CN103483877A - Formula and preparation method of coloring agent for yellowing setae - Google Patents
Formula and preparation method of coloring agent for yellowing setae Download PDFInfo
- Publication number
- CN103483877A CN103483877A CN201310410408.1A CN201310410408A CN103483877A CN 103483877 A CN103483877 A CN 103483877A CN 201310410408 A CN201310410408 A CN 201310410408A CN 103483877 A CN103483877 A CN 103483877A
- Authority
- CN
- China
- Prior art keywords
- mane
- preparation
- fully
- formula
- certain amount
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Coloring (AREA)
Abstract
The invention relates to a formula and preparation method of a coloring agent for yellowing setae. The formula comprises the following components in percentage by mass: 15-20% of bisdiazo condensate, 12-18% of isoindolinone, 20-28% of bismuth vanadate, 18-20% of cadmium yellow, 4-8% of aramid and 20-25% of an organic solvent. The coloring agent prepared according to the formula and preparation method disclosed by the invention has the advantages of reasonable collocation, convenient manufacturing, low cost, high durability and the like, can ensure that the yellowed setae can not fade for a long time, and is good in coloring effect, so that the quality of the setae is ensured.
Description
Technical field
The present invention relates to bristle brush manufacturing technology field, specifically a kind of yellow staining agent formula and preparation method thereof that dyes for mane.
Background technology
As everyone knows, bristle brush is comparatively common in daily life, as the polish applying shoes-brush of leather shoes, dust cleaning brush, aint brush etc.The color of bristle brush is also varied, adularescent, redness, brown, black etc., and traditional mane is brown color or brownish black, the bright-coloured degree of color is poor, and contains a lot of off-color markings in mane, in the process of mane process for processing, it need to be dyed to unified color, as yellow.Because the sticking power of traditional Yellow colorant on mane is poor, after mane is used for some time, yellow can be faded, show the intrinsic colour of mane, affect the outward appearance of product, people often just can abandon it when fading appears in this series products, can cause the waste of product, and cause negative impact to the public praise of product.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of and arranges in pairs or groups reasonably, convenient manufacture, with low cost, durability is high, can guarantee that mane dyes yellow rear permanent non-fading formula and preparation method thereof, i.e. a kind of yellow staining agent formula and preparation method thereof that dyes for mane.
Technical problem to be solved by this invention realizes by the following technical solutions:
A kind ofly for mane, dye yellow staining agent formula, this formula comprises disazo condensation thing, isoindolinone, pucherite, cadmium yellow, fragrant acid amides and organic solvent, and the shared mass percent of each component is as follows:
The performance of each component and effect are as follows:
The disazo condensation thing: as organic yellow dyes, have the advantages such as with low cost, that affinity is stronger, the shade of colour is too deep, and Color is good.
Isoindolinone: lovely luster, strong coloring force, thermotolerance is high, and fine heat-resisting performance is acidproof, alkali resistance, non-migratory property.Purposes: be mainly used in plastics and coating, paint, printing ink painted, also, for the synthesis of the original liquid coloring of fiber, can be used with other dyestuff fusion, can improve the tinctorial property of other dyestuff.
Pucherite: pucherite is a kind of glassy yellow inorganic chemical, and it, containing harmful heavy metal element, is not a kind of burning material of environmental protection low-carbon (LC).Pucherite has multiple lattice, and the pucherite of different crystalline lattice has different character and application.Strong adhesion on mane, durable in use, fugitive color not.
Cadmium yellow: flour, odorless, without gas, is insoluble in water, is insoluble in acetone, is insoluble in ethanol, is insoluble to soda acid, without explosion hazard, non-inflammable, non-aggressive.Color clear is saturated, its spectral range from yellowish through true yellow until the ruddiness Huang.The cadmium yellow of Containing Sulfur zinc, its yellow chromaticity shoals with the increase of ZnS solid solution capacity, until yellowish.The filled-type cadmium yellow has not only reduced cost, and some performance makes moderate progress, as proportion and oil number reduce, dispersed better in organic medium, can effectively promote that each component dyes to mane, and improve sticking power.
The virtue acid amides: have high abrasion, high heat-resisting degraded and high resistance to chemicals material, stability is higher, thereby can effectively guarantee that mane has dyeing characteristic not easy to fade later.
Organic solvent: be mainly used in each components dissolved is mixed.
A kind of preparation method who dyes yellow staining agent formula for mane, this preparation method comprises the following steps:
1) measure a certain amount of isoindolinone and disazo condensation thing, guarantee fully to pulverize powdered, then add in organic solvent, stir fully, until dissolve fully;
2) take a certain amount of pucherite, be crushed into powder, add in the container in step 1), be heated to 50 degrees centigrade, rapid stirring is until dissolve fully;
3) take a certain amount of fragrant acid amides, be crushed into powder, add step 2 to) in, temperature is risen to 65 degrees centigrade of left and right, constant temperature stirs, until dissolve fully;
4) take a certain amount of cadmium yellow, evenly add in step 3), fully be uniformly mixed;
5) mixed solution formed in step 4) is cooled to room temperature, then filters the impurity existed in the elimination mixed solution.
The invention has the beneficial effects as follows: the present invention have collocation rationally, conveniently manufacture, the advantage such as with low cost and durability is high, can guarantee that mane dyes after Huang colour-fast for a long time, Color is good, thereby has guaranteed the quality of mane.
Embodiment
For technique means, creation characteristic that the present invention is realized, reach purpose and effect is easy to understand, below the present invention is further set forth.
Embodiment mono-:
A kind ofly for mane, dye yellow staining agent formula, this formula comprises disazo condensation thing, isoindolinone, pucherite, cadmium yellow, fragrant acid amides and organic solvent, and the shared mass percent of each component is as follows:
A kind of preparation method who dyes yellow staining agent formula for mane, this preparation method comprises the following steps:
1) measure a certain amount of isoindolinone and disazo condensation thing, guarantee fully to pulverize powdered, then add in organic solvent, stir fully, until dissolve fully;
2) take a certain amount of pucherite, be crushed into powder, add in the container in step 1), be heated to 50 degrees centigrade, rapid stirring is until dissolve fully;
3) take a certain amount of fragrant acid amides, be crushed into powder, add step 2 to) in, temperature is risen to 65 degrees centigrade of left and right, constant temperature stirs, until dissolve fully;
4) take a certain amount of cadmium yellow, evenly add in step 3), fully be uniformly mixed;
5) mixed solution formed in step 4) is cooled to room temperature, then filters the impurity existed in the elimination mixed solution.
The mane Yellow colorant of making according to above-mentioned formula and preparation method, can improve the sticking power of staining agent on mane, guarantees the persistence of dyeing, improves the durability of mane, guaranteed the quality of mane.
Embodiment bis-:
A kind ofly for mane, dye yellow staining agent formula, this formula comprises disazo condensation thing, isoindolinone, pucherite, cadmium yellow, fragrant acid amides and organic solvent, and the shared mass percent of each component is as follows:
A kind of preparation method who dyes yellow staining agent formula for mane, this preparation method comprises the following steps:
1) measure a certain amount of isoindolinone and disazo condensation thing, guarantee fully to pulverize powdered, then add in organic solvent, stir fully, until dissolve fully;
2) take a certain amount of pucherite, be crushed into powder, add in the container in step 1), be heated to 50 degrees centigrade, rapid stirring is until dissolve fully;
3) take a certain amount of fragrant acid amides, be crushed into powder, add step 2 to) in, temperature is risen to 65 degrees centigrade of left and right, constant temperature stirs, until dissolve fully;
4) take a certain amount of cadmium yellow, evenly add in step 3), fully be uniformly mixed;
5) mixed solution formed in step 4) is cooled to room temperature, then filters the impurity existed in the elimination mixed solution.
The mane Yellow colorant of making according to above-mentioned formula and preparation method, can improve the sticking power of staining agent on mane, guarantees the persistence of dyeing, improves the durability of mane, guaranteed the quality of mane.
Embodiment tri-:
A kind ofly for mane, dye yellow staining agent formula, this formula comprises disazo condensation thing, isoindolinone, pucherite, cadmium yellow, fragrant acid amides and organic solvent, and the shared mass percent of each component is as follows:
A kind of preparation method who dyes yellow staining agent formula for mane, this preparation method comprises the following steps:
1) measure a certain amount of isoindolinone and disazo condensation thing, guarantee fully to pulverize powdered, then add in organic solvent, stir fully, until dissolve fully;
2) take a certain amount of pucherite, be crushed into powder, add in the container in step 1), be heated to 50 degrees centigrade, rapid stirring is until dissolve fully;
3) take a certain amount of fragrant acid amides, be crushed into powder, add step 2 to) in, temperature is risen to 65 degrees centigrade of left and right, constant temperature stirs, until dissolve fully;
4) take a certain amount of cadmium yellow, evenly add in step 3), fully be uniformly mixed;
5) mixed solution formed in step 4) is cooled to room temperature, then filters the impurity existed in the elimination mixed solution.
The mane Yellow colorant of making according to above-mentioned formula and preparation method, can improve the sticking power of staining agent on mane, guarantees the persistence of dyeing, improves the durability of mane, guaranteed the quality of mane.
Above demonstration and described ultimate principle of the present invention, principal character and advantage of the present invention.The technician of the industry should understand; the present invention is not restricted to the described embodiments; what in above-described embodiment and specification sheets, describe is principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.The claimed scope of the present invention is defined by appending claims and equivalent thereof.
Claims (2)
1. one kind is dyed yellow staining agent formula for mane, and it is characterized in that: this formula comprises disazo condensation thing, isoindolinone, pucherite, cadmium yellow, fragrant acid amides and organic solvent, and the shared mass percent of each component is as follows:
2. one kind is dyed for mane the preparation method that yellow staining agent is filled a prescription, and it is characterized in that: this preparation method comprises the following steps:
1) measure a certain amount of isoindolinone and disazo condensation thing, guarantee fully to pulverize powdered, then add in organic solvent, stir fully, until dissolve fully;
2) take a certain amount of pucherite, be crushed into powder, add in the container in step 1), be heated to 50 degrees centigrade, rapid stirring is until dissolve fully;
3) take a certain amount of fragrant acid amides, be crushed into powder, add step 2 to) in, temperature is risen to 65 degrees centigrade of left and right, constant temperature stirs, until dissolve fully;
4) take a certain amount of cadmium yellow, evenly add in step 3), fully be uniformly mixed;
5) mixed solution formed in step 4) is cooled to room temperature, then filters the impurity existed in the elimination mixed solution.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310410408.1A CN103483877A (en) | 2013-09-10 | 2013-09-10 | Formula and preparation method of coloring agent for yellowing setae |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310410408.1A CN103483877A (en) | 2013-09-10 | 2013-09-10 | Formula and preparation method of coloring agent for yellowing setae |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103483877A true CN103483877A (en) | 2014-01-01 |
Family
ID=49824496
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310410408.1A Pending CN103483877A (en) | 2013-09-10 | 2013-09-10 | Formula and preparation method of coloring agent for yellowing setae |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103483877A (en) |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20020076546A1 (en) * | 2000-12-18 | 2002-06-20 | Johnson Daniel D. | Two layer coating system having an enhanced visual effect |
| US20040163569A1 (en) * | 2003-01-17 | 2004-08-26 | Shakhnovich Alexander I. | Methods of preparing aqueous colored pigment dispersions, and inkjet ink compositions |
| CN1849374A (en) * | 2003-09-12 | 2006-10-18 | 科莱恩产品（德国）有限公司 | Pigment compositions consisting of organic and inorganic pigments |
| CN1995141A (en) * | 2006-01-03 | 2007-07-11 | 德古萨公司 | Universal pigment preparations |
| US20100266945A1 (en) * | 2009-04-17 | 2010-10-21 | Canon Kabushiki Kaisha | Pigment, method for manufacturing the same, pigment dispersion, and yellow toner |
| KR20100114423A (en) * | 2009-04-15 | 2010-10-25 | 주식회사 디젠 | Copolymer, methods for producing the same, and aqueous pigment compositions comprising the same |
| CN102453354A (en) * | 2010-10-29 | 2012-05-16 | 深圳市惠乐光电有限公司 | Pigment dispersion, preparation method thereof, pigment photoresist and color filter |
-
2013
- 2013-09-10 CN CN201310410408.1A patent/CN103483877A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20020076546A1 (en) * | 2000-12-18 | 2002-06-20 | Johnson Daniel D. | Two layer coating system having an enhanced visual effect |
| US20040163569A1 (en) * | 2003-01-17 | 2004-08-26 | Shakhnovich Alexander I. | Methods of preparing aqueous colored pigment dispersions, and inkjet ink compositions |
| CN1849374A (en) * | 2003-09-12 | 2006-10-18 | 科莱恩产品（德国）有限公司 | Pigment compositions consisting of organic and inorganic pigments |
| CN1995141A (en) * | 2006-01-03 | 2007-07-11 | 德古萨公司 | Universal pigment preparations |
| KR20100114423A (en) * | 2009-04-15 | 2010-10-25 | 주식회사 디젠 | Copolymer, methods for producing the same, and aqueous pigment compositions comprising the same |
| US20100266945A1 (en) * | 2009-04-17 | 2010-10-21 | Canon Kabushiki Kaisha | Pigment, method for manufacturing the same, pigment dispersion, and yellow toner |
| CN102453354A (en) * | 2010-10-29 | 2012-05-16 | 深圳市惠乐光电有限公司 | Pigment dispersion, preparation method thereof, pigment photoresist and color filter |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Kumar et al. | Structure and properties of dyes and pigments | |
| Gürses et al. | Dyes and pigments | |
| CN101824246B (en) | Water-based flexographic ink system dedicated to dual-PE paper cups | |
| CN102382515B (en) | Environment-friendly, strong acid-resistant, strong base-resistant and steaming-resistant ink and preparation method | |
| CN104231719B (en) | A kind of High temperature tempered glass coloured silk crystalline substance ink and preparation method thereof | |
| CN104231721B (en) | A kind of goth black environmental protection safety glass ink and preparation method thereof | |
| CN100569866C (en) | A kind of environment-friendly type and alkaline-resisting type disperse orange dyes mixture | |
| CN103694758B (en) | A kind of biological environmental production pigment for artistic design | |
| CN104497710A (en) | New thermochromic ink | |
| CN103525184B (en) | Environmental-protection stamp-pad ink and preparation method thereof | |
| CN101857491B (en) | Preparation method of fertilizer colorant and application method thereof | |
| CN102964924A (en) | Hydrolyzable color-fading color ink | |
| CN102796400A (en) | Yellow azo metallized dye composition, method and application thereof | |
| CN103483877A (en) | Formula and preparation method of coloring agent for yellowing setae | |
| CN103589238B (en) | Red brown silver light ink for silk screen printing | |
| CN103554993B (en) | Red reactive dye composition and the tint applications on fiber thereof | |
| CN105544238A (en) | Printing color paste containing grape pigment and printing process by using the same | |
| CN104446293A (en) | Environment-friendly colored water-based decorative coating | |
| CN106046853A (en) | Organic composite dye and preparation method thereof | |
| CN105985680A (en) | Glass UV-cured printing ink and preparation method thereof | |
| CN101117470A (en) | Light-stable water-resistant microemulsion aqueous ink | |
| CN105647280A (en) | Novel ink composition | |
| CN104263007B (en) | A kind of high light fastness reactive dyestuffs | |
| CN102241902B (en) | Photoluminescent waterborne pigment glue solution and production method thereof | |
| CN106479215A (en) | A kind of polymolecularity high coloring power 57:1 pigment and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20140101 |