CN103525140B - A kind of Non-expansive fireproof paint - Google Patents
A kind of Non-expansive fireproof paint Download PDFInfo
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- CN103525140B CN103525140B CN201310419061.7A CN201310419061A CN103525140B CN 103525140 B CN103525140 B CN 103525140B CN 201310419061 A CN201310419061 A CN 201310419061A CN 103525140 B CN103525140 B CN 103525140B
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- fireproof paint
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- 239000003973 paint Substances 0.000 title claims abstract description 14
- 238000002360 preparation method Methods 0.000 claims abstract description 11
- 239000002994 raw material Substances 0.000 claims description 18
- 238000003756 stirring Methods 0.000 claims description 15
- 239000000853 adhesive Substances 0.000 claims description 12
- 230000001070 adhesive effect Effects 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims description 9
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 9
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 9
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 claims description 6
- 239000004354 Hydroxyethyl cellulose Substances 0.000 claims description 6
- RCEAADKTGXTDOA-UHFFFAOYSA-N OS(O)(=O)=O.CCCCCCCCCCCC[Na] Chemical compound OS(O)(=O)=O.CCCCCCCCCCCC[Na] RCEAADKTGXTDOA-UHFFFAOYSA-N 0.000 claims description 6
- 239000002202 Polyethylene glycol Substances 0.000 claims description 6
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 6
- 239000008367 deionised water Substances 0.000 claims description 6
- 229910021641 deionized water Inorganic materials 0.000 claims description 6
- JYIMWRSJCRRYNK-UHFFFAOYSA-N dialuminum;disodium;oxygen(2-);silicon(4+);hydrate Chemical compound O.[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Na+].[Na+].[Al+3].[Al+3].[Si+4] JYIMWRSJCRRYNK-UHFFFAOYSA-N 0.000 claims description 6
- 239000006185 dispersion Substances 0.000 claims description 6
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 claims description 6
- 238000002454 metastable transfer emission spectrometry Methods 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 229920000058 polyacrylate Polymers 0.000 claims description 6
- 229920001223 polyethylene glycol Polymers 0.000 claims description 6
- 229920002545 silicone oil Polymers 0.000 claims description 6
- CPUDPFPXCZDNGI-UHFFFAOYSA-N triethoxy(methyl)silane Chemical compound CCO[Si](C)(OCC)OCC CPUDPFPXCZDNGI-UHFFFAOYSA-N 0.000 claims description 6
- 229910002012 Aerosil® Inorganic materials 0.000 claims description 3
- 239000004642 Polyimide Substances 0.000 claims description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 3
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 3
- 229960000892 attapulgite Drugs 0.000 claims description 3
- 239000000839 emulsion Substances 0.000 claims description 3
- 238000001914 filtration Methods 0.000 claims description 3
- 239000010436 fluorite Substances 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- UEGPKNKPLBYCNK-UHFFFAOYSA-L magnesium acetate Chemical compound [Mg+2].CC([O-])=O.CC([O-])=O UEGPKNKPLBYCNK-UHFFFAOYSA-L 0.000 claims description 3
- 239000011654 magnesium acetate Substances 0.000 claims description 3
- 229940069446 magnesium acetate Drugs 0.000 claims description 3
- 235000011285 magnesium acetate Nutrition 0.000 claims description 3
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 claims description 3
- 239000000347 magnesium hydroxide Substances 0.000 claims description 3
- 229910001862 magnesium hydroxide Inorganic materials 0.000 claims description 3
- 229910052625 palygorskite Inorganic materials 0.000 claims description 3
- 229920001721 polyimide Polymers 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 3
- 230000000630 rising effect Effects 0.000 claims description 3
- 229910052710 silicon Inorganic materials 0.000 claims description 3
- 239000010703 silicon Substances 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
- 239000011248 coating agent Substances 0.000 abstract description 10
- 238000000576 coating method Methods 0.000 abstract description 10
- 230000000694 effects Effects 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 238000012546 transfer Methods 0.000 abstract description 2
- 238000000034 method Methods 0.000 description 2
- 230000001681 protective effect Effects 0.000 description 2
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 125000002534 ethynyl group Chemical group [H]C#C* 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- -1 foxiness Substances 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Paints Or Removers (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
The invention discloses a kind of Non-expansive fireproof paint, first and second liang of components that it is 2-3:1 by mass ratio form, coating preparation method of the present invention is simple, easy to operate, reduce production costs, component first and component second are packed respectively the operating period that can improve product, coating film heat-transfer effect of the present invention is good, film thermally equivalent, film temperature raises slowly, effectively plays smokeless fireproof effect.
Description
Technical field
The present invention relates generally to a kind of coating, relates in particular to a kind of Non-expansive fireproof paint.
Background technology
That coating should have is anticorrosion, waterproof, grease proofing, chemicals-resistant, fast light, heatproof etc., and object is exposed among atmosphere, is subject to the erosion of oxygen, moisture etc., causes the breakoff phenomenons such as corrosion of metal, foxiness, cement weathering. Be coated with coating at object surface, form layer protecting film, can stop or postpone generation and the development of these breakoff phenomenons, extended the service life of various materials. So protective effect is a Main Function of coating, improve the protective effect of traditional coating, could further improve the quality of coating.
Summary of the invention
The object of the invention is exactly for a kind of Non-expansive fireproof paint is provided.
The present invention is achieved by the following technical solutions:
A kind of Non-expansive fireproof paint, first and second liang of components that it is 2-3:1 by weight ratio form, and described first component is made up of the raw material of following weight parts:
Alumina sol 40-60, polyethylene glycol 10-16, silicon whisker 10-15, aerosil 1-2, nano-attapulgite 4-6, Fluorspar Powder 10-13, magnesium hydroxide 2-4, lauryl sodium sulfate 0.6-1, methyl-silicone oil 0.8-1, adhesive aid 10-14;
Described adhesive aid is made up of the raw material of following weight parts:
Benzene emulsion 60-70, bassora gum 6-8, ZPT 1-2, sodium silicoaluminate 4-6, butyl polyacrylate 1-2, hydroxyethylcellulose 2-4, BHT 0.1-0.3, water are appropriate;
The 10-20% of above-mentioned weight bassora gum is joined in 10-15 times of water, add hydroxyethylcellulose and BHT, dispersed with stirring 10-15 minute under the speed of 400-600 rev/min, rising temperature is 60-80 DEG C, add ZPT, sodium silicoaluminate, butyl polyacrylate, after fully mixing, add the each raw material of residue, after stirring, cross the Steam Heating of 80-100 DEG C, the system solid content of making is 60-65%, is cooled to normal temperature, obtains described adhesive aid;
Described component B is made up of the raw material of following weight parts:
MTES 40-60, alumina sol 10-20, ethylene glycol 4-6, polyimides 1-2, magnesium acetate 1-2, deionized water 10-30.
A preparation method for Non-expansive fireproof paint, comprises the following steps:
(1) preparation of first component:
Above-mentioned alumina sol, polyethylene glycol, lauryl sodium sulfate, methyl-silicone oil, adhesive aid are mixed, and 600-800 rev/min of dispersed with stirring 20-30 minute, adds the each raw material of residue, after fully mixing, grinds 1-2 hour, filters, and obtains first component;
(2) preparation of component B:
Above-mentioned MTES and deionized water are mixed to join in dispersion tank, and at 30-40 DEG C, 800-1000 rev/min of dispersed with stirring 10-15 minute, adds the each raw material of residue, filters, and obtains component B
(3) be that 2-3:1 is mixed to join in airtight dispersion tank by first and second liang of components according to weight ratio, at room temperature, stir lower slaking 10-100 hour with the speed of 600-800r/min, after filtration, make Non-expansive fireproof paint.
Advantage of the present invention is:
Coating preparation method of the present invention is simple, easy to operate, reduces production costs, component first and component second are packed respectively the operating period that can improve product, and coating film heat-transfer effect of the present invention is good, film thermally equivalent, film temperature raises slowly, effectively plays smokeless fireproof effect.
Detailed description of the invention
Embodiment 1
A kind of Non-expansive fireproof paint, first and second liang of components that it is 2:1 by weight ratio form, and described first component is made up of the raw material of following weight parts:
Alumina sol 60, polyethylene glycol 16, silicon whisker 15, aerosil 2, nano-attapulgite 4, Fluorspar Powder 13, magnesium hydroxide 4, lauryl sodium sulfate 0.6, methyl-silicone oil 1, adhesive aid 14;
Described adhesive aid is made up of the raw material of following weight parts:
Benzene emulsion 70, bassora gum 8, ZPT 2, sodium silicoaluminate 4, butyl polyacrylate 1, hydroxyethylcellulose 2, BHT 0.3, water are appropriate;
Join in 15 times of water 20% of above-mentioned weight bassora gum, add hydroxyethylcellulose and BHT, dispersed with stirring 15 minutes under the speed of 600 revs/min, rising temperature is 80 DEG C, add ZPT, sodium silicoaluminate, butyl polyacrylate, after fully mixing, add the each raw material of residue, after stirring, cross the Steam Heating of 100 DEG C, the system solid content of making is 65%, is cooled to normal temperature, obtains described adhesive aid;
Described component B is made up of the raw material of following weight parts:
MTES 60, alumina sol 20, ethylene glycol 6, polyimides 1, magnesium acetate 1, deionized water 30.
A preparation method for Non-expansive fireproof paint, comprises the following steps:
(1) preparation of first component:
Above-mentioned alumina sol, polyethylene glycol, lauryl sodium sulfate, methyl-silicone oil, adhesive aid are mixed, and 800 revs/min of dispersed with stirring 30 minutes, add the each raw material of residue, after fully mixing, grind 1 hour, filter, and obtain first component;
(2) preparation of component B:
Above-mentioned MTES and deionized water are mixed to join in dispersion tank, and at 40 DEG C, 1000 revs/min of dispersed with stirring 1 minute, add the each raw material of residue, filter, and obtain component B
(3) be that 2:1 is mixed to join in airtight dispersion tank by first and second liang of components according to weight ratio, at room temperature, stir lower slaking 60 hours with the speed of 800r/min, after filtration, make Non-expansive fireproof paint.
Performance test:
Red hardness: (Mitsubishi's pencil hardness method) 5H;
Chill degree: (Mitsubishi's pencil hardness method) 5H;
Firing resistance: (acetylene flame burning aluminium sheet) do not fire, smokelessly.
Claims (2)
1. a Non-expansive fireproof paint, is characterized in that first and second liang of components that it is 2-3:1 by weight ratio form, and described first component is made up of the raw material of following weight parts:
Alumina sol 40-60, polyethylene glycol 10-16, silicon whisker 10-15, aerosil 1-2, nano-attapulgite 4-6, Fluorspar Powder 10-13, magnesium hydroxide 2-4, lauryl sodium sulfate 0.6-1, methyl-silicone oil 0.8-1, adhesive aid 10-14;
Described adhesive aid is made up of the raw material of following weight parts:
Benzene emulsion 60-70, bassora gum 6-8, ZPT 1-2, sodium silicoaluminate 4-6, butyl polyacrylate 1-2, hydroxyethylcellulose 2-4, BHT 0.1-0.3, water are appropriate;
The 10-20% of above-mentioned weight bassora gum is joined in 10-15 times of water, add hydroxyethylcellulose and BHT, dispersed with stirring 10-15 minute under the speed of 400-600 rev/min, rising temperature is 60-80 DEG C, add ZPT, sodium silicoaluminate, butyl polyacrylate, after fully mixing, add the each raw material of residue, after stirring, cross the Steam Heating of 80-100 DEG C, the system solid content of making is 60-65%, is cooled to normal temperature, obtains described adhesive aid;
Described component B is made up of the raw material of following weight parts:
MTES 40-60, alumina sol 10-20, ethylene glycol 4-6, polyimides 1-2, magnesium acetate 1-2, deionized water 10-30.
2. a preparation method for Non-expansive fireproof paint as claimed in claim 1, is characterized in that comprising the following steps:
(1) preparation of first component:
Above-mentioned alumina sol, polyethylene glycol, lauryl sodium sulfate, methyl-silicone oil, adhesive aid are mixed, and 600-800 rev/min of dispersed with stirring 20-30 minute, adds the each raw material of residue, after fully mixing, grinds 1-2 hour, filters, and obtains first component;
(2) preparation of component B:
Above-mentioned MTES and deionized water are mixed to join in dispersion tank, and at 30-40 DEG C, 800-1000 rev/min of dispersed with stirring 10-15 minute, adds the each raw material of residue, filters, and obtains component B
(3) be that 2-3:1 is mixed to join in airtight dispersion tank by first and second liang of components according to weight ratio, at room temperature, stir lower slaking 10-100 hour with the speed of 600-800r/min, after filtration, make Non-expansive fireproof paint.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310419061.7A CN103525140B (en) | 2013-09-13 | 2013-09-13 | A kind of Non-expansive fireproof paint |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310419061.7A CN103525140B (en) | 2013-09-13 | 2013-09-13 | A kind of Non-expansive fireproof paint |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103525140A CN103525140A (en) | 2014-01-22 |
| CN103525140B true CN103525140B (en) | 2016-05-25 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201310419061.7A Active CN103525140B (en) | 2013-09-13 | 2013-09-13 | A kind of Non-expansive fireproof paint |
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| CN (1) | CN103525140B (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104031460B (en) * | 2014-06-27 | 2015-07-22 | 威远县大禾陶瓷原料有限公司 | Inorganic filler material for transparent lacquer and preparation method thereof |
| CN104292951A (en) * | 2014-09-26 | 2015-01-21 | 锐展(铜陵)科技有限公司 | Special filler for durable high-hardness automobile paints and preparation method thereof |
| CN104312252A (en) * | 2014-09-26 | 2015-01-28 | 锐展(铜陵)科技有限公司 | High-airtightness filler for automobile coating and preparation method thereof |
| CN104893572A (en) * | 2015-05-29 | 2015-09-09 | 苏州德翔装饰工程有限公司 | Fire-retardant coating for interior wall decoration veneer board and preparation method of fire-retardant coating |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102173667A (en) * | 2011-01-25 | 2011-09-07 | 常州工程职业技术学院 | Non-intumescent fireproofing coating and preparation method thereof |
| CN102815887A (en) * | 2012-08-10 | 2012-12-12 | 三棵树涂料股份有限公司 | Lightweight sound-absorbing environment-friendly interior wall paint |
-
2013
- 2013-09-13 CN CN201310419061.7A patent/CN103525140B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102173667A (en) * | 2011-01-25 | 2011-09-07 | 常州工程职业技术学院 | Non-intumescent fireproofing coating and preparation method thereof |
| CN102815887A (en) * | 2012-08-10 | 2012-12-12 | 三棵树涂料股份有限公司 | Lightweight sound-absorbing environment-friendly interior wall paint |
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| CN103525140A (en) | 2014-01-22 |
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Effective date of registration: 20190520 Address after: 071300 Xiaodian Village North, Xiaodian Town, Boye County, Baoding City, Hebei Province Patentee after: Ruian Tiandi (Boye) Fireproof Material Manufacturing Co., Ltd. Address before: 236000 Wenfeng Road Fengyu District, Yingquan District, Fuyang City, Anhui Province Patentee before: Ren Zhenzhou |