CN103525151A - Environmentally-friendly interior wall putty powder, putty paste, and preparation methods of putty powder and putty paste - Google Patents
Environmentally-friendly interior wall putty powder, putty paste, and preparation methods of putty powder and putty paste Download PDFInfo
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Abstract
The invention discloses an environmentally-friendly interior wall putty powder, a putty paste, and preparation methods of the putty powder and the putty paste. The putty powder comprises, by weight, 45-72 parts of talcum powder, 18-30 parts of heavy calcium carbonate, 5-10 parts of calcium bentonite, 0.6-1.5 parts of carboxymethylcellulose sodium, 1-5 parts of polyacrylamide, 0.3-1.7 parts of hydroxyethyl cellulose, 0-20 parts of building gypsum powder, 0-0.8 parts of carboxymethyl cellulose, 0-8 parts of alpha-pregelatinized starch, 0-3 parts of hydroxypropyl methyl cellulose and 0-0.5 parts of sodium dodecyl benzene sulfonate. The preparation method of the putty powder comprises the following steps: uniformly mixing the above components, stirring for 10-15min, and discharging the above obtained mixture. The putty paste is obtained by adding water having a weight 0.3-0.5 times the weight of the putty powder and uniformly stirring. The putty powder/putty paste contains no or a tiny amount of formaldehyde and an extremely low content of heavy metal elements, is an environmentally-friendly product, and has the advantages of excellent impact resistance, excellent hydrophobicity and waterproofness, high elasticity, good crack resistance, stable storage and easy construction.
Description
Technical field
The invention belongs to decorative material for wall surface technical field, is building decorative gelatinous material, is specifically related to a kind of environment-friendly type putty powder and putty paste, and preparation method thereof.
Background technology
Inner wall putty is a kind of decoration gelatinous material of smooth surface of wall, in order to fill the space of metope and to repair, is coated with the upper rugged defect in surface, to can make coating or lacquer painting be coated on metope, can form smooth and uniform paint film.Because inner wall putty is used extensively, can be used for multiple different places, required functional requirement also has difference according to field of employment more.Thereby, the existing patent of invention about inner wall putty.Mainly contain as follows:
Aspect water-fast inner wall putty powder, CN1228399C discloses a kind of water-proof putty powder, it is that raw material 3:2:5 allotment by weight proportion forms by calcium hydroxide, white cement, coarse whiting, and above-mentioned raw materials adds methylcellulose gum 4-6 kilogram after being mixed evenly again in raw material per ton.CN1260313C discloses a kind of environmental protection type water resisting putty, mainly comprises the component of following weight parts: heavy calcium carbonate 70-75, light weight calcium acid calcium powder 20-35, grey matter calcium powder 50-55, alpha's starch 15-20, carboxymethyl cellulose 18-25, water-soluble gelatin powder 14-18.
Have aspect adsorption function putty powder, CN101585684B discloses a kind of attapulgite interior wall putty powder, Concavo-convex stick after purifying, activated attapulgite, white portland cement, polyacrylamide and anatase thpe white powder, consist of, its production method is: batching, pulverizing, abrasive dust, packing.Attapulgite interior wall putty powder is put into container, add water infiltration 5-30 minute, the ratio of attapulgite interior wall putty powder and water is l:0.5-1:4, after stirring, just can carry out knife-coat application.CN100564459C discloses a kind of water resistance putty powder with adsorption function and preparation method thereof.Zeolite powder and/or diatomite are used for to putty powder as sorbent material, give the performance of putty powder absorption toxic and harmful, and strengthen the sticking power of putty powder.In putty powder, use water-resisting agent, cross-linking starch especially, can obviously improve the water tolerance of putty powder.
Aspect nourishing function putty powder, CN101319103B discloses a kind of negative ion putty powder, by talcum powder, plant gum powder and tourmaline powder, is mixed.CN101225261B discloses a kind of architectural interior anion waterproof putty powder and preparation method thereof, by following weight part proportioning, is: activated calcium powder 100-300 part, Paris white 100-700 part, negative ion powder 50-200 part, organogel material 1-10 part, Mierocrystalline cellulose 1-5 part.Above-mentioned negative ion powder is the mixed powder of ultra-fine tourmaline powder and physisorption material, and wherein the fineness of ultra-fine tourmaline powder is more than 2.6um, and purity is more than 95%; Physisorption material is a kind of in diatomite and modified activated carbon, and the weight of physisorption material accounts for the 20-35% of negative ion powder gross weight.CN101418153B discloses a kind of health care putty powder, by the raw material of following parts by weight, is made: heavy calcium carbonate 60-65 part, calcium hydroxide powder 16-30 part, talcum powder 10-15 part, methylcellulose gum powder 0.5-1 part, bentonite in powder 1-2.5 part, titanium dioxide 0.5-1 part, plant long jiao powder 3-4 part, sandalwood powder 2-3 part, Japanese Honeysuckle flower dry powder 1-2 part, chrysanthemum flower dry powder 1-2 part, Long Gu Powder 2-3 part, Powder Phaseoli radiati 1-2 part.
Aspect environment-friendly type putty powder, CN102786828 discloses a kind of compound method of inner wall environmentally-friendly sealing compound rubber powder.Gelatinization Hydroxypropyl Tapioca Starch, pva powder, sodium bentonite (400 order), light calcium carbonate, Vltra tears, potassium aluminium sulfate, soda ash, the ammonia chloride being dried of take is raw material, and the technique that is aided with fragmentation, mixing is produced inner wall environmentally-friendly sealing compound rubber powder, can use with the material mixing such as talcum powder, dry powder, light calcium carbonate powder, grey calcium powder, terra alba, white cement, black cement, both glue can be produced, also putty powder, thermal insulation mortar etc. can be produced.
In the above-mentioned inner wall putty powder of mentioning, have plenty of in order to improve water tolerance, have plenty of in order to there is the functions such as absorption, health care, the former easy hollowing, peeling, cracking, and the latter's cohesive strength is lower, poor adhesive force, water resistance are poor.And aspect the preparation of environment-friendly type putty, composition and engineering program is complicated, contains unstable chemcial property, easily turn to be yellow and play the raw material of blackspot.
The known inner wall putty of China mostly adopts talcum powder, dry powder, carboxymethyl cellulose and formaldehyde polyvinyl acetal to stick the materials such as agent (107 glue) and is prepared from, although raw materials cost is low, but complex process, comprehensive cost is high, particularly contain the objectionable impuritiess such as formaldehyde, neural system to people has a great impact, and especially infant and elderly and infirm's harm are larger, even cause serious disease.
Summary of the invention
The object of the invention is to improve the environmental requirement of putty, provide a kind of not containing the environment-friendly type inner wall putty powder of formaldehyde and putty paste and preparation method thereof.
In order to reach above-mentioned technique effect, the present invention takes following technical scheme:
A putty powder, comprises the component of following weight part: basic raw material: talcum powder 45-72 part, water-ground limestone 18-30 part, calcium-base bentonite 5-10 part, Xylo-Mucine 0.6-1.5 part, polyacrylamide 1-5 part, Natvosol 0.3-1.7 part; Auxiliary material: the parts by weight of building gypsum plaster 0-20 part, carboxymethyl cellulose 0-0.8 part, α-pre-gelatinized starch 0-8 part, Vltra tears 0-3 part, Sodium dodecylbenzene sulfonate are 0-0.5 part.
Further technical scheme is: described talcous granularity is more than 200 orders, and as a part for filler, itself can improve the application property of slip, makes putty be easy to blade coating, increases surface flatness and reduces costs.
Further technical scheme is: the whiteness of described water-ground limestone is more than 80 degree, granularity is more than 200 orders, as stopping composition, can increase small product size, reduce costs, improve processing characteristics (as adjusting viscosity, rheological property, fluidizing performance), reinforcement or half reinforcement.
Further technical scheme is: the granularity of described calcium-base bentonite is more than 200 orders, not only cheap, itself has stronger water-absorbent, and can improve putty intensity, also has thickening power, can improve the thixotropy of putty slurry.
Described Xylo-Mucine (tackiness agent) easily the moisture absorption, odorless, can be directly water-soluble.The aqueous solution has good viscosity, stability, protective colloid and film-forming properties, is difficult for corrupt mildew, stable under alkalescence and solutions of weak acidity, cheap can use with carboxymethyl cellulose collocation.
Further technical scheme is: described polyacrylamide is a kind of macromolecular compound, in an embodiment of the present invention, has the effect of flocculation, bonding, thickening under neutral and acidic conditions, can further strengthen putty resistance to cleavage.
Described Natvosol (binding agent) is a kind of white or pale yellow powder, has good thickening, suspension, dispersion, emulsification, bonding, film forming, protection moisture and the characteristics such as protective colloid are provided.Water retention capacity exceeds one times than methylcellulose gum, has good flow adjustment; It is the poorest that its dispersive ability and generally acknowledged methylcellulose gum and Vltra tears are compared dispersive ability, but protective colloid ability is the strongest.
Further technical scheme is: described building gypsum plaster meets the requirement of GB9776-1988 standard, and granularity is more than 120 orders; Presetting period is no earlier than 6min, ultimate compression strength: be greater than 3MPa; Folding strength: be greater than 2MPa, in building gypsum plaster, the content of CaSO42H2O is less than 1%.
Described carboxymethyl cellulose or and the superiority of α-pre-gelatinized starch comprise thickening property, water-retentivity, metabolism inertia, film forming plasticity, dispersion stabilization etc., can be used as thickening material, tackiness agent, lubricant.
The water retention property of described Vltra tears makes slurry can, because of so dry that to chap too soon, not strengthen the rear intensity of sclerosis after smearing.
Described Sodium dodecylbenzene sulfonate (permeate agent) is white powder, can strengthen the infiltration affinity of putty and matrix.
The preparation method of described environment-friendly type inner wall putty powder, comprise the following steps: take 1/3 talcum powder and be placed in mixed stirring device, then according to the ascending auxiliary material that adds successively of parts by weight, after premix is even, again according to ascending remaining talcum powder and other the basic raw material of adding successively of parts by weight, after mixing, stir discharging after 10～15min.
A putty paste, comprises the component of following weight part: basic raw material: talcum powder 45-72 part, water-ground limestone 18-30 part, calcium-base bentonite 5-10 part, Xylo-Mucine 0.6-1.5 part, polyacrylamide 1-5 part, Natvosol 0.3-1.7 part; Auxiliary material: the parts by weight of building gypsum plaster 0-20 part, carboxymethyl cellulose 0-0.8 part, α-pre-gelatinized starch 0-8 part, Vltra tears 0-3 part, Sodium dodecylbenzene sulfonate are 0-0.5 part; Water, 0.3～0.5 times of above-mentioned solid ingredient gross weight.
In above-mentioned putty paste, described talcous granularity is more than 200 orders; The whiteness of described water-ground limestone is more than 80 degree, and granularity is more than 200 orders; The granularity of described calcium-base bentonite is more than 200 orders.Described building gypsum plaster meets the requirement of GB9776-1988 standard, and granularity is more than 120 orders; Presetting period is no earlier than 6min, ultimate compression strength: be greater than 3MPa; Folding strength: be greater than 2MPa, in building gypsum plaster, the content of CaSO42H2O is less than 1%.The preparation method of described environment-friendly type inner wall putty paste, comprise the following steps: take 1/3 talcum powder and be placed in mixed stirring device, then according to the ascending auxiliary material that adds successively of parts by weight, after premix is even, according to ascending remaining talcum powder and other the basic raw material of adding successively of parts by weight, after mixing, stir after 10～15min again, add uniformly water, stir discharging after 10～15min.
The difference of putty powder and putty paste is in component, whether have water, in putty paste, solid ingredient is consistent with component in putty powder, and the preparation method of putty paste adds water by putty powder to stir.
The present invention compared with prior art, has following beneficial effect:
(1) putty powder of the present invention and putty paste are white or grey, do not contain or only contain trace formaldehyde, and contents of heavy metal elements is extremely low, belongs to environmental type product.
(2) putty powder of the present invention and putty paste have good shock-resistance, good hydrophobicity and water-repellancy, snappiness, good resistance to cleavage, shelf-stable and easily construction.
(3) putty powder of the present invention and putty paste are applicable to indoor wall leveling, easily construction; Drying shrinkage dimensional change is little, can fill up fine cracks; Exquisite in texture, flat once scraping.
(4) preparation method of the present invention only needs component to mix, and preparation method is easy.
Embodiment
Below in conjunction with embodiments of the invention, the invention will be further elaborated.
Embodiment 1
1. by the proportioning raw materials of setting, weigh respectively basic raw material and auxiliary material, by weight, wherein basic raw material is: 50 parts of talcum powder, 25 parts of water-ground limestones, 10 parts of calcium-base bentonites, 1 part of Xylo-Mucine, 0.5 part of Natvosol, 4.9 parts of polyacrylamides; Auxiliary material is: 8 parts of α-pre-gelatinized starches, 0.6 part of carboxymethyl cellulose.
2. load weighted talcum powder is got approximately 1/3 and is placed in mixed stirring device according to a certain ratio, then the ascending auxiliary material that adds successively of percentage ratio by weight, premix evenly after ascending basic raw material and the remaining talcum powder of adding successively of percentage ratio by weight again, be uniformly mixed in advance.
3. discharging after the material high-speed stirring 10～15min directly step 2 being mixed, sends into finished bin, is finished product putty powder;
To in the putty powder of step 3 in solid-liquid weight ratio 1:(0.3～0.5) ratio adds required water equably, discharging after high-speed stirring 10～15min, sends into finished bin, is finished product putty paste.
Embodiment 2
1. by the proportioning raw materials of setting, weigh respectively basic raw material and auxiliary material, by weight, wherein basic raw material is: 60 parts of talcum powder, 18 parts of water-ground limestones, 6 parts of calcium-base bentonites, 0.6 part of Xylo-Mucine, 1 part of Natvosol, 1.5 parts of polyacrylamides; Auxiliary material is: the parts by weight of 12 parts of building gypsum plasters, Sodium dodecylbenzene sulfonate are 0.4 part of 0.5 part, carboxymethyl cellulose.
2. load weighted talcum powder is got approximately 1/3 and is placed in mixed stirring device according to a certain ratio, then the ascending auxiliary material that adds successively of percentage ratio by weight, premix evenly after ascending basic raw material and the remaining talcum powder of adding successively of percentage ratio by weight again, be uniformly mixed in advance.
3. discharging after material high-speed stirring 10～15min step 2 being mixed, sends into finished bin;
4. the powder of step 3 being produced is finished product putty powder after metering packing.
Embodiment 3
1. by the proportioning raw materials of setting, weigh respectively basic raw material and auxiliary material, by weight, wherein basic raw material is: 72 parts of talcum powder, 10 parts of water-ground limestones, 5 parts of calcium-base bentonites, 0.6 part of Xylo-Mucine, 0.3 part of Natvosol, 1.3 parts of polyacrylamides; Auxiliary material is: 10 parts of building gypsum plasters, 0.3 part of α-pre-gelatinized starch, 0.5 part of Vltra tears.
2. treatment step 2～4 is identical with embodiment 2.
Embodiment 4:
1. by the proportioning raw materials of setting, weigh respectively basic raw material and auxiliary material, by weight, wherein basic raw material is: 47 parts of talcum powder, 30 parts of water-ground limestones, 10 parts of calcium-base bentonites, 1 part of Xylo-Mucine, 0.8 part of Natvosol, 1.2 parts of polyacrylamides; Auxiliary material is: 8 parts of α-pre-gelatinized starches, 2 parts of Vltra tearss.
2. treatment step 2～4 is identical with embodiment 1.
Embodiment 5:
1. by the proportioning raw materials of setting, weigh respectively basic raw material and auxiliary material, by weight, wherein basic raw material is: 65 parts of talcum powder, 20 parts of water-ground limestones, 9 parts of calcium-base bentonites, 1 part of polyacrylamide, 1.5 parts of Xylo-Mucines, 0.5 part of Natvosol; Auxiliary material is: 2 parts of α-pre-gelatinized starches, 1 part of Vltra tears.
2. treatment step 2～4 is identical with embodiment 1.
Embodiment 6:
1. by the proportioning raw materials of setting, weigh respectively basic raw material and auxiliary material, by weight, wherein basic raw material is: 53 parts of talcum powder, 23 parts of water-ground limestones, 7 parts of calcium-base bentonites, 5 parts of polyacrylamides, 1.2 parts of Natvosols, 1.5 parts of Xylo-Mucines; Auxiliary material is: the parts by weight of 6.8 parts of α-pre-gelatinized starches, 2 parts of Vltra tearss, Sodium dodecylbenzene sulfonate are 0.5 part.
2. treatment step 2～4 is identical with embodiment 1.
The concrete effect of product of the present invention, comprises physical parameter and limit of harmful substance parameter, in Table 1 and table 2.
Table 1 physical parameter
Table 2 limit of harmful substance parameter
Although with reference to explanatory embodiment of the present invention, invention has been described here, above-described embodiment is only preferably embodiment of the present invention, embodiments of the present invention are not restricted to the described embodiments, should be appreciated that, those skilled in the art can design a lot of other modification and embodiments, and these are revised and within embodiment will drop on the disclosed principle scope and spirit of the application.
Claims (10)
1. an environment-friendly type inner wall putty powder, is characterized in that comprising the component of following weight part:
Basic raw material:
Talcum powder 45-72 part,
Water-ground limestone 18-30 part,
Calcium-base bentonite 5-10 part,
Xylo-Mucine 0.6-1.5 part,
Polyacrylamide 1-5 part,
Natvosol 0.3-1.7 part;
Auxiliary material:
Building gypsum plaster 0-20 part,
Carboxymethyl cellulose 0-0.8 part,
α-pre-gelatinized starch 0-8 part,
Vltra tears 0-3 part,
The parts by weight of Sodium dodecylbenzene sulfonate are 0-0.5 part.
2. environment-friendly type inner wall putty powder according to claim 1, is characterized in that described talcous granularity is more than 200 orders.
3. environment-friendly type inner wall putty powder according to claim 1, is characterized in that the whiteness of described water-ground limestone is more than 80 degree, and granularity is more than 200 orders.
4. environment-friendly type inner wall putty powder according to claim 1, is characterized in that the granularity of described calcium-base bentonite is more than 200 orders.
5. environment-friendly type inner wall putty powder according to claim 1, is characterized in that described building gypsum plaster meets the requirement of GB9776-1988 standard, and granularity is more than 120 orders; Presetting period is no earlier than 6min, ultimate compression strength: be greater than 3MPa; Folding strength: be greater than 2MPa, CaSO in building gypsum plaster
42H
2the content of O is less than 1%.
6. the preparation method of the environment-friendly type inner wall putty powder described in claim 1-5 any one, it is characterized in that comprising the following steps: take 1/3 talcum powder and be placed in mixed stirring device, then according to the ascending auxiliary material that adds successively of parts by weight, after premix is even, again according to ascending remaining talcum powder and other the basic raw material of adding successively of parts by weight, after mixing, stir discharging after 10～15min.
7. an environment-friendly type inner wall putty paste, is characterized in that comprising the component of following weight part:
Basic raw material:
Talcum powder 45-72 part,
Water-ground limestone 18-30 part,
Calcium-base bentonite 5-10 part,
Xylo-Mucine 0.6-1.5 part,
Polyacrylamide 1-5 part,
Natvosol 0.3-1.7 part;
Auxiliary material:
Building gypsum plaster 0-20 part,
Carboxymethyl cellulose 0-0.8 part,
α-pre-gelatinized starch 0-8 part,
Vltra tears 0-3 part,
The parts by weight of Sodium dodecylbenzene sulfonate are 0-0.5 part;
Water, 0.3～0.5 times of above-mentioned solid ingredient gross weight.
8. environment-friendly type inner wall putty paste claimed in claim 7, is characterized in that described talcous granularity is more than 200 orders; The whiteness of described water-ground limestone is more than 80 degree, and granularity is more than 200 orders; The granularity of described calcium-base bentonite is more than 200 orders.
9. environment-friendly type inner wall putty paste claimed in claim 7, is characterized in that described building gypsum plaster meets the requirement of GB9776-1988 standard, and granularity is more than 120 orders; Presetting period is no earlier than 6min, ultimate compression strength: be greater than 3MPa; Folding strength: be greater than 2MPa, in building gypsum plaster, the content of CaSO42H2O is less than 1%.
10. the preparation method of the environment-friendly type inner wall putty paste described in claim 7～9 any one, it is characterized in that comprising the following steps: take 1/3 talcum powder and be placed in mixed stirring device, then according to the ascending auxiliary material that adds successively of weight percent, after premix is even, according to ascending remaining talcum powder and other the basic raw material of adding successively of weight percent, after mixing, stir after 10～15min again, add equably required water, stir discharging after 10～15min.
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