CN103483915A - Preparation method of pigment yellow 17 emulsion - Google Patents
Preparation method of pigment yellow 17 emulsion Download PDFInfo
- Publication number
- CN103483915A CN103483915A CN201310411001.0A CN201310411001A CN103483915A CN 103483915 A CN103483915 A CN 103483915A CN 201310411001 A CN201310411001 A CN 201310411001A CN 103483915 A CN103483915 A CN 103483915A
- Authority
- CN
- China
- Prior art keywords
- pigment yellow
- parts
- preparation
- container
- emulsion
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000049 pigment Substances 0.000 title claims abstract description 40
- 239000000839 emulsion Substances 0.000 title claims abstract description 17
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 239000007788 liquid Substances 0.000 claims abstract description 12
- 239000000203 mixture Substances 0.000 claims abstract description 12
- 239000000843 powder Substances 0.000 claims abstract description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 7
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 6
- 150000002148 esters Chemical class 0.000 claims abstract description 6
- 239000003208 petroleum Substances 0.000 claims abstract description 6
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 6
- 239000011734 sodium Substances 0.000 claims abstract description 6
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims abstract description 6
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 24
- NXMUXTAGFPJGTQ-UHFFFAOYSA-N decanoic acid;octanoic acid Chemical compound CCCCCCCC(O)=O.CCCCCCCCCC(O)=O NXMUXTAGFPJGTQ-UHFFFAOYSA-N 0.000 claims description 12
- 235000011187 glycerol Nutrition 0.000 claims description 12
- 150000005691 triesters Chemical class 0.000 claims description 12
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 5
- RSWGJHLUYNHPMX-ONCXSQPRSA-N abietic acid Chemical compound C([C@@H]12)CC(C(C)C)=CC1=CC[C@@H]1[C@]2(C)CCC[C@@]1(C)C(O)=O RSWGJHLUYNHPMX-ONCXSQPRSA-N 0.000 claims description 5
- -1 polyoxyethylene Polymers 0.000 claims description 5
- 238000004321 preservation Methods 0.000 claims description 5
- 239000002245 particle Substances 0.000 abstract description 4
- 238000010008 shearing Methods 0.000 abstract 3
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 abstract 2
- LADGBHLMCUINGV-UHFFFAOYSA-N tricaprin Chemical compound CCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCC)COC(=O)CCCCCCCCC LADGBHLMCUINGV-UHFFFAOYSA-N 0.000 abstract 2
- 239000004530 micro-emulsion Substances 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
Landscapes
- Cosmetics (AREA)
Abstract
The invention relates to a preparation method of a pigment yellow 17 emulsion. The preparation method comprises the steps of (1) putting 10-12 parts of pigment yellow 17 powder of which the mesh number is 400-500 meshes into a container; (2) adding 5-9 parts of caprylic capric triglyceride into the container, and uniformly mixing pigment yellow 17 with caprylic capric triglyceride to obtain a mixture A; (3) adding 20-24 parts of rosin-polythylene oxide ester, 18-25 parts of petroleum sodium sulfonate and 160-170 parts of water into another container, and uniformly mixing to obtain liquid B; (4) mixing the mixture A with the liquid B, and shearing for 10-20 minutes by using a shearing machine at a rotating speed of 6000-8000rpm; (5) preserving after shearing. The particle size of the pigment yellow 17 emulsion prepared by the preparation method disclosed by the invention is 10-16 mum, and the application space of the pigment yellow 17 is expanded.
Description
Technical field
The present invention relates to a kind of preparation method of emulsion, particularly relate to a kind of preparation method of pigment yellow 17 emulsion.
Background technology
Pigment yellow 17 is a kind of azo pigment, has water-fast characteristics.Because it is water insoluble, under some aqueous systems, will restrict purposes and the space of pigment yellow 17.In order to expand the Application Areas of pigment yellow 17, a lot of people attempt pigment yellow 17 as microemulsion or emulsion, at present it are become to not having of microemulsion, because its structure decides to do, to become the microemulsion difficulty larger.As emulsion, current research is also less, and the effect obtained is very not remarkable, still has a lot of shortcomings, has restricted its large-scale application.
Summary of the invention
The technical problem solved: conventional pigment yellow 17 emulsion particle diameter is large, the problem of poor stability.
Technical scheme: the invention discloses a kind of preparation method of pigment yellow 17 emulsion, the preparation method comprises the following steps: (1) gets the order number is that 400～500 purpose pigment yellow 17 powder are 10～12 parts, and pigment yellow 17 is put into to container; (2) being 5～9 parts to adding Glycerin, mixed triester with caprylic acid capric acid in container, pigment yellow 17 is mixed with Glycerin, mixed triester with caprylic acid capric acid, is the A mixture; (3) separately getting a container, is 20～24 parts to adding the sylvic acid polyoxyethylene ester in container, then to add petroleum sodium sulfonate be 18～25 parts, then to add water be 160 to 170 parts, mixes the liquid into B; (4) the A mixture is mixed with B liquid, use shears to shear 10～20min, rotating speed is 6000rpm to 8000rpm; (5) shear and finish rear preservation.Pigment yellow 17 powder order number is preferably 500 orders.The pigment yellow 17 powder is preferably 12 parts
.glycerin, mixed triester with caprylic acid capric acid is preferably 5 parts.The shears shear time is preferably 20min.
Beneficial effect: it is very little that this preparation method prepares the pigment yellow 17 emulsion particle diameter, is 10um～16um.There is good thermal stability and centrifugal stability simultaneously.Emulsion heats 5～10h demixing phenomenon does not occur under 50 ℃.At rotating speed, be that under 4000rpm, centrifugal 30min～60min does not have layering and demulsifying phenomenon to produce yet in addition.
Embodiment
Embodiment 1
(1) getting the order number is that 400 purpose pigment yellow 17 powder are 10kg, and pigment yellow 17 is put into to container; (2) being 9kg to adding Glycerin, mixed triester with caprylic acid capric acid in container, pigment yellow 17 is mixed with Glycerin, mixed triester with caprylic acid capric acid, is the A mixture; (3) separately getting a container, is 24kg to adding the sylvic acid polyoxyethylene ester in container, then to add petroleum sodium sulfonate be 25kg, then to add water be 160kg, mixes the liquid into B; (4) the A mixture is mixed with B liquid, use shears to shear 10min, rotating speed is 6000rpm; (5) shear and finish rear preservation.
Embodiment 2
(1) getting the order number is that 500 purpose pigment yellow 17 powder are 11kg, and pigment yellow 17 is put into to container; (2) being 5kg to adding Glycerin, mixed triester with caprylic acid capric acid in container, pigment yellow 17 is mixed with Glycerin, mixed triester with caprylic acid capric acid, is the A mixture; (3) separately getting a container, is 20kg to adding the sylvic acid polyoxyethylene ester in container, then to add petroleum sodium sulfonate be 23kg, then to add water be 170kg, mixes the liquid into B; (4) the A mixture is mixed with B liquid, use shears to shear 20min, rotating speed is 7000rpm; (5) shear and finish rear preservation.
Embodiment 3
(1) getting the order number is that 450 purpose pigment yellow 17 powder are 12kg, and pigment yellow 17 is put into to container; (2) being 7kg to adding Glycerin, mixed triester with caprylic acid capric acid in container, pigment yellow 17 is mixed with Glycerin, mixed triester with caprylic acid capric acid, is the A mixture; (3) separately getting a container, is 22kg to adding the sylvic acid polyoxyethylene ester in container, then to add petroleum sodium sulfonate be 18kg, then to add water be 165kg, mixes the liquid into B; (4) the A mixture is mixed with B liquid, use shears to shear 15min, rotating speed is 8000rpm; (5) shear and finish rear preservation.
Product to embodiment 1, embodiment 2, embodiment 3 has carried out particle diameter, thermostability, centrifugal Stability Determination.Result is as following table.
The product prepared has possessed good thermostability and centrifugal stability.
Claims (5)
1. the preparation method of a pigment yellow 17 emulsion, it is characterized in that the preparation method comprises the following steps: (1) gets the order number is that 400～500 purpose pigment yellow 17 powder are 10～12 parts, and pigment yellow 17 is put into to container; (2) being 5～9 parts to adding Glycerin, mixed triester with caprylic acid capric acid in container, pigment yellow 17 is mixed with Glycerin, mixed triester with caprylic acid capric acid, is the A mixture; (3) separately getting a container, is 20～24 parts to adding the sylvic acid polyoxyethylene ester in container, then to add petroleum sodium sulfonate be 18～25 parts, then to add water be 160 to 170 parts, mixes the liquid into B; (4) the A mixture is mixed with B liquid, use shears to shear 10～20min, rotating speed is 6000rpm to 8000rpm; (5) shear and finish rear preservation.
2. the preparation method of a kind of pigment yellow 17 emulsion according to claim 1, is characterized in that pigment yellow 17 powder order number is 500 orders.
3. the preparation method of a kind of pigment yellow 17 emulsion according to claim 1, is characterized in that the pigment yellow 17 powder is 12 parts
.
4. the preparation method of a kind of pigment yellow 17 emulsion according to claim 1, is characterized in that Glycerin, mixed triester with caprylic acid capric acid is 5 parts.
5. the preparation method of a kind of pigment yellow 17 emulsion according to claim 1, is characterized in that the shears shear time is 20min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310411001.0A CN103483915B (en) | 2013-09-11 | 2013-09-11 | Preparation method of pigment yellow 17 emulsion |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310411001.0A CN103483915B (en) | 2013-09-11 | 2013-09-11 | Preparation method of pigment yellow 17 emulsion |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103483915A true CN103483915A (en) | 2014-01-01 |
| CN103483915B CN103483915B (en) | 2015-01-21 |
Family
ID=49824532
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310411001.0A Expired - Fee Related CN103483915B (en) | 2013-09-11 | 2013-09-11 | Preparation method of pigment yellow 17 emulsion |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103483915B (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2048206A1 (en) * | 2006-07-31 | 2009-04-15 | DIC Corporation | Process for producing aqueous pigment dispersion and ink for ink-jet recording |
| CN101469155A (en) * | 2007-12-24 | 2009-07-01 | 深圳市海川实业股份有限公司 | Environment friendly transparent iron oxide yellow superfine aqueous color sizing dispersion and preparation thereof |
| CN101597443A (en) * | 2008-12-25 | 2009-12-09 | 天津兆阳纳米科技有限公司 | A kind of Yellow nanometer water-type pigment dispersion |
| CN101597446A (en) * | 2008-12-25 | 2009-12-09 | 天津兆阳纳米科技有限公司 | A kind of stable-type yellow nanometer water-type pigment dispersion |
-
2013
- 2013-09-11 CN CN201310411001.0A patent/CN103483915B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2048206A1 (en) * | 2006-07-31 | 2009-04-15 | DIC Corporation | Process for producing aqueous pigment dispersion and ink for ink-jet recording |
| CN101469155A (en) * | 2007-12-24 | 2009-07-01 | 深圳市海川实业股份有限公司 | Environment friendly transparent iron oxide yellow superfine aqueous color sizing dispersion and preparation thereof |
| CN101597443A (en) * | 2008-12-25 | 2009-12-09 | 天津兆阳纳米科技有限公司 | A kind of Yellow nanometer water-type pigment dispersion |
| CN101597446A (en) * | 2008-12-25 | 2009-12-09 | 天津兆阳纳米科技有限公司 | A kind of stable-type yellow nanometer water-type pigment dispersion |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103483915B (en) | 2015-01-21 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103695177B (en) | A kind of red date essence and preparation method thereof | |
| CN103497753B (en) | One is applicable to the of the fracturing fluid linking agent of concentrated water | |
| CN114191455A (en) | Extraction process and preparation method of seaweed polyphenol | |
| CN103113874B (en) | Organic titanium crosslinking agent, and preparation method and application method thereof | |
| CN103694987A (en) | Composite acidizing and fracturing liquid and preparation method thereof | |
| CN102550659A (en) | Method for microwave pretreatment and water extraction of edible oil | |
| CN104711063B (en) | A kind of NEW TYPE OF COMPOSITE solid fuel and preparation method thereof | |
| CN103483915B (en) | Preparation method of pigment yellow 17 emulsion | |
| CN106561748A (en) | Potted plant pest control agent | |
| CN104974179A (en) | Extraction method of azadirachtin | |
| CN103333769A (en) | Radix puerariae fruit wine and preparation method thereof | |
| CN103689549B (en) | Water-dispersibility paprika red pigment micro emulsion and preparation method thereof | |
| CN104263440B (en) | A kind of diesel oil microemulsion and preparation method thereof | |
| CN104147071A (en) | Method for extracting effective components from saussurea involucrata | |
| CN103866609B (en) | A kind of foam-killing agent in paper-making and preparation method thereof | |
| CN105295430A (en) | Preparation method of water-soluble capsanthin | |
| CN102265831A (en) | Botanical pesticide Chamaejasmine A suspension and preparation method thereof | |
| CN104152194A (en) | Microemulsified fuel oil and preparation method thereof | |
| CN108164620A (en) | The method of Subcritical water chromotagraphy chitin | |
| CN105086637A (en) | High-stability pigment yellow 73 preparation and preparation method thereof | |
| CN103222935B (en) | Armeniaca sibirica oil skin-moisturizing lotion and preparation method thereof | |
| CN104341253B (en) | Efficient rock powdery emulsion explosive and its preparation method | |
| CN105494402A (en) | Preparation method of indoxacarb-emamectin benzoate water emulsion formula | |
| CN102987487B (en) | Preparation method of functional beverage for quickly replenishing physical ability | |
| CN103483196A (en) | Method for extracting oleocanthal from olive oil |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| ASS | Succession or assignment of patent right |
Owner name: WUJIANG HUACHENG COMPOSITE TECHNOLOGY CO., LTD. Free format text: FORMER OWNER: WUJIANG BINGXIN CULTURAL + EDUCATIONAL GOODS CO., LTD. Effective date: 20141126 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| COR | Change of bibliographic data |
Free format text: CORRECT: ADDRESS; FROM: 215221 SUZHOU, JIANGSU PROVINCE TO: 215000 SUZHOU, JIANGSU PROVINCE |
|
| TA01 | Transfer of patent application right |
Effective date of registration: 20141126 Address after: 215000 Jiangsu Province, Wujiang District of Suzhou city with Wu Road No. 22 Applicant after: WUJIANG HUACHENG COMPOSITE MATERIAL SCIENCE & TECHNOLOGY Co.,Ltd. Address before: The village Pingwang town Wujiang District Suzhou City, Jiangsu province 215221 Applicant before: WUJIANG BINGXIN CULTURAL & EDUCATIONAL GOODS Co.,Ltd. |
|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150121 |