CN103498340B - A kind of cotton spinning wool spinning cold slurry agent for chemical fibre - Google Patents
A kind of cotton spinning wool spinning cold slurry agent for chemical fibre Download PDFInfo
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- CN103498340B CN103498340B CN201310485598.3A CN201310485598A CN103498340B CN 103498340 B CN103498340 B CN 103498340B CN 201310485598 A CN201310485598 A CN 201310485598A CN 103498340 B CN103498340 B CN 103498340B
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- 238000009987 spinning Methods 0.000 title claims abstract description 61
- 210000002268 wool Anatomy 0.000 title claims abstract description 55
- 239000002002 slurry Substances 0.000 title claims abstract description 47
- 239000000835 fiber Substances 0.000 title claims abstract description 39
- 239000003795 chemical substances by application Substances 0.000 title claims abstract description 36
- 229920000742 Cotton Polymers 0.000 title claims abstract description 31
- 239000000126 substance Substances 0.000 title claims abstract description 30
- BAPJBEWLBFYGME-UHFFFAOYSA-N Methyl acrylate Chemical compound COC(=O)C=C BAPJBEWLBFYGME-UHFFFAOYSA-N 0.000 claims abstract description 33
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 26
- 239000000203 mixture Substances 0.000 claims abstract description 16
- ROOXNKNUYICQNP-UHFFFAOYSA-N ammonium persulfate Chemical compound [NH4+].[NH4+].[O-]S(=O)(=O)OOS([O-])(=O)=O ROOXNKNUYICQNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 235000014113 dietary fatty acids Nutrition 0.000 claims abstract description 14
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 claims abstract description 14
- 229940043237 diethanolamine Drugs 0.000 claims abstract description 14
- 229930195729 fatty acid Natural products 0.000 claims abstract description 14
- 239000000194 fatty acid Substances 0.000 claims abstract description 14
- 150000004665 fatty acids Chemical class 0.000 claims abstract description 14
- 235000013162 Cocos nucifera Nutrition 0.000 claims abstract description 13
- 244000060011 Cocos nucifera Species 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims abstract description 11
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 11
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 claims abstract description 10
- USHAGKDGDHPEEY-UHFFFAOYSA-L potassium persulfate Chemical compound [K+].[K+].[O-]S(=O)(=O)OOS([O-])(=O)=O USHAGKDGDHPEEY-UHFFFAOYSA-L 0.000 claims abstract description 10
- 235000019394 potassium persulphate Nutrition 0.000 claims abstract description 10
- 229910001870 ammonium persulfate Inorganic materials 0.000 claims abstract description 7
- 238000010792 warming Methods 0.000 claims abstract description 6
- 239000004744 fabric Substances 0.000 claims description 28
- 239000000047 product Substances 0.000 claims description 9
- 150000001408 amides Chemical class 0.000 claims description 8
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 5
- 229960003511 macrogol Drugs 0.000 claims description 5
- 239000003240 coconut oil Substances 0.000 claims description 4
- 235000019864 coconut oil Nutrition 0.000 claims description 4
- 239000007859 condensation product Substances 0.000 claims description 4
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 claims description 3
- -1 alkyl phenol Chemical compound 0.000 claims description 3
- 239000004359 castor oil Substances 0.000 claims description 2
- 235000019438 castor oil Nutrition 0.000 claims description 2
- 150000001875 compounds Chemical class 0.000 claims description 2
- 238000009833 condensation Methods 0.000 claims description 2
- 230000005494 condensation Effects 0.000 claims description 2
- 150000002191 fatty alcohols Chemical class 0.000 claims description 2
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims description 2
- 239000007788 liquid Substances 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims description 2
- QYKIQEUNHZKYBP-UHFFFAOYSA-N Vinyl ether Chemical compound C=COC=C QYKIQEUNHZKYBP-UHFFFAOYSA-N 0.000 claims 1
- 125000000217 alkyl group Chemical group 0.000 claims 1
- 230000001804 emulsifying effect Effects 0.000 claims 1
- 238000000034 method Methods 0.000 abstract description 15
- 238000009941 weaving Methods 0.000 abstract description 15
- 239000008118 PEG 6000 Substances 0.000 abstract description 5
- 229920002584 Polyethylene Glycol 6000 Polymers 0.000 abstract description 5
- 230000008595 infiltration Effects 0.000 abstract description 4
- 238000001764 infiltration Methods 0.000 abstract description 4
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 230000009187 flying Effects 0.000 abstract description 2
- BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 abstract description 2
- 238000004513 sizing Methods 0.000 description 14
- 238000009955 starching Methods 0.000 description 9
- 235000014676 Phragmites communis Nutrition 0.000 description 7
- 238000005516 engineering process Methods 0.000 description 4
- 239000003981 vehicle Substances 0.000 description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 150000001412 amines Chemical class 0.000 description 2
- 230000009245 menopause Effects 0.000 description 2
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 description 1
- 125000000129 anionic group Chemical group 0.000 description 1
- 238000010009 beating Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000010779 crude oil Substances 0.000 description 1
- 238000009990 desizing Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 230000009191 jumping Effects 0.000 description 1
- 150000002605 large molecules Chemical class 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
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- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention provides a kind of cold slurry agent for cotton spinning wool spinning chemical fibre, comprise emulsifying agent TX-40, Emulsifier EL-40, AEO, cocoanut fatty acid diethanolamide, PEG-6000, methyl acrylate, acrylic acid, acrylamide, ammonium persulfate, potassium peroxydisulfate, water and diethanol amine; By emulsifying agent TX-40 and EL-40, AEO, cocoanut fatty acid diethanolamide, PEG-6000, methyl acrylate, acrylic acid, acrylamide and water mix and blend, be warming up to 65 DEG C, keep 3 hours, then cool to 30 DEG C, the target product that adds diethanol amine to regulate pH value to 6～7 to obtain. Product of the present invention has excellent infiltration and antistatic property, be not only applicable to cotton spinning and chemical fibre, also be applicable to pure wool and wool blend yarn, improve the weaving performance of fine yarn, reduce flyings, adhesion and skips in weaving process, improve the brute force of single thread and undertwisted yarn, product is easy to use, containing APEO, not phosphorous, environmental protection, easily wash and move back after weaving end.
Description
Technical field
The present invention relates to a kind of textile warp starching slurry, relate in particular to one and be applicable on pure wool and wool blend yarnThe efficient cool slashing sizes such as the cotton spinning wool spinning chemical fibre of slurry.
Background technology
Warp thread is as forming the part of shed open, in woven process, due to warp thread and heald, reed, menopause tabletThe friction repeatedly of parts such as (in the processes of warping, the friction between warp thread and tensioner, lease reed, grade bars), Yi JiIn harness motion, under the effect of beating motion, bear continuous stretching, impact and complications, the fiber on warp thread is very easily ground and is sent outHair, mutually assembles, tangles, and causes shed open unclear, causes that warp end break and float increase, and the object of warp thread being carried out to starching is exactlyIn order to reduce filoplume, improve the weavability of wool yarn.
Along with the development of the use industries such as cotton spinning wool spinning chemical fibre, the extensive use of new technology, new material, new technology, spinningThe upgrading of velvet fabric is constantly accelerated, and tending to become strong demand day of frivolous, strong twisted yarn, institutional framework diversification fabric propped up to height in marketStrong, the cycle of the quality to kind, production also has higher requirement simultaneously. This just makes long-term puzzlement weave grey quality to carryHigh wool yarn is scared, the static that returns sth. made by twisting, inverse ratio kind of strong twisted yarn etc. becomes problem in the urgent need to address. At warping apparatusIt is to improve yarn quality that upper introducing quetsch carries out starching to warp thread, and the one of clear opening raising wool yarn weavability is importantApproach. Be different from general cotton yarn starching because the distinctive physicochemical property of wool fiber itself has determined wool sizing, it existsFollowing problem: 1) wool surface has scale and wool containing grease, add in spinning, apply cause wool with crude oil etc.Wetability is poor, thereby has reduced the affinity between high polymer and wool fibre large molecule in slurries, easily causes infiltration not enough, serous coatThe phenomenon such as come off; 2) extension at break of wool yarn is generally all larger, wool fibre good springiness, but serous coat extension at break is little, yarn after starchingThread breakage extends and is less than raw yarn; 3) relatively the elasticity of common and braid wool fiber itself is large for wool fiber fiber number, the filoplume on wool yarn surfaceIn the time of starching, be difficult for submissive; 4) wool belongs to natural protein fibre, more responsive to high temperature, alkali and strong mechanism, because ofThis should not adopt the starching mode of the long-time digestion of high temperature, powerful roll compacting in the time of starching; 5) meeting as bad in fabric desizing causes and knitsThing plate is hard and nonelastic, makes wool fabric lose original style. Therefore wool sizing palpus solution wool yarn wetability, filoplume paste and lie prostrate,The problems such as low temperature starching and easily destarch.
Summary of the invention
The object of the present invention is to provide a kind of cotton spinning wool spinning chemical fibre with excellent infiltration and antistatic property with highImitate cold slurry agent.
For solving the problems of the technologies described above, the present invention adopts following technical scheme to realize:
A kind of cotton spinning wool spinning cold slurry agent for chemical fibre, it comprises emulsifying agent TX-40, Emulsifier EL-40, aliphatic alcohol polyethenoxyEther, cocoanut fatty acid diethanolamide, PEG-6000, methyl acrylate, water and diethanol amine, according to weight portion meter, described inEach component content is:
Emulsifying agent TX-4075～85 weight portion
Emulsifier EL-40 75～85 weight portions
AEO 45～55 weight portions
Cocoanut fatty acid diethanolamide 90～100 weight portions
PEG-600040～50 weight portion
Methyl acrylate 115～125 weight portions
Acrylic acid 100～105 weight portions
Acrylamide 40～50 weight portions
Ammonium persulfate 0.1～0.2 weight portion
Potassium peroxydisulfate 0.1～0.2 weight portion
Water 500～520 weight portions
Diethanol amine 15～25 weight portions
Cotton spinning wool spinning chemical fibre of the present invention by the preferred proportioning of efficient cool slurry agent is:
Emulsifying agent TX-4080 weight portion
Emulsifier EL-40 80 weight portions
AEO 50 weight portions
Cocoanut fatty acid diethanolamide 95 weight portions
PEG-600045 weight portion
Methyl acrylate 120 weight portions
Acrylic acid 102 weight portions
Acrylamide 45 weight portions
Ammonium persulfate 0.15 weight portion
Potassium peroxydisulfate 0.15 weight portion
Water 510 weight portions
Diethanol amine 20 weight portions
Described emulsifying agent TX-40 is condensation compound of alkyl phenol and epoxy ethane.
Described Emulsifier EL-40 is castor oil/rilanit special and ethylene oxide condensate.
Described AEO is fatty alcohol and APEO condensation product.
Described cocoanut fatty acid diethanolamide is coco-nut oil fatty acid and diglycollic amide condensation product.
Described PEG-6000 is Macrogol 6000 monoleate.
Described methyl acrylate is 95% technical grade methyl acrylate.
Described diethanol amine is 98% technical grade diethanol amine.
The present invention also provides the preparation method of the cold slurry agent of a kind of cotton spinning wool spinning chemical fibre: by emulsifying agent TX-40 and EL-40, AEO, cocoanut fatty acid diethanolamide, PEG-6000, methyl acrylate, acrylamide, propyleneAcid, ammonium persulfate, potassium peroxydisulfate and water mix and blend, be warming up to 65 DEG C, keeps 3 hours, then cools to 30 DEG C, adds diethylHydramine regulates pH value to 6～7, obtains target product.
Described cotton spinning wool spinning chemical fibre with cold slurry agent be micro-Huang to yellow transparent thick liquid, be nonionic or anionic property,PH value is that under 6～8,25 DEG C of conditions, viscosity is 110 ± 30mps.s, and its consumption is fabric weight 4～12%.
Beneficial effect of the present invention: cold slurry agent of the present invention has excellent infiltration and antistatic property, is not only applicable toCotton spinning and chemical fibre, and be applicable to pure wool and wool blend yarn, can improve the weaving performance of fine yarn, comprise crape and bobbinDyed yarn, product, containing APEO, not phosphorous, environmental protection, is not embodied in following premium properties:
(1) starching amount be fabric heavy 4%～12% time, can effectively improve tradition spinning bifilar wool yarn weaving performance,Also can improve weaving performance for crape etc.
(2) can reduce the generation of the flyings in weaving process, reduce the pollution of fabric, extend the cleaning cycle of loom.
(3) improve single thread and the low brute force of picking up yarn, make yarn more easily by menopause tablet, heald and reed, adhesion and skipsCan obviously reduce.
(4) design of this product is used for directly using without dilution.
(5) weave after end, this product, under 40 DEG C of alkali conditions, is very easily water-washed away in rinsing bowl.
Detailed description of the invention
More cheer and bright in order to be object of the present invention, technical scheme and advantage, the following specific embodiment of the present inventionTechnical scheme of the present invention is described further, but the invention is not restricted to following specific embodiment.
Embodiment 1: cotton spinning wool spinning chemical fibre is prepared with cold slurry agent
By 8kg emulsifying agent TX-40,8kg Emulsifier EL-40,5kg AEO, 9.5kg coco-nut oil fatty acidDiglycollic amide, 4.5kgPEG-6000,12kg methyl acrylate and 10.2kg acrylamide, 4.5kg acrylic acid, 15g over cureAcid ammonium, 15g potassium peroxydisulfate and 51kg water mix and blend, be warming up to 65 DEG C, keeps 3 hours, then cools to 30 DEG C, adds 2kgDiethanol amine regulates pH value to 6～7, obtains target product.
Embodiment 2: cotton spinning wool spinning chemical fibre is prepared with cold slurry agent
By 7.5kg emulsifying agent TX-40,7.5kg Emulsifier EL-40,4.5kg AEO, 9kg coconut greaseFat acid diglycollic amide, 4kgPEG-6000,11.5kg methyl acrylate and 10kg acrylamide, 4kg acrylic acid, 10g persulfuric acidAmmonium, 10g potassium peroxydisulfate and 50kg water mix and blend, be warming up to 65 DEG C, keeps 3 hours, then cools to 30 DEG C, adds 1.5kgDiethanol amine regulates pH value to 6～7, obtains target product.
Embodiment 3: cotton spinning wool spinning chemical fibre is prepared with cold slurry agent
By 8.5kg emulsifying agent TX-40,8.5g Emulsifier EL-40,5.5kg AEO, 10kg coconut greaseFat acid diglycollic amide, 5kgPEG-6000,12.5kg methyl acrylate and 10.5kg acrylamide, 5kg acrylic acid, 20g over cureAcid ammonium, 20g potassium peroxydisulfate and 52kg water mix and blend, be warming up to 65 DEG C, keeps 3 hours, then cools to 30 DEG C, adds2.5kg diethanol amine regulates pH value to 6～7, obtains target product.
Embodiment 4: the cotton spinning wool spinning chemical fibre of embodiment 1 is washed to wool fabric with cold slurry agent for inverse ratio
In mao fancy suiting warping process, use cold slurry agent for cotton spinning wool spinning chemical fibre of the present invention washing.
The specification of fabric: upper machine reed width 169.2cm
Weft density: through close: 27.6/cm, filling density: 27.5/cm
Yarn count: 66s/2 × 38s/1
Holoaxial length: 1050m
Fabric tissue: 2/2 ↗
On THEMA-11EXCEL rapier loom, weave, the speed of a motor vehicle is 380rpm.
Slurry roller by quetsch in sectional warper beaming process imposes on cold slurry on warp thread, and warp sizing amount is8.8%。
The quality of weaving the cold slurry agent of front upper sizing and not going up the grey cloth of the cold slurry agent of warp thread sees the following form.
As can be known from the above table, by warp sizing, the thin skips in mao fancy suiting weaving process, little bow yarn have effectively been suppressed to washDeng the generation of some float, the running efficiency of First Grade Percentage Before Cloth Repairing, loom has obtained certain raising.
Embodiment 5: the cotton spinning wool spinning chemical fibre of embodiment 2 is used for to double ends list weft fabric with cold slurry agent
In the warping process of all woolen back satin serge, use cold slurry agent for cotton spinning wool spinning chemical fibre of the present invention.
The specification of fabric: upper machine reed width 167.9cm
Weft density: through close: 49.6/cm, filling density: 39.4/cm
Yarn count: 80s/2 × 48s/1
Holoaxial length: 1470m
Fabric tissue: 22/25 ↗
On THEMA-11EXCEL rapier loom, weave, the speed of a motor vehicle is 380rpm.
Slurry roller by quetsch in sectional warper beaming process imposes on cold slurry on warp thread, and warp sizing amount is9.3%。
The quality of weaving the cold slurry agent of front upper sizing and not going up the grey cloth of the cold slurry agent of warp thread sees the following form.
As can be known from the above table, by warp sizing, thin skips in all woolen back satin serge weaving process, little have effectively been suppressedThe generation of some float such as bow yarn, the running efficiency of First Grade Percentage Before Cloth Repairing, loom has obtained certain raising.
Embodiment 6: the cotton spinning wool spinning chemical fibre of embodiment 3 is used for to single-warp single-abb fabric with cold slurry agent
In the warping process of all woolen fancy suiting, use cold slurry agent for cotton spinning wool spinning chemical fibre of the present invention.
The specification of fabric: upper machine reed width 177.4cm
Weft density: through close: 33.2/cm, filling density: 22.4/cm
Yarn count: 30s/1 × 30s/1
Holoaxial length: 1014m
Fabric tissue: 33/13 ↗
On THEMA-11EXCEL rapier loom, weave, the speed of a motor vehicle is 380rpm.
Slurry roller by quetsch in sectional warper beaming process imposes on cold slurry on warp thread, and warp sizing amount is12.4%。
The quality of weaving the cold slurry agent of front upper sizing and not going up the grey cloth of the cold slurry agent of warp thread sees the following form.
As can be known from the above table, by warp sizing, effectively suppressed the thin jumping in single-warp single-abb all woolen fancy suiting weaving processThe generation of some float such as colored, little bow yarn, the running efficiency of First Grade Percentage Before Cloth Repairing, loom has obtained certain raising.
Embodiment 7: the cotton spinning wool spinning chemical fibre of embodiment 1 is used for matching network yarn fabric with cold slurry agent
In the warping process of all woolen fancy suiting, use cold slurry agent for cotton spinning wool spinning chemical fibre of the present invention.
The specification of fabric: upper machine reed width 184.5cm
Weft density: through close: 16.06/cm, filling density: 15.8/cm
Yarn count: 66s/2,66s/4 × 66s/2,66s/4
Holoaxial length: 900m
Fabric tissue: 1/1 ↗
On THEMA-11EXCEL rapier loom, weave, the speed of a motor vehicle is 380rpm.
Slurry roller by quetsch in sectional warper beaming process imposes on cold slurry on warp thread, and warp sizing amount is7.9%。
The quality of weaving the cold slurry agent of front upper sizing and not going up the grey cloth of the cold slurry agent of warp thread sees the following form.
As can be known from the above table, by warp sizing, effectively suppressed match network spin thin skips in all woolen fancy suiting weaving process,The generation of some float such as little bow yarn, the running efficiency of First Grade Percentage Before Cloth Repairing, loom has obtained certain raising.
The present invention can use without prejudice to the concrete form of spirit of the present invention or principal character and summarize, and above-mentioned embodiment onlyIn order to technical scheme of the present invention to be described but not design of the present invention and protection domain are limited to ordinary skill of the present inventionPersonnel modify to technical scheme of the present invention or are equal to replacement, and do not depart from aim and the scope of technical scheme, and it is equalShould be encompassed in claim scope of the present invention.
Claims (5)
1. a cold slurry agent for cotton spinning wool spinning chemical fibre, is characterized in that: comprise emulsifying agent TX-40, Emulsifier EL-40, fatty alcoholAPEO, cocoanut fatty acid diethanolamide, Macrogol 6000 monoleate, methyl acrylate, acrylic acid, propyleneAcid amides, ammonium persulfate, potassium peroxydisulfate, water and diethanol amine, according to weight portion meter, the content of described each composition is:
Emulsifying agent TX-4075～85 weight portion
Emulsifier EL-40 75～85 weight portions
AEO 45～55 weight portions
Cocoanut fatty acid diethanolamide 90～100 weight portions
Macrogol 6000 monoleate 40～50 weight portions
Methyl acrylate 115～125 weight portions
Acrylic acid 100～105 weight portions
Acrylamide 40～50 weight portions
Ammonium persulfate 0.1～0.2 weight portion
Potassium peroxydisulfate 0.1～0.2 weight portion
Water 500～520 weight portions
Diethanol amine 15～25 weight portions
Described a kind of cotton spinning wool spinning chemical fibre by the preparation method of cold slurry agent is: by emulsifying agent TX-40 and EL-40, poly alkyl alcoholOxygen vinethene, cocoanut fatty acid diethanolamide, Macrogol 6000 monoleate, methyl acrylate, acrylic acid, propyleneAcid amides and water mix and blend, be warming up to 65 DEG C, keeps 3 hours, then cools to 30 DEG C, adds diethanol amine to regulate pH value to 6～7, obtain target product; Described cotton spinning wool spinning chemical fibre with cold slurry agent be micro-Huang to yellow transparent thick liquid, be nonionic orAnionic property, pH value is that under 6～8,25 DEG C of conditions, viscosity is 110 ± 30mPas.
2. a kind of cold slurry agent for cotton spinning wool spinning chemical fibre according to claim 1, is characterized in that: the content of described each compositionFor:
Emulsifying agent TX-4080 weight portion
Emulsifier EL-40 80 weight portions
AEO 50 weight portions
Cocoanut fatty acid diethanolamide 95 weight portions
Macrogol 6000 monoleate 45 weight portions
Methyl acrylate 120 weight portions
Acrylic acid 102 weight portions
Acrylamide 45 weight portions
Ammonium persulfate 0.15 weight portion
Potassium peroxydisulfate 0.15 weight portion
Water 510 weight portions
Diethanol amine 20 weight portions.
3. a kind of cold slurry agent for cotton spinning wool spinning chemical fibre according to claim 1 and 2, is characterized in that: described emulsifying agentTX-40 is condensation compound of alkyl phenol and epoxy ethane, and described Emulsifier EL-40 is castor oil/rilanit special and oxiraneCondensation product, described AEO is fatty alcohol and APEO condensation product, described coco-nut oil fatty acid twoGlycollic amide is coco-nut oil fatty acid and diglycollic amide condensation product.
4. a kind of cold slurry agent for cotton spinning wool spinning chemical fibre according to claim 1 and 2, is characterized in that: described acrylic acidMethyl esters is 95% technical grade methyl acrylate, the technical grade diethanol amine that described diethanol amine is 98%.
5. a kind of cold slurry agent for cotton spinning wool spinning chemical fibre according to claim 1 and 2, is characterized in that: described cotton spinning wool spinningChemical fibre is fabric weight with the consumption of cold slurry agent 4～12%.
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| CN201310485598.3A CN103498340B (en) | 2013-10-17 | 2013-10-17 | A kind of cotton spinning wool spinning cold slurry agent for chemical fibre |
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| CN108486889B (en) * | 2015-11-01 | 2020-11-27 | 杭州富阳何氏化纤助剂有限公司 | Preparation method of sizing agent for sizing poplin compact fabric |
| CN106381706A (en) * | 2016-08-31 | 2017-02-08 | 常熟市裕茗企业管理咨询有限公司 | Pure cotton fabric yarn sizing process |
| CN107626254B (en) * | 2017-09-26 | 2018-07-10 | 江苏宇道生物科技有限公司 | A kind of textile auxiliary's production control system |
| CN111648135A (en) * | 2020-04-13 | 2020-09-11 | 威海诺葳信和新材料有限公司 | High-efficiency cold paste containing polysiloxane acrylate and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005105042A (en) * | 2003-09-29 | 2005-04-21 | Dainippon Ink & Chem Inc | Textile size composition and thread adhered therewith |
| CN1730807A (en) * | 2005-08-24 | 2006-02-08 | 西北大学 | Antibacterial fabric finishing agent and its preparation method |
| CN102400379A (en) * | 2010-09-14 | 2012-04-04 | 曹平 | Wrap dressing agent |
| CN102532399A (en) * | 2011-12-10 | 2012-07-04 | 江阴市尼美达助剂有限公司 | Acrylic acid textile size and preparation method thereof |
-
2013
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005105042A (en) * | 2003-09-29 | 2005-04-21 | Dainippon Ink & Chem Inc | Textile size composition and thread adhered therewith |
| CN1730807A (en) * | 2005-08-24 | 2006-02-08 | 西北大学 | Antibacterial fabric finishing agent and its preparation method |
| CN102400379A (en) * | 2010-09-14 | 2012-04-04 | 曹平 | Wrap dressing agent |
| CN102532399A (en) * | 2011-12-10 | 2012-07-04 | 江阴市尼美达助剂有限公司 | Acrylic acid textile size and preparation method thereof |
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| CN103498340A (en) | 2014-01-08 |
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Address after: 226500 Jiangsu city of Nantong province Rugao City Bai Pu Zhen Lin Zi guide Committee 12 Group No. 8 Patentee after: RUGAO XILIN CHEMICAL Co.,Ltd. Address before: 226500 Jiangsu city of Nantong province Rugao City Bai Pu Zhen Lin Zi No. 8 neighborhood 12 groups Patentee before: Rugao Xilin chemical plant Address after: 226500 Jiangsu city of Nantong province Rugao City Bai Pu Zhen Lin Zi No. 8 neighborhood 12 groups Patentee after: Rugao Xilin chemical plant Address before: 226500 Jiangsu city of Nantong province Rugao City Hayashi 12 neighborhood No. 8 Patentee before: Rugao City Linzi Town Xilin Chemical Plant |
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