CN103483915B - Preparation method of pigment yellow 17 emulsion - Google Patents
Preparation method of pigment yellow 17 emulsion Download PDFInfo
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- CN103483915B CN103483915B CN201310411001.0A CN201310411001A CN103483915B CN 103483915 B CN103483915 B CN 103483915B CN 201310411001 A CN201310411001 A CN 201310411001A CN 103483915 B CN103483915 B CN 103483915B
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Abstract
The invention relates to a preparation method of a pigment yellow 17 emulsion. The preparation method comprises the steps of (1) putting 10-12 parts of pigment yellow 17 powder of which the mesh number is 400-500 meshes into a container; (2) adding 5-9 parts of caprylic capric triglyceride into the container, and uniformly mixing pigment yellow 17 with caprylic capric triglyceride to obtain a mixture A; (3) adding 20-24 parts of rosin-polythylene oxide ester, 18-25 parts of petroleum sodium sulfonate and 160-170 parts of water into another container, and uniformly mixing to obtain liquid B; (4) mixing the mixture A with the liquid B, and shearing for 10-20 minutes by using a shearing machine at a rotating speed of 6000-8000rpm; (5) preserving after shearing. The particle size of the pigment yellow 17 emulsion prepared by the preparation method disclosed by the invention is 10-16 mum, and the application space of the pigment yellow 17 is expanded.
Description
Technical field
The present invention relates to a kind of preparation method of emulsion, particularly relate to a kind of preparation method of pigment yellow 17 emulsion.
Background technology
Pigment yellow 17 is a kind of azo pigment, has water-fast feature.Because it is water insoluble, under some aqueous systems, purposes and the space of pigment yellow 17 will be constrained.In order to expand the Application Areas of pigment yellow 17, a lot of people to attempt pigment yellow 17, as microemulsion or emulsion, being become not having of microemulsion at present, because its structure decides to do, to become microemulsion difficulty larger.As emulsion, current research is also less, and the effect obtained is very not remarkable, still there is a lot of shortcomings, constrains its large-scale application.
Summary of the invention
The technical problem solved: yellow 17 emulsion particle diameters of convention pigment are large, the problem of poor stability.
Technical scheme: the preparation method that the invention discloses a kind of pigment yellow 17 emulsion, preparation method comprises the following steps: (1) gets order number be 400 ~ 500 object pigment yellow 17 powder is 10 ~ 12 parts, and pigment yellow 17 is put into container; (2) in container, adding Glycerin, mixed triester with caprylic acid capric acid is 5 ~ 9 parts, is mixed by pigment yellow 17 with Glycerin, mixed triester with caprylic acid capric acid, is A mixture; (3) separately get a container, in container, add polyoxylethylene abietate is 20 ~ 24 parts, then to add petroleum sodium sulfonate be 18 ~ 25 parts, then adds water and be 160 to 170 parts, mixes as B liquid; (4) mixed with B liquid by A mixture, use shears to shear 10 ~ 20min, rotating speed is 6000rpm to 8000rpm; (5) shearing terminates rear preservation.Pigment yellow 17 powder order number is preferably 500 orders.Pigment yellow 17 powder is preferably 12 parts
.glycerin, mixed triester with caprylic acid capric acid is preferably 5 parts.Shears shear time is preferably 20min.
Beneficial effect: it is very little that this preparation method prepares pigment yellow 17 emulsion particle diameter is 10um ~ 16um.There is good thermal stability and dewatering ability simultaneously.Emulsion heats 5 ~ 10h and demixing phenomenon does not occur at 50 DEG C.Under rotating speed is 4000rpm, centrifugal 30min ~ 60min does not have layering and demulsifying phenomenon to produce yet in addition.
Embodiment
Embodiment 1
(1) to get order number be 400 object pigment yellow 17 powder is 10kg, and pigment yellow 17 is put into container; (2) in container, adding Glycerin, mixed triester with caprylic acid capric acid is 9kg, is mixed by pigment yellow 17 with Glycerin, mixed triester with caprylic acid capric acid, is A mixture; (3) separately get a container, in container, add polyoxylethylene abietate is 24kg, then to add petroleum sodium sulfonate be 25kg, then to add water be 160kg, mixes as B liquid; (4) mixed with B liquid by A mixture, use shears to shear 10min, rotating speed is 6000rpm; (5) shearing terminates rear preservation.
Embodiment 2
(1) to get order number be 500 object pigment yellow 17 powder is 11kg, and pigment yellow 17 is put into container; (2) in container, adding Glycerin, mixed triester with caprylic acid capric acid is 5kg, is mixed by pigment yellow 17 with Glycerin, mixed triester with caprylic acid capric acid, is A mixture; (3) separately get a container, in container, add polyoxylethylene abietate is 20kg, then to add petroleum sodium sulfonate be 23kg, then to add water be 170kg, mixes as B liquid; (4) mixed with B liquid by A mixture, use shears to shear 20min, rotating speed is 7000rpm; (5) shearing terminates rear preservation.
Embodiment 3
(1) to get order number be 450 object pigment yellow 17 powder is 12kg, and pigment yellow 17 is put into container; (2) in container, adding Glycerin, mixed triester with caprylic acid capric acid is 7kg, is mixed by pigment yellow 17 with Glycerin, mixed triester with caprylic acid capric acid, is A mixture; (3) separately get a container, in container, add polyoxylethylene abietate is 22kg, then to add petroleum sodium sulfonate be 18kg, then to add water be 165kg, mixes as B liquid; (4) mixed with B liquid by A mixture, use shears to shear 15min, rotating speed is 8000rpm; (5) shearing terminates rear preservation.
Particle diameter, thermostability, dewatering ability mensuration have been carried out to the product of embodiment 1, embodiment 2, embodiment 3.Result is as following table.
The product prepared has possessed good thermostability and dewatering ability.
Claims (5)
1. a preparation method for pigment yellow 17 emulsion, is characterized in that preparation method comprises the following steps: (1) gets order number be 400 ~ 500 object pigment yellow 17 powder is 10 ~ 12 parts, and pigment yellow 17 powder is put into container; (2) in container, adding Glycerin, mixed triester with caprylic acid capric acid is 5 ~ 9 parts, is mixed by pigment yellow 17 powder with Glycerin, mixed triester with caprylic acid capric acid, is A mixture; (3) separately get a container, in container, add polyoxylethylene abietate is 20 ~ 24 parts, then to add petroleum sodium sulfonate be 18 ~ 25 parts, then adds water and be 160 to 170 parts, mixes as B liquid; (4) mixed with B liquid by A mixture, use shears to shear 10 ~ 20min, rotating speed is 6000rpm to 8000rpm; (5) shearing terminates rear preservation.
2. the preparation method of a kind of pigment yellow 17 emulsion according to claim 1, is characterized in that pigment yellow 17 powder order number is 500 orders.
3. the preparation method of a kind of pigment yellow 17 emulsion according to claim 1, is characterized in that pigment yellow 17 powder is 12 parts
.
4. the preparation method of a kind of pigment yellow 17 emulsion according to claim 1, is characterized in that Glycerin, mixed triester with caprylic acid capric acid is 5 parts.
5. the preparation method of a kind of pigment yellow 17 emulsion according to claim 1, is characterized in that shears shear time is 20min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310411001.0A CN103483915B (en) | 2013-09-11 | 2013-09-11 | Preparation method of pigment yellow 17 emulsion |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310411001.0A CN103483915B (en) | 2013-09-11 | 2013-09-11 | Preparation method of pigment yellow 17 emulsion |
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| Publication Number | Publication Date |
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| CN103483915A CN103483915A (en) | 2014-01-01 |
| CN103483915B true CN103483915B (en) | 2015-01-21 |
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| CN201310411001.0A Active CN103483915B (en) | 2013-09-11 | 2013-09-11 | Preparation method of pigment yellow 17 emulsion |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2048206A1 (en) * | 2006-07-31 | 2009-04-15 | DIC Corporation | Process for producing aqueous pigment dispersion and ink for ink-jet recording |
| CN101469155A (en) * | 2007-12-24 | 2009-07-01 | 深圳市海川实业股份有限公司 | Environment friendly transparent iron oxide yellow superfine aqueous color sizing dispersion and preparation thereof |
| CN101597443A (en) * | 2008-12-25 | 2009-12-09 | 天津兆阳纳米科技有限公司 | A kind of Yellow nanometer water-type pigment dispersion |
| CN101597446A (en) * | 2008-12-25 | 2009-12-09 | 天津兆阳纳米科技有限公司 | A kind of stable-type yellow nanometer water-type pigment dispersion |
-
2013
- 2013-09-11 CN CN201310411001.0A patent/CN103483915B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2048206A1 (en) * | 2006-07-31 | 2009-04-15 | DIC Corporation | Process for producing aqueous pigment dispersion and ink for ink-jet recording |
| CN101469155A (en) * | 2007-12-24 | 2009-07-01 | 深圳市海川实业股份有限公司 | Environment friendly transparent iron oxide yellow superfine aqueous color sizing dispersion and preparation thereof |
| CN101597443A (en) * | 2008-12-25 | 2009-12-09 | 天津兆阳纳米科技有限公司 | A kind of Yellow nanometer water-type pigment dispersion |
| CN101597446A (en) * | 2008-12-25 | 2009-12-09 | 天津兆阳纳米科技有限公司 | A kind of stable-type yellow nanometer water-type pigment dispersion |
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| CN103483915A (en) | 2014-01-01 |
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Owner name: WUJIANG HUACHENG COMPOSITE TECHNOLOGY CO., LTD. Free format text: FORMER OWNER: WUJIANG BINGXIN CULTURAL + EDUCATIONAL GOODS CO., LTD. Effective date: 20141126 |
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Free format text: CORRECT: ADDRESS; FROM: 215221 SUZHOU, JIANGSU PROVINCE TO: 215000 SUZHOU, JIANGSU PROVINCE |
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Effective date of registration: 20141126 Address after: 215000 Jiangsu Province, Wujiang District of Suzhou city with Wu Road No. 22 Applicant after: Wujiang Huacheng Composite Technology Co., Ltd. Address before: The village Pingwang town Wujiang District Suzhou City, Jiangsu province 215221 Applicant before: Wujiang Bingxin Cultural & Educational Goods Co., Ltd. |
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