CN103525248A - Composite floor paint, preparation method thereof and using method thereof - Google Patents
Composite floor paint, preparation method thereof and using method thereof Download PDFInfo
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- CN103525248A CN103525248A CN201310465796.3A CN201310465796A CN103525248A CN 103525248 A CN103525248 A CN 103525248A CN 201310465796 A CN201310465796 A CN 201310465796A CN 103525248 A CN103525248 A CN 103525248A
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Abstract
The invention belongs to the technical field of floor paint, and particularly relates to composite floor paint, a preparation method thereof and a using method thereof. The composite floor paint comprises an epoxy primer, leveling blanket paint and surface coating paint. The surface coating paint comprises solvent-free epoxy self-leveling surface paint and polyurethane finish paint. When construction is performed, the epoxy primer, the leveling blanket paint, the solvent-free epoxy self-leveling surface paint and the polyurethane finish paint are painted in order on a pretreated floor. The composite floor paint has a low content of volatile organic compounds, and is suitable for indoor or outdoor floor decorative painting. A composite floor manufactured by the composite floor paint is antiskid, wear resistant, acid and alkali resistant and weather-proof, and is high in hardness, high in bonding strength with a floor base surface.
Description
Technical field
The present invention relates to terrace paint technical field, relate in particular to a kind of compound terrace paint and preparation method thereof and using method.
Background technology
Terrace paint is mainly used in the building ground in the places such as industrial premises, warehouse, parking lot, market, playground, school, hospital and office and decorates.Terrace paint can be divided into the kinds such as epoxy flooring coating, polyurethane floor coatings, vinyl floor coating and acrylic ester floor coating.
Parking garage is often used epoxy flooring coating to carry out application to the building ground in parking lot, and motor pool is used polyurethane coating to carry out application to the building ground in parking lot conventionally.The driving region of parking garage is different with the terrace coating of parking area, and parking area is level and smooth epoxide terrace coating, and driving region is anti-skidding epoxide terrace coating.Level and smooth epoxide terrace coating has the features such as easy to clean and wear-resisting, but it is not anti-skidding, so vehicle easily skids in this region and produces ear-piercing sound.The general employing of anti-skidding epoxide terrace broadcasted sowing the aggregates such as coarse grained quartz sand, roller coating one deck epoxy finish on the aggregate layer broadcasting sowing again, this coating good antiskid effect, but there is the aggregate of water caltrop larger to the wearing and tearing of tire, during running car, can produce larger friction sound, and this coating is difficult to clean.In addition, because the outside durabitity of epoxide terrace coating is poor, easy xanthochromia, easily efflorescence, so epoxide terrace coating is only applicable to indoor use.And the polyurethane floor coatings that at present Outdoor Parking place is used, it contains a large amount of organic solvents, can discharge a large amount of volatile organic matters in construction process, and the feature of environmental protection is poor and be unfavorable for that workmen's is healthy.
Summary of the invention
The object of the invention is to overcome the defect of prior art, a kind of indoor and outdoor all applicable, anti-skidding, wear-resisting, weather-proof and compound terrace paint that organic solvent content is low and the preparation method of this compound terrace paint are provided.
Another object of the present invention is to provide a kind of using method about above-mentioned compound terrace paint.
For achieving the above object, the present invention is by the following technical solutions:
A terrace paint, comprises epoxy primer, screed-coat coating and finishing coat coating, and described finishing coat coating is comprised of solvent-free epoxy self-leveling finish paint and polyurethane finish;
Described polyurethane finish is comprised of the material of following mass percent: 5～10% catalyst solution is A
1component; 30～50% aliphatic isocyanates prepolymer is B
1component; 25～40% 150～300 order aluminum oxide aggregates are C
1component; 8～13% colour polyurethane paste is D
1component;
Described solvent-free epoxy self-leveling finish paint is comprised of the material of following mass percent: 25～40% liquid epoxies, 3～10% reactive thinner, 30～45% 325～600 order silica powders, 1～10% auxiliary agent, 3～10% epoxy mill bases are B
2component; 12～25% modification alicyclic ring amine curing agent is A
2component;
Described screed-coat coating is comprised of the material of following mass percent: 50～70% liquid epoxies, 5～10% reactive thinner are B
3component; 30～100% 100 order quartz sands and 200 order silica powders are C
3component; 20～35% modification alicyclic ring amine curing agent is A
3component.
Described epoxy primer is comprised of the material of following mass percent: 50～70% liquid epoxies, 5～10% reactive thinner are B
4component; 20～35% modification alicyclic ring amine curing agent is A
4component.
Described auxiliary agent is comprised of following weight part material: defoamer 0.1-0.5 part, flow agent 0.2-0.5 part, anti-settling agent 0.2-1.0 part
Described defoamer is at least one in BYK-A501, BYK-057, BYK-066N, TEGO-900 and EFKA-2722.At least one in described flow agent BYK-320, BYK-333, EFKA-3777 and TEGO-1484.Described anti-settling agent is at least one in A-200, SD-2 and R-972.
Described catalyst solution is by ultraviolet absorbers, photostabilizer, catalyzer, the second flow agent and solvent composition.The weight part of each material is: catalyzer 0.1-0.5 part, ultraviolet absorbers 0.5-1.0 part, photostabilizer 0.1-0.5 part, flow agent 0.1-0.5 part.
Preferably, ultraviolet absorbers is steady 1130 over being day, and photostabilizer be steady 292 over sky, and flow agent is BYK-306, and solvent is dipropylene glycol methyl ether acetate (DPMA).Catalyzer is at least one in stannous octoate, dibutyl tin dilaurate and dimethylethanolamine.
Described aliphatic isocyanates prepolymer is at least one in hexamethylene diisocyanate biuret, hexamethylene diisocyanate trimer and hexamethylene diisocyanate polymer.Particularly, aliphatic isocyanates prepolymer is at least one in TPA-100, TLA-100, N3300 and N3400.
Described liquid epoxies is at least one in lower molecular weight bisphenol-A liquid epoxy resin and lower molecular weight Bisphenol F type liquid epoxies; Described lower molecular weight bisphenol-A liquid epoxy resin is at least one in EPON828, DER331, GELR128 and NPEL128; Described lower molecular weight Bisphenol F type liquid epoxies is at least one in EPON862 and DER351.
Described reactive thinner is phenyl glycidyl ether (PGE), C
12-14at least one in alkyl glycidyl ether (AGE) and neodecanoic acid glycidyl ester (E-10).
Described modification alicyclic ring amine curing agent is at least one in the different fluorine that of modification ketone Diamines solidifying agent, modification cyclohexanediamine class solidifying agent and modified methyl ring pentamethylene diamine class solidifying agent.Particularly, modification alicyclic ring amine curing agent is at least one in Ancamine 1618, Epikure F205 and Versamine C-31.
The preparation method of the above compound terrace paint is as follows:
The preparation method of described polyurethane finish comprises the following steps: take respectively in proportion each component and each component is distinguished to independent packaging, wherein A
1, D
1before component independent packaging, first mix.Hybrid mode is: solvent, flow agent, photostabilizer, UV light absorber, catalyzer, under the rotating speed of 300-500r/min, are stirred to 10-20min, after stirring, filter and package as A
1component; Mill base, under the rotating speed of 500-800r/min, is stirred to 10-20min, stir.
The preparation method of described solvent-free epoxy self-leveling finish paint comprises the following steps: take respectively in proportion each component and each component is distinguished to independent packaging, wherein B
2before component independent packaging, first mix.Hybrid mode is: lower molecular weight bisphenol-A liquid epoxy resin, lower molecular weight Bisphenol F type liquid epoxies and reactive thinner, under the rotating speed of 300-500r/min, are stirred to 5-10min; Then under the rotating speed of 500-800r/min, add auxiliary agent, churning time is 5-10min; Then under 700-1300r/min rotating speed, add 325-600 order silica powder, dispersion 30min is less than 100 microns to fineness above, then adds epoxy mill base, under the rotating speed of 500-800r/min, disperses 5-10min to mix.
The preparation method of described screed-coat coating comprises the following steps: take respectively in proportion each component and each component is distinguished to independent packaging, wherein B
3before component independent packaging, first mix.Hybrid mode is: lower molecular weight bisphenol-A liquid epoxy resin, lower molecular weight Bisphenol F type liquid epoxies and reactive thinner are stirred to 10-20min under the rotating speed of 300-500r/min and mix.
The preparation method of described epoxy primer comprises the following steps: take respectively in proportion each component and each component is distinguished to independent packaging, wherein B
4before component independent packaging, first mix.Hybrid mode is: first lower molecular weight bisphenol a liquid epoxy resin, lower molecular weight Bisphenol F type liquid epoxies and reactive thinner are stirred to 5-10min under the rotating speed of 300-500r/min and mix, then under the rotating speed of 500-800r/min, add auxiliary agent, stirring 5-10min mixes, then under 700-1300r/min rotating speed, add silica powder, high speed dispersion 30min is above is less than 100 microns to fineness.
The using method of compound terrace paint above, comprises the following steps:
(1) first by A
4component and B
4component mixes, and is then coated on and carries out on pretreated ground, forms undercoat, and the consumption of epoxy primer is 0.3-0.5kg/ ㎡;
(2) after undercoat is done solid work, by A
3component, B
3component and C
3component mixes, and is then coated on levelling on undercoat, forms screed-coat, and the consumption of screed-coat coating is 0.3-1.0kg/ ㎡;
(3) after screed-coat is done solid work, by A
2component and B
2component mixes, and is then coated on screed-coat, forms solvent-free epoxy self-leveling top coat layer, and the consumption of solvent-free epoxy self-leveling finish paint is 0.8-1.8kg/ ㎡;
(4) after solvent-free epoxy self-leveling top coat layer is done solid work, by A
1component, B
1component, C
1component and D1 component mix, and are then coated on solvent-free epoxy self-leveling top coat layer, form polyurethane finish layer, and the consumption of polyurethane finish is 0.1-0.15kg/ ㎡.
The total thickness of described undercoat, screed-coat and finishing coat is 1.0-2.5mm, and the thickness of described solvent-free epoxy self-leveling top coat layer is 0.5-2.0mm, and the thickness of polyurethane finish layer is 0.1-0.2mm.
Compared with prior art, the invention has the beneficial effects as follows: by the prepared terrace of coating of the present invention, anti-skid wearable performance is good, and applicable to the ground decoration application of indoor and outdoor, be particularly useful for the ground decoration application of parking garage and motor pool.Overcome level and smooth epoxide terrace and easily skidded, anti-slip epoxy floor is large to auto tire wear, friction sound is large, difficult cleans, epoxide terrace poor durability, and the high problem of polyurethane floor volatile organic solvent content.
By the prepared terrace of coating of the present invention, itself and terrace basal plane bonding strength is high, acid and alkali-resistance, anti-skidding, hardness can reach 4H, easy to clean, UV resistant, wear resistance is higher more than five times than common epoxy self-leveling floor, little to auto tire wear.And epoxy primer, screed-coat coating and solvent-free epoxy self-leveling finish paint are solventless coatings, and the solid content of polyurethane finish is also up to more than 90%, therefore in construction process, volatile organic matter burst size is low, environmental protection and can reduce the harm to workmen's health.
The terrace that the present invention can be applicable to require terrace to have anti-skidding, dustproof and wear-resistant etc. place is decorated application, as parking garage, motor pool, harbour, warehouse, market, school, hospital and playground etc.
Embodiment
In order to more fully understand technology contents of the present invention, below in conjunction with specific embodiment, technical scheme of the present invention is described further and is illustrated.
Embodiment 1
The proportioning raw materials of epoxy primer, screed-coat coating, solvent-free epoxy self-leveling finish paint, polyurethane finish is as shown in table 1.
The proportioning raw materials of each coated coating in table 1 embodiment 1
The preparation of epoxy primer: lower molecular weight bisphenol a liquid epoxy resin, lower molecular weight Bisphenol F type liquid epoxies and reactive thinner are stirred to 10-20min under the rotating speed of 300-500r/min and mix, after filtration and pack to obtain B
4component, obtains A by the independent packaging of no-solvent type modification aliphatic cyclic amine solidifying agent
4component.During construction, by A
4component and B
4component is mixed and the no-solvent type epoxy primer that stirs to obtain.
The preparation of screed-coat coating: lower molecular weight bisphenol-A liquid epoxy resin, lower molecular weight Bisphenol F type liquid epoxies and reactive thinner are stirred to 10-20min under the rotating speed of 300-500r/min and mix, pack after filtration to obtain B
3component; The independent packaging of no-solvent type modification alicyclic ring amine curing agent is obtained to A
3component; 100 order quartz sands and 200 order silica powders are mixed to rear independent packaging and obtain C
3component.During construction, by A
3component, B
3component and C
3component is mixed and the no-solvent type epoxy alignment material that stirs to obtain.
The preparation of solvent-free epoxy self-leveling finish paint: lower molecular weight bisphenol-A liquid epoxy resin, lower molecular weight Bisphenol F type liquid epoxies and reactive thinner, under the rotating speed of 300-500r/min, are stirred to 5-10min and mix; Then under the rotating speed of 500-800r/min, add auxiliary agent, stir 5-10min and mix; Then under 700-1300r/min rotating speed, add 325-600 order silica powder, high speed dispersion 30min is less than 100 microns to fineness above, then adds epoxy mill base, under the rotating speed of 500-800r/min, disperses 5-10min to mix, and packs after filtration to obtain B
2component; By A
2component independent packaging.During construction, by A
2component, B
2component is mixed and the epoxy self-leveling finishing coat coating that stirs to obtain.
The preparation of polyurethane finish: solvent, flow agent, photostabilizer, UV light absorber, catalyzer, under the rotating speed of 300-500r/min, are stirred to 10-20min, filter and package as A after stirring
1component; By B
1component independent packaging; By C
1component independent packaging; Mill base, under the rotating speed of 500-800r/min, is stirred to 10-20min, after stirring, filter and package as D
1component.During construction, by A
1component, B
1component, C
1component and D
1component is mixed and the finishing coat coating that stirs to obtain.
The using method of compound terrace paint:
With sander by the ground dust suction of polishing, in the epoxy resin grouting solidating of loosely organized part.By A
4component and B
4component mix and by its roller coating on pretreated ground, form undercoat, and the consumption of epoxy primer is 0.3kg/ ㎡; After undercoat solidifies, by A
3component, B
3component and C
3component mixes and by the levelling on undercoat of its blade coating, forms screed-coat, and the consumption of screed-coat coating is 1.0kg/ ㎡; After the curing at least 16h of screed-coat, by A
2component and B
2component mixes and its trowel is applied on screed-coat, forms solvent-free epoxy self-leveling top coat layer, and the consumption of solvent-free epoxy self-leveling finish paint is 0.8kg/ ㎡; Solvent-free epoxy self-leveling top coat layer solidifies after 16h, by A
1component, B
1component, C
1component and D
1component mixes, with flat mouth scraper by its blade coating on solvent-free epoxy self-leveling top coat layer, and then with 10mm undercoat cylinder, along direction in length and breadth, roll even, formation polyurethane finish layer, the consumption of polyurethane finish is 0.1kg/ ㎡.
Until anti-skid wearable polyurethane finish layer, solidify after 16 hours, pedestrian can walk in coating, solidifies after 7 days, and coating just can be used.
The compound terrace consisting of undercoat, screed-coat, solvent-free epoxy self-leveling top coat layer and polyurethane finish layer, its performance is as shown in table 4.
Embodiment 2
The proportioning raw materials of epoxy primer, screed-coat coating, solvent-free epoxy self-leveling finish paint, polyurethane finish is as shown in table 2.
The proportioning raw materials of each coated coating in table 2 embodiment 2
The preparation method of the epoxy primer of the present embodiment, screed-coat coating, solvent-free epoxy self-leveling finish paint and polyurethane finish is identical with method described in embodiment 1.
Using method described in the using method of the compound terrace paint of the present embodiment and embodiment 1 is basic identical, and difference is: the consumption of screed-coat coating is 0.5kg/ ㎡; The consumption of solvent-free epoxy self-leveling finish paint is 1.5kg/ ㎡, and the consumption of polyurethane finish is 0.15kg/ ㎡.
The compound terrace consisting of undercoat, screed-coat, solvent-free epoxy self-leveling top coat layer and polyurethane finish layer, its performance is as shown in table 4.
Embodiment 3
The proportioning raw materials of epoxy primer, screed-coat coating, solvent-free epoxy self-leveling finish paint, polyurethane finish is as shown in table 3.
The proportioning raw materials of each coated coating in table 3 embodiment 3
The preparation method of the epoxy primer of the present embodiment, screed-coat coating, solvent-free epoxy self-leveling finish paint and polyurethane finish is identical with method described in embodiment 1.
Using method described in the using method of the compound terrace paint of the present embodiment and embodiment 1 is basic identical, and difference is: the consumption of screed-coat coating is 0.3kg/ ㎡; The consumption of solvent-free epoxy self-leveling finish paint is 1.8kg/ ㎡, and the consumption of polyurethane finish is 0.13kg/ ㎡.
The compound terrace consisting of undercoat, screed-coat, solvent-free epoxy self-leveling top coat layer and polyurethane finish layer, its performance is as shown in table 4.
The performance test data of the formed compound terrace of table 4 embodiment 1-3
The above only further illustrates technology contents of the present invention with embodiment, so that reader is easier to understand, but does not represent that embodiments of the present invention only limit to this, and any technology of doing according to the present invention is extended or recreation, is all subject to protection of the present invention.
Claims (8)
1. a compound terrace paint, is comprised of epoxy primer, screed-coat coating and finishing coat coating, it is characterized in that, described finishing coat coating is comprised of solvent-free epoxy self-leveling finish paint and polyurethane finish;
Described polyurethane finish is comprised of the material of following mass percent: 5～10% catalyst solution is A
1component; 30～50% aliphatic isocyanates prepolymer is B
1component; 25～40% 150～300 order aluminum oxide aggregates are C
1component; 8～13% colour polyurethane paste is D
1component;
Described solvent-free epoxy self-leveling finish paint is comprised of the material of following mass percent: 25～40% liquid epoxies, 3～10% reactive thinner, 30～45% 325～600 order silica powders, 1～10% auxiliary agent, 3～10% epoxy mill bases are B
2component; 12～25% modification alicyclic ring amine curing agent is A
2component;
Described auxiliary agent is comprised of following weight part material: defoamer 0.1-0.5 part, flow agent 0.2-0.5 part, anti-settling agent 0.2-1.0 part.
2. compound terrace paint according to claim 1, is characterized in that, described screed-coat coating is comprised of the material of following mass percent: 50～70% liquid epoxies, 5～10% reactive thinner are B
3component; 30～100% 100 order quartz sands and 200 order silica powders are C
3component; 20～35% modification alicyclic ring amine curing agent is A
3component.
3. compound terrace paint according to claim 2, is characterized in that, described epoxy primer is comprised of the material of following mass percent: 50～70% liquid epoxies, 5～10% reactive thinner are B
4component; 20～35% modification alicyclic ring amine curing agent is A
4component.
4. compound terrace paint according to claim 1, is characterized in that, described aliphatic isocyanates prepolymer is at least one in hexamethylene diisocyanate biuret, hexamethylene diisocyanate trimer and hexamethylene diisocyanate polymer; Described catalyst solution is by ultraviolet absorbers, photostabilizer, catalyzer, the second flow agent and solvent composition; Described catalyzer is at least one in stannous octoate, dibutyl tin dilaurate and dimethylethanolamine.
5. according to compound terrace paint described in claim 1-4 any one, it is characterized in that, described liquid epoxies is at least one in lower molecular weight bisphenol-A liquid epoxy resin and lower molecular weight Bisphenol F type liquid epoxies; Described reactive thinner is phenyl glycidyl ether, C
12-14at least one in alkyl glycidyl ether and neodecanoic acid glycidyl ester; Described defoamer is at least one in BYK-A501, BYK-057, BYK-066N, TEGO-900 and EFKA-2722; Described flow agent is at least one in BYK-320, BYK-333, EFKA-3777 and TEGO-1484; Described anti-settling agent is at least one in A-200, SD-2 and R-972; Described modification alicyclic ring amine curing agent is at least one in the different fluorine that of modification ketone Diamines solidifying agent, modification cyclohexanediamine class solidifying agent and modified methyl ring pentamethylene diamine class solidifying agent.
6. a preparation method for compound terrace paint as claimed in claim 3, is characterized in that,
The preparation method of described polyurethane finish comprises the following steps: take respectively in proportion each component and each component is distinguished to independent packaging, wherein A
1and D
1before component independent packaging, first mix;
The preparation method of described solvent-free epoxy self-leveling finish paint comprises the following steps: take respectively in proportion each component and each component is distinguished to independent packaging, wherein B
2before component independent packaging, first mix;
The preparation method of described screed-coat coating comprises the following steps: take respectively in proportion each component and each component is distinguished to independent packaging, wherein B
3and C
3before component independent packaging, first mix;
The preparation method of described epoxy primer comprises the following steps: take respectively in proportion each component and each component is distinguished to independent packaging, wherein B
4before component independent packaging, first mix.
7. a using method for compound terrace paint as claimed in claim 3, is characterized in that, comprises the following steps:
(1) first by A
4component and B
4component mixes, and is then coated on and carries out on pretreated ground, forms undercoat, and the consumption of epoxy primer is 0.3-0.5kg/m
2;
(2) after undercoat is done solid work, by A
3component, B
3component and C
3component mixes, and is then coated on levelling on undercoat, forms screed-coat, and the consumption of screed-coat coating is 0.3-1.0kg/m
2;
(3) after screed-coat is done solid work, by A
2component and B
2component mixes, and is then coated on screed-coat, forms solvent-free epoxy self-leveling top coat layer, and the consumption of solvent-free epoxy self-leveling finish paint is 0.8-1.8kg/m
2;
(4) after solvent-free epoxy self-leveling top coat layer is done solid work, by A
1component, B
1component, C
1component and D
1component mixes, and is then coated on solvent-free epoxy self-leveling top coat layer, forms polyurethane finish layer, and the consumption of polyurethane finish is 0.1-0.15kg/m
2.
8. the using method of compound terrace paint according to claim 7, it is characterized in that, the total thickness of described undercoat, screed-coat and finishing coat is 1.0-2.5mm, and the thickness of described solvent-free epoxy self-leveling top coat layer is 0.5-2.0mm, and the thickness of polyurethane finish layer is 0.1-0.2mm.
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