon locating surface and the octagon of measuring flume insert port
Dress face coordinates, and make it that the measuring flume positioning mark block on the orientation number and measuring flume on positioning bottle-cover is symmetrical, is thus determined
Position;
(3)After positioning, the positioning bottle-cover for being connected with sample bottle is assigned into measuring flume from measuring flume insert port so that fixed
The sample bottle connected on the bottle cap of position is vacantly placed in measuring flume, is not directly contacted with measuring flume, because locating surface and measuring flume are slotting
Attachment structure between entrance is matched using octagon so that it is 45 ° that positioning bottle-cover, which often rotates an orientation, in bottle cap
Lower sample bottle is driven also to rotate 45 °, which raises the stability and precision during positioning.
The invention also discloses a kind of sample bottle identification method, identification method comprises the following steps:
(1)In the sample bottle that high purity water is added to cleaning, and sample bottle positioning bottle-cover is fixedly connected with sample bottle, herein
Using threaded connection;
(2)By sample bottle wiped clean, and the painting last layer silicone oil on sample bottle, then by sample bottle positioning bottle-cover
Sample bottle, is inserted into measuring flume by the alignment measuring flume positioning mark block of orientation number 1 after alignment from measuring flume insert port;
(3)Apparatus measures key, record number and reading value are pressed, after number No. 1 position measurement in orientation is finished, by sample bottle
Positioning bottle-cover is separated with measuring flume insert port, 45 ° of rotation sample bottle positioning bottle-covers, and ensures the orientation on sample bottle positioning bottle-cover
The alignment measuring flume positioning mark block of number 2, then sample bottle is inserted in measuring flume, is put into after finishing, presses apparatus measures key, remember
Record number and reading value;So measure successively totally 8 times, azimuth mark is turned into reading value minimum after being compared to 8 data
Orientation number;
(4)From now on when using the sample bottle, as long as azimuth mark can be obtained by with measuring flume positioning mark block alignment
Accurate reading.
In general, a transmissometer is commonly provided with 2-6 sample bottle, and user's validation instrument work at any time for convenience is
No normal, instrument may be equipped with 1 or 1 set secondary correction solution easily and fast, in order to ensure the consistent of these sample bottles
Property, it is necessary to optics pairing is carried out to sample bottle used.
The invention also discloses a kind of optical match method of multiple sample bottles, optical match method comprises the following steps:
(1)The step being first according in claim 8 is identified measurement to first sample bottle, records reading value, and
Azimuth mark is turned into the minimum orientation number of reading value:
(2)Step in by second sample bottle according to claim 8 is identified measurement, and records reading value, directly
To when obtaining reading and first sample bottle least count difference less than ± 0.1NTU, azimuth mark block is turned into the reading corresponding
Orientation number, such second sample bottle and first sample bottle optical match are completed;
(3)Repeat step(2)Optical match is carried out to other sample bottles.
Herein it must be noted that:Due to glass material and the difference made, not every sample bottle can be matched, this
The sample bottle that can not be matched a bit can be used when being measured using only a sample bottle.
In order to verify the actual effect of turbidimetry optical match device, we are using the sample bottle group Jing Guo optical match
Tested with 5-120NTU standard turbidity solution, test result such as following table:
The general principle and principal character and advantages of the present invention of the present invention has been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the simply explanation described in above-described embodiment and specification is originally
The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (8)
1. a kind of turbidimetry optical match device, the measuring flume and sample bottle of the optical match device and transmissometer match
Close, it is characterised in that the optical match device includes transmissometer sample bottle positioning bottle-cover and the measurement being arranged on measuring flume
Groove positioning mark block, the bottle cap includes lid and the shade stretched out at the top of lid, and the top end face of the shade is
It is provided with octagon, and every side at the top of corresponding orientation number, lid and is rotatably provided with instruction disk, the finger on end face
Show the azimuth mark set on disk with the measuring flume positioning mark block corresponding matching on the orientation number and measuring flume on end face, it is described
Indicate that disk is arranged at the top of lid on end face by elastic rotation mechanism, and rotate 45 ° every time;Indicate that disk often rotates 45 °, then side
Position mark also rotates 45 °;The lid generally eight prisms, the octagon side of eight prisms is corresponding with measuring flume insert port
Coordinate, form the locating surface positioned to bottle cap rotational orientation, and distribution corresponding with octagonal lid top end face, lid
It is 45 ° that body, which often rotates an orientation, to ensure to install and measurement accuracy;The lid bottom end face is provided with and sample bottle bottle
The placement positioning port that mouth detachably connects;Shade and the end face of measuring flume insert port at the top of the lid coordinate;The turbidity
Instrument sample bottle positioning bottle-cover, is positioned to sample bottle, and it is directly contacted with bottleneck, without being contacted with body.
2. a kind of turbidimetry optical match device according to claim 1, it is characterised in that the placement positioning port is
The screw thread mouth being spirally connected with sample bottle bottleneck.
3. a kind of turbidimetry optical match device according to claim 1, it is characterised in that the lid of eight prism
Body has 1 degree of taper.
4. a kind of transmissometer, it includes measuring flume and sample bottle, it is characterised in that the transmissometer also includes claims 1 to 3
Any one of turbidimetry optical match device, measuring flume top be provided with measuring flume insert port, sample bottle is when mounted
Inserted into the mouth loading from measuring flume, the diameter of measuring flume insert port is slightly larger than the width of sample bottle body, the height of measuring flume and
Width is all higher than the length and width of sample bottle;
Transmissometer sample bottle positioning bottle-cover in the optical match device is connected by placement positioning port thereon with sample bottle,
Coordinated again by its octagon locating surface and measuring flume insert port, assign into measuring flume and insert into the mouth so that sample bottle is vacantly put
In measuring flume, it is not directly contacted with measuring flume;
Locating surface on bottle cap lid and be hermetic seal between the mounting surface of measuring flume insert port, it can reduce outer space in measuring flume
The flowing of gas, improves the degree of accuracy of measurement.
5. a kind of transmissometer according to claim 4, it is characterised in that the bottom of the measuring flume is correspondingly arranged on and sample
The stopper slot that product bottle coordinates.
6. a kind of localization method of transmissometer sample bottle, it is characterised in that the localization method is based on one of claim 4 or 5
Described transmissometer is implemented, and it comprises the following steps:
(1) bottleneck of sample bottle is placed in the placement positioning port on transmissometer sample bottle positioning bottle-cover, realize sample bottle with
Transmissometer sample bottle positioning bottle-cover is fixedly connected;
(2) positioning bottle-cover for being connected with sample bottle is disposed to pass through its octagon locating surface and the cooperation of measuring flume insert port so that fixed
Orientation number on the bottle cap of position is corresponding with the measuring flume positioning mark block on measuring flume, is thus positioned;
(3) positioning bottle-cover for being connected with sample bottle will be disposed to assign into measuring flume to insert into the mouth so that connect on positioning bottle-cover
Sample bottle is vacantly placed in measuring flume, is not directly contacted with measuring flume.
7. a kind of sample bottle identification method, it is characterised in that the identification method is based on turbid described in one of claim 4 or 5
Spend instrument to implement, it comprises the following steps:
(1) high purity water is added in the sample bottle of cleaning, and sample bottle positioning bottle-cover is fixedly connected with sample bottle;
(2) by sample bottle wiped clean, and last layer silicone oil is applied on sample bottle, then by the orientation number on sample bottle positioning bottle-cover
Code alignment measuring flume positioning mark block, inserts sample bottle in measuring flume after alignment;
(3) apparatus measures key, record number and reading value are pressed, is so measured successively totally 8 times, after being compared to 8 data
Azimuth mark is turned into the minimum orientation number of reading value;
(4) when using the sample bottle, azimuth mark and measuring flume positioning are marked block alignment to obtain accurate reading.
8. a kind of optical match method of multiple sample bottles, it is characterised in that the optical match method comprises the following steps:
(1) step being first according in claim 7 is identified measurement to first sample bottle, records reading value, and general side
Position mark turns to the minimum orientation number of reading value:
(2) step in by second sample bottle according to claim 7 is identified measurement, and records reading value, until obtaining
When being less than ± 0.1NTU to reading and first sample bottle least count difference, azimuth mark block is turned into the corresponding orientation of the reading
Number, such second sample bottle and first sample bottle optical match are completed;
(3) repeat step (2) carries out optical match to other sample bottles.
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CN1401766A (en) * | 2001-08-15 | 2003-03-12 | 中国科学院遗传研究所 | Method for high-efficiency introducing exogenous genetic matter into living cell |
CN1488074A (en) * | 2000-12-20 | 2004-04-07 | 纳球有限公司 | Device for conducting assays |
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CN1488074A (en) * | 2000-12-20 | 2004-04-07 | 纳球有限公司 | Device for conducting assays |
CN1401766A (en) * | 2001-08-15 | 2003-03-12 | 中国科学院遗传研究所 | Method for high-efficiency introducing exogenous genetic matter into living cell |
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