CN101857491B - Preparation method of fertilizer colorant and application method thereof - Google Patents
Preparation method of fertilizer colorant and application method thereof Download PDFInfo
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- CN101857491B CN101857491B CN2010101842422A CN201010184242A CN101857491B CN 101857491 B CN101857491 B CN 101857491B CN 2010101842422 A CN2010101842422 A CN 2010101842422A CN 201010184242 A CN201010184242 A CN 201010184242A CN 101857491 B CN101857491 B CN 101857491B
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Abstract
The invention relates to a preparation method of a fertilizer colorant and an application method thereof. The preparation method comprises the following steps of: respectively dissolving water-soluble dyes such as bright red, rose red, acid blue, brilliant blue, golden yellow or lemon yellow into water; respectively adding 1-3% dispersing agent; stirring and respectively preparing into red inner colorant, blue inner colorant and yellow inner colorant for later use; respectively dissolving oil-soluble dyes such as lithol red, toluidine red, phthalocyanine blue, transparent blue, benzidine yellow or fluorescence yellow into base oil dissolvent; respectively adding the 1-3% dispersing agent; stirring and respectively preparing into red outer colorant, blue outer colorant and yellow outer colorant; directly stirring and blending the inner colorants and fertilizer raw materials; and spraying the outer colorants, so that the fertilizer is evenly colored. The preparation method can prepare the colored fertilizer which can not discolor under the functions of strong acid, strong base, strong reductant, strong oxygenant and microbe, and has the characteristics of small use amount of the colorant, stable coloration, low cost, pure color, good appearance, wide adaptability, high safety, good performance and the like.
Description
Technical field
The present invention relates to a kind of preparation and method of use of tinting material, be specifically related to a kind of preparation and method of use of fertilizer staining agent, belong to fertilizer staining technique field.
Background technology
Development along with the chemical industry technology; Staining technique has slowly got into the chemical fertilizers production technical field; Some chemical fertilizers production enterprises add some staining agents or tinting material in producing the process of fertilizer, be in order to prevent other people counterfeit oneself brand on the one hand; Be in order to improve the appearance luster of fertilizer, to be convenient to kind and brand that the user differentiates chemical fertilizer intuitively simultaneously on the other hand.The staining agent or the tinting material that are used for fertilizer coloration is divided into the water-soluble and oily type that dissolves; General staining agent all is by dyestuff or pigment and solvent composition; Some solvent or dyestuff are not easy degraded, can get into soil, have polluted soil; Some can be damaged human body by plant absorbing, brings bad influence for people's life health.In order to produce the fertilizer coloration agent of safety and reliability; The researchist is constantly making great efforts; Seek various natural-staining agent, but natural staining agent processing conditions such as acid and alkali-resistance, high temperature not, stability is poor; Be unfavorable for producing the stable color-tinted product of color and luster, influence the aspects such as sale of product.
Summary of the invention
Technical problem to be solved by this invention is: a kind of preparation method and method of use thereof of resistant to elevated temperatures coloring stabilized, uniform tinting material are provided, and colour-fast under strong acid, highly basic, strong oxidizer, strong reductant and biological action with the tinting material that this method is produced.
In order to address the above problem, the technical scheme that the present invention adopted is:
Water-soluble dye is dissolved with suitable quantity of water, add dispersion agent and process the intrinsic color agent, then oil color is dissolved with an amount of base oil kind solvent; Add dispersion agent, process the accretion toner, intrinsic color agent and the direct stirring and evenly mixing of chemical fertilizer raw material; The add-on of intrinsic color agent is the 0.1-0.3 ‰ of by weight of fertilizer, with the spraying of accretion toner, stirs again; Make the chemical fertilizer raw material uniformly colour, process coloured fertilizer of even dyeing.
The concrete operations step is:
Water-soluble dye is bright red, rose-red, acid lake blue, light blue, golden yellow or lemon yellow difference are soluble in water, add dispersion agent 1-3% more respectively, process red, indigo plant and the agent of xanchromatic intrinsic color after the stirring respectively.
Oil color Lithol Red, toluidine red, phthalocyanine blue, transparent indigo plant, diarylide yellow or fluorescent yellow are dissolved in the base oil kind solvent respectively, add dispersion agent 1-3% more respectively, process red, indigo plant and xanchromatic accretion toner after the stirring respectively.
Directly mix with intrinsic color agent and chemical fertilizer raw material, and then, make fertilizer evenly catch color with the chemical fertilizer raw material that the spraying of accretion toner has stirred with the intrinsic color agent.
Described dispersion agent is meant modified lignin mahogany sulfonate.
The invention has the beneficial effects as follows:
It is colour-fast under strong acid, highly basic, strong reductant, strong oxidizer, microbial process to produce coloured chemical fertilizer with method of the present invention; This kind tinting material consumption is few, and is coloring stabilized, and cost is low; Chemical fertilizer can uniform coloring, color is pure, outward appearance good; Pollution-free, have wide adaptability, characteristics such as safe, excellent property.
Embodiment
Through embodiment the present invention is explained further details below, these embodiment only are used for explaining the present invention, do not limit the scope of the invention.
Embodiment 1
Water-soluble dye is bright red soluble in water, add modified lignin resin sodium sulfonate dispersion agent 1% again, process red intrinsic color agent after the stirring respectively.
The oil color Lithol Red is dissolved in the base oil kind solvent, adds modified lignin resin sodium sulfonate dispersion agent 1% again, process red accretion toner after the stirring respectively.
Directly mix with 0.1 ‰ intrinsic color agent and chemical fertilizer raw material, and then, make fertilizer evenly catch color with the chemical fertilizer raw material that the spraying of accretion toner has stirred with the intrinsic color agent.
Embodiment 2
Water-soluble dye is bright red soluble in water, add modified lignin resin sodium sulfonate dispersion agent 3% again, process red intrinsic color agent after the stirring respectively.
The oil color Lithol Red is dissolved in the base oil kind solvent, adds modified lignin resin sodium sulfonate dispersion agent 3% again, process red accretion toner after the stirring respectively.
Directly mix with 0.3 ‰ intrinsic color agent and chemical fertilizer raw material, and then, make fertilizer evenly catch color with the chemical fertilizer raw material that the spraying of accretion toner has stirred with the intrinsic color agent.
Embodiment 3
Water-soluble dye is bright red soluble in water, add modified lignin resin sodium sulfonate dispersion agent 2% again, process red intrinsic color agent after the stirring respectively.
The oil color Lithol Red is dissolved in the base oil kind solvent, adds modified lignin resin sodium sulfonate dispersion agent 2% again, process red accretion toner after the stirring respectively.
Directly mix with 0.2 ‰ intrinsic color agent and chemical fertilizer raw material, and then, make fertilizer evenly catch color with the chemical fertilizer raw material that the spraying of accretion toner has stirred with the intrinsic color agent.
Embodiment 4
Water-soluble dye is rose-red soluble in water, add dispersing agent MF dispersion agent 1% again, process red intrinsic color agent after the stirring respectively.
The oil color toluidine red is dissolved in the base oil kind solvent, adds dispersing agent MF dispersion agent 1% again, process red accretion toner after the stirring respectively.
Directly mix with 0.2 ‰ intrinsic color agent and chemical fertilizer raw material, and then, make fertilizer evenly catch color with the chemical fertilizer raw material that the spraying of accretion toner has stirred with the intrinsic color agent.
Embodiment 5
Water-soluble dye is rose-red soluble in water, add modified lignin resin sodium sulfonate dispersion agent 3% again, process red intrinsic color agent after the stirring respectively.
The oil color toluidine red is dissolved in the base oil kind solvent, adds modified lignin resin sodium sulfonate dispersion agent 3% again, process red accretion toner after the stirring respectively.
Directly mix with 0.1 ‰ intrinsic color agent and chemical fertilizer raw material, and then, make fertilizer evenly catch color with the chemical fertilizer raw material that the spraying of accretion toner has stirred with the intrinsic color agent.
Embodiment 6
Water-soluble dye is rose-red soluble in water, add modified lignin resin sodium sulfonate dispersion agent 2% again, process red intrinsic color agent after the stirring respectively.
The oil color toluidine red is dissolved in the base oil kind solvent, adds modified lignin resin sodium sulfonate dispersion agent 2% again, process red accretion toner after the stirring respectively.
Directly mix with 0.3 ‰ intrinsic color agent and chemical fertilizer raw material, and then, make fertilizer evenly catch color with the chemical fertilizer raw material that the spraying of accretion toner has stirred with the intrinsic color agent.
Embodiment 7
The water-soluble dye acid lake blue is soluble in water, add dispersing agent MF dispersion agent 1% again, process blue intrinsic color agent after the stirring respectively.
The oil color phthalocyanine blue is dissolved in the base oil kind solvent, adds dispersing agent MF dispersion agent 1% again, process blue accretion toner after the stirring respectively.
Directly mix with 0.1 ‰ intrinsic color agent and chemical fertilizer raw material, and then, make fertilizer evenly catch color with the chemical fertilizer raw material that the spraying of accretion toner has stirred with the intrinsic color agent.
Embodiment 8
The water-soluble dye light blue is soluble in water, add dispersing agent MF dispersion agent 2% again, process blue intrinsic color agent after the stirring respectively.
The transparent indigo plant of oil color is dissolved in the base oil kind solvent, adds dispersing agent MF dispersion agent 2% again, process blue accretion toner after the stirring respectively.
Directly mix with 0.2 ‰ intrinsic color agent and chemical fertilizer raw material, and then, make fertilizer evenly catch color with the chemical fertilizer raw material that the spraying of accretion toner has stirred with the intrinsic color agent.
Embodiment 9
Water-soluble dye is golden yellow soluble in water, add dispersing agent MF dispersion agent 3% again, process the agent of xanchromatic intrinsic color after the stirring respectively.
The oil color diarylide yellow is dissolved in the base oil kind solvent, adds dispersing agent MF dispersion agent 3% again, process xanchromatic accretion toner after the stirring respectively.
Directly mix with 0.3 ‰ intrinsic color agent and chemical fertilizer raw material, and then, make fertilizer evenly catch color with the chemical fertilizer raw material that the spraying of accretion toner has stirred with the intrinsic color agent.
Embodiment 10
Water-soluble dye is lemon yellow soluble in water, add dispersing agent MF dispersion agent 1% again, process the agent of xanchromatic intrinsic color after the stirring respectively.
Oil color fluorescent yellow is dissolved in the base oil kind solvent, adds dispersing agent MF dispersion agent 1% again, process xanchromatic accretion toner after the stirring respectively.
Directly mix with 0.3 ‰ intrinsic color agent and chemical fertilizer raw material, and then, make fertilizer evenly catch color with the chemical fertilizer raw material that the spraying of accretion toner has stirred with the intrinsic color agent.
Claims (1)
1. the preparation of a fertilizer tinting material and method of use is characterized in that: water-soluble dye is dissolved with suitable quantity of water, add dispersion agent and process the intrinsic color agent; Then oil color is dissolved with an amount of base oil kind solvent, add dispersion agent, process the accretion toner; Intrinsic color agent and chemical fertilizer raw material are directly stirred, and the add-on of intrinsic color agent is the 0.1-0.3 ‰ of by weight of fertilizer, sprays with the accretion toner again; Stir; Make the chemical fertilizer raw material uniformly colour, process coloured fertilizer of even dyeing, the consumption of outer staining agent is with the fertilizer uniformly colour;
Described water-soluble dye is bright red, rose-red, acid lake blue, light blue, golden yellow or lemon yellow;
The add-on of described dispersion agent is the 1-3% of dyestuff;
Described oil color is Lithol Red, toluidine red, phthalocyanine blue, transparent indigo plant, diarylide yellow or fluorescent yellow;
Described dispersion agent is meant modified lignin mahogany sulfonate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010101842422A CN101857491B (en) | 2010-05-20 | 2010-05-20 | Preparation method of fertilizer colorant and application method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010101842422A CN101857491B (en) | 2010-05-20 | 2010-05-20 | Preparation method of fertilizer colorant and application method thereof |
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| CN101857491A CN101857491A (en) | 2010-10-13 |
| CN101857491B true CN101857491B (en) | 2012-03-21 |
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Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102093136A (en) * | 2010-12-27 | 2011-06-15 | 湖北富邦科技股份有限公司 | Inner fertilizer additive adopting edible bright cyanine and preparation method thereof |
| CN102816011B (en) * | 2012-09-13 | 2013-11-13 | 安徽金正大生态工程有限公司 | Marking compound for fertilizer, and method and device for controlled-release marking of granulated fertilizer |
| CN103848676A (en) * | 2012-11-29 | 2014-06-11 | 倪伟华 | Fertilizer with easily identified fertilizer efficiency and preparation method thereof |
| CN104865359A (en) * | 2015-05-11 | 2015-08-26 | 刘俊平 | Meal residue liquid regenerated oil dyeing agent |
| CN105237288A (en) * | 2015-09-12 | 2016-01-13 | 云南润杰农业科技股份有限公司 | Medium element water-soluble fertilizer and preparation method thereof |
| AU2017285193B2 (en) * | 2016-06-18 | 2020-04-30 | Milliken & Company | Compositions suitable for use in making fertilizers, methods for making such compositions, and method for making fertilizers using the same |
| CN115403938B (en) * | 2022-09-22 | 2024-02-09 | 浙江纳美新材料股份有限公司 | Organic pigment color paste for chemical fertilizer dyeing and preparation method and application thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1762915A (en) * | 2005-09-01 | 2006-04-26 | 刘天暘 | Coloured phosphorus ammonium fertilizer production method and its dying wrapping agent |
| CN1762914A (en) * | 2005-08-31 | 2006-04-26 | 刘天暘 | Coloured phosphorus ammonium fertilizer production method and its dying wrapping agent |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1762914A (en) * | 2005-08-31 | 2006-04-26 | 刘天暘 | Coloured phosphorus ammonium fertilizer production method and its dying wrapping agent |
| CN1762915A (en) * | 2005-09-01 | 2006-04-26 | 刘天暘 | Coloured phosphorus ammonium fertilizer production method and its dying wrapping agent |
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Effective date of registration: 20160302 Address after: 510000, Suixi County, Zhanjiang Province, Guangdong Province, Beizhen Province, 374 lines north Patentee after: GUANGDONG BOKE INDUSTRIAL Co.,Ltd. Address before: 524000, Suixi County, Guangdong City, Zhanjiang Province, 57 town agriculture and forestry road Patentee before: GUANG DONG NEW LUYUAN CHEMICAL Co.,Ltd. |
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Effective date of registration: 20180416 Address after: 524338 Jin Yuan Road 1, Ling Bei Industrial Park, Suixi County, Zhanjiang, Guangdong. Patentee after: GUANG DONG NEW LUYUAN CHEMICAL Co.,Ltd. Address before: 510000, Suixi County, Zhanjiang Province, Guangdong Province, Beizhen Province, 374 lines north Patentee before: GUANGDONG BOKE INDUSTRIAL Co.,Ltd. |
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