CN103466944A - Colored glaze with favorable clarification effect and high product quality - Google Patents
Colored glaze with favorable clarification effect and high product quality Download PDFInfo
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Abstract
The invention relates to a colored glaze with favorable clarification effect and high product quality, which is prepared from the following raw materials in parts by weight: 95-110 parts of quartz sand, 42-46 parts of soda ash, 10-12 parts of aluminum oxide, 45-50 parts of lead peroxide, 1-1.5 parts of cerium oxide, 3-4 parts of antimony trioxide, 0.1-0.5 part of sodium nitrate and 1-1.5 parts of pigment. The cerium oxide and antimony trioxide are combined to be used as a clarifier, and thus, the clarification effect is obviously better than that of the independently used cerium oxide or antimony trioxide; by controlling the cerium oxide:antimony trioxide ratio at 1:(2-4), the prepared colored glaze has the advantages of high gloss, few bubbles, high transparency, few stripes in the finished product, obviously improved quality and short clarification time (6-8 hours); and the colored glaze formula materials have long acting property and low softening point, and thus, are suitable for forming the colored glaze.
Description
Technical field
The present invention relates to inorganic amorphous technical field of material, specifically, is the coloured glaze that a kind of clarifying effect is good, product property is good.
Background technology
Coloured glaze is a kind of silicate product, has a long history, and its quality is glittering and translucent, bright and glittering, it is magnificent to change irregularly, and fully demonstrates Oriental's exquisiteness, exquisiteness and implicit, is the important decoration element in building, is also a wonderful work in artistic decoration.The main component of coloured glaze is SiO
2(being silicon-dioxide), aluminum oxide, fusing assistant plumbous oxide and pigment etc.
The coloured glaze composition is low with softening temperature, material property is long for good characteristic is arranged, and so is convenient to the technique manufacture, is applicable to the coloured glaze shaping, and the quality of colored glaze product is embodied in good luster, and bubble, striped, calculus are few.The softening temperature of coloured glaze, material property depend primarily on kind and the ratio thereof of composition in the coloured glaze formula, and in the coloured glaze basic ingredient, add finings can make the reduction of coloured glaze temperature of fusion, refining quality be improved, and avoid producing the defects such as bubble, striped, calculus.Finings can be emitted decomposition gas in the coloured glaze production process, or self gasifies, and produces a large amount of bubbles, receives peripheral small bubbles, follows blub to rise and promotes the coloured glaze clarification.Finings commonly used has cerium dioxide, white arsenic etc. at present, but white arsenic is highly toxic substance, threatens operator ' s health serious environment pollution; The clarifying effect of cerium dioxide still can, but settling time is longer, and cerium is rare earth element, cost is more expensive.Therefore need the coloured glaze formula that a kind of softening temperature is low, material property is long, clarifying effect is good, settling time is short, product property is good badly.
Patent documentation CN201210526726.X, open day 2013.03.06, a kind of light color terra-cotta for building are disclosed, described light color terra-cotta for building are to add 0.4-0.6kg magnesium oxide in every kilogram of magnesium chloride solution, stir 6-8 minute, then add successively the 0.05-0.1kg Magnesium Silicate q-agent, 0.02-0.03kg urea-formaldehyde resin, 0.06-0.1g volatile salt, 2-3g tertiary sodium phosphate and 2-3g colorant, stir 20-30 minute, then the material be stirred is poured on glasscloth, strike off compacting, after the spontaneous curing drying, make, by the way, , light color terra-cotta smooth surface for building is clean and tidy, bright in colour beautiful, will never fade, there is good anti-folding and anti-pressing, anti-rapid heat cycle, acid-proof alkaline and frost resistance energy, quality is light, water-intake rate is low, and insulation and soundproof effect are good, cost is low.But at present about being applicable to prepare azure stone handicraft, colory coloured glaze formula report is less.
Summary of the invention
The objective of the invention is, for deficiency of the prior art, provides the coloured glaze that a kind of clarifying effect is good, product property is good.
For achieving the above object, the technical scheme that the present invention takes is:
The coloured glaze that a kind of clarifying effect is good, product property is good, described coloured glaze is made by the raw material of following weight part: quartz sand 93-105 part, soda ash 42-46 part, aluminium sesquioxide 9-13 part, plumbic oxide 45-50 part, cerium dioxide 1-1.5 part, antimonous oxide 3-4 part, SODIUMNITRATE 0.1-0.5 part, pigment 1-1.5 part.
Preferably, described coloured glaze is made by the raw material of following weight part: quartz sand 98-100 part, soda ash 45-46 part, aluminium sesquioxide 10-12 part, plumbic oxide 48-50 part, cerium dioxide 1-1.2 part, antimonous oxide 3-3.5 part, SODIUMNITRATE 0.1-0.5 part, pigment 1-1.5 part.
Preferred, described coloured glaze is made by the raw material of following weight part: 99 parts of quartz sands, 45 parts of soda ash, 10 parts of aluminium sesquioxides, 49 parts of plumbic oxide, 1 part of cerium dioxide, 3.5 parts of antimonous oxides, 0.4 part of SODIUMNITRATE, pigment 1-1.5 part.
Described pigment can be Cr
2o
3, CuO, CoO, Mn
2o
3and TiO
2in one or more.
The invention has the advantages that:
The present invention is used in conjunction with cerium dioxide and antimonous oxide as finings, the through performance test, confirm that its clarifying effect significantly is better than using merely cerium dioxide or antimonous oxide, and find cerium dioxide or antimonous oxide ratio control at 1:(2-4) best results in scope, product good luster, the bubble prepared is few, transparency is high, in finished product, striped is few, quality is significantly improved, and settling time is short, within 6-8 hour, can complete, coloured glaze formula material property simultaneously of the present invention is long, softening temperature is low, is applicable to the coloured glaze moulding.
Embodiment
Below embodiment provided by the invention is elaborated.
embodiment 1 coloured glaze preparation of the present invention (one)
1) take each raw material: 99 parts of quartz sands, 45 parts of soda ash, 10 parts of aluminium sesquioxides, 49 parts of plumbic oxide, 1 part of cerium dioxide, 3.5 parts of antimonous oxides, 0.4 part of SODIUMNITRATE, Cr
2o
30.6 0.6 part of part, CuO, mix;
2) raw material is melted in tank furnace, 1630 ℃ of temperature of fusion, 1680 ℃ of clarifying temps, fusing time 13 hours, settling time 6 hours, obtain glass metal;
3) glass metal melted is cooled to 1100 ℃, according to design shape, manually is shaped, the artificial shaping is specially: artificial feeding, by instruments such as scissors, handle, blowpipe, moulds, through processes such as manually blowing, draw, press, turn, squeeze, make coloured glaze become desired shape;
4) goods after being shaped are sent into annealing in annealing furnace, and 500 ℃ of annealing temperatures slowly cool to room temperature after being incubated 2.5 hours, obtain product.
embodiment 2 coloured glaze preparation of the present invention (two)
1) take each raw material: 93 parts of quartz sands, 46 parts of soda ash, 9 parts of aluminium sesquioxides, 50 parts of plumbic oxide, 1 part of cerium dioxide, 4 parts of antimonous oxides, 0.1 part of SODIUMNITRATE, Cr
2o
31.2 0.3 part of part, CuO, mix;
2) raw material is melted in tank furnace, 1650 ℃ of temperature of fusion, 1660 ℃ of clarifying temps, fusing time 14 hours, settling time 7 hours, obtain glass metal;
3) glass metal melted is cooled to 1200 ℃, according to design shape, manually is shaped, the artificial shaping is specially: artificial feeding, by instruments such as scissors, handle, blowpipe, moulds, through processes such as manually blowing, draw, press, turn, squeeze, make coloured glaze become desired shape;
4) goods after being shaped are sent into annealing in annealing furnace, and 520 ℃ of annealing temperatures slowly cool to room temperature after being incubated 3 hours, obtain product.
embodiment 3 coloured glaze preparation of the present invention (three)
1) take each raw material: 105 parts of quartz sands, 42 parts of soda ash, 13 parts of aluminium sesquioxides, 45 parts of plumbic oxide, 1.5 parts of cerium dioxides, 3 parts of antimonous oxides, 0.5 part of SODIUMNITRATE, 0.98 part of CuO, 0.02 part of CoO mix;
2) raw material is melted in tank furnace, 1600 ℃ of temperature of fusion, 1700 ℃ of clarifying temps, fusing time 12 hours, settling time 8 hours, obtain glass metal;
3) glass metal melted is cooled to 1200 ℃, according to design shape, manually is shaped, the artificial shaping is specially: artificial feeding, by instruments such as scissors, handle, blowpipe, moulds, through processes such as manually blowing, draw, press, turn, squeeze, make coloured glaze become desired shape;
4) goods after being shaped are sent into annealing in annealing furnace, and 480 ℃ of annealing temperatures slowly cool to room temperature after being incubated 2 hours, obtain product.
embodiment 4 coloured glaze preparation of the present invention (four)
1) take each raw material: 93 parts of quartz sands, 42 parts of soda ash, 13 parts of aluminium sesquioxides, 50 parts of plumbic oxide, 1 part of cerium dioxide, 3 parts of antimonous oxides, 0.5 part of SODIUMNITRATE, Mn
2o
31.5 part, mix;
2) raw material is melted in tank furnace, 1650 ℃ of temperature of fusion, 1660 ℃ of clarifying temps, fusing time 13 hours, settling time 6 hours, obtain glass metal;
3) glass metal melted is cooled to 1150 ℃, according to design shape, manually is shaped, the artificial shaping is specially: artificial feeding, by instruments such as scissors, handle, blowpipe, moulds, through processes such as manually blowing, draw, press, turn, squeeze, make coloured glaze become desired shape;
4) goods after being shaped are sent into annealing in annealing furnace, and 480 ℃ of annealing temperatures slowly cool to room temperature after being incubated 2 hours, obtain product.
embodiment 5 coloured glaze preparation of the present invention (five)
1) take each raw material: 93 parts of quartz sands, 46 parts of soda ash, 10 parts of aluminium sesquioxides, 50 parts of plumbic oxide, 1 part of cerium dioxide, 3.5 parts of antimonous oxides, 0.1 part of SODIUMNITRATE, 1.5 parts of CoO mix;
2) raw material is melted in tank furnace, 1630 ℃ of temperature of fusion, 1680 ℃ of clarifying temps, fusing time 12 hours, settling time 6 hours, obtain glass metal;
3) glass metal melted is cooled to 1200 ℃, according to design shape, manually is shaped, the artificial shaping is specially: artificial feeding, by instruments such as scissors, handle, blowpipe, moulds, through processes such as manually blowing, draw, press, turn, squeeze, make coloured glaze become desired shape;
4) goods after being shaped are sent into annealing in annealing furnace, and 520 ℃ of annealing temperatures slowly cool to room temperature after being incubated 3 hours, obtain product.
embodiment 6 coloured glaze preparation of the present invention (six)
1) take each raw material: 99 parts of quartz sands, 45 parts of soda ash, 12 parts of aluminium sesquioxides, 48 parts of plumbic oxide, 1.2 parts of cerium dioxides, 3 parts of antimonous oxides, 0.5 part of SODIUMNITRATE, TiO
21 part, mix;
2) raw material is melted in tank furnace, 1630 ℃ of temperature of fusion, 1680 ℃ of clarifying temps, fusing time 12 hours, settling time 6 hours, obtain glass metal;
3) glass metal melted is cooled to 1100 ℃, according to design shape, manually is shaped, the artificial shaping is specially: artificial feeding, by instruments such as scissors, handle, blowpipe, moulds, through processes such as manually blowing, draw, press, turn, squeeze, make coloured glaze become desired shape;
4) goods after being shaped are sent into annealing in annealing furnace, and 520 ℃ of annealing temperatures slowly cool to room temperature after being incubated 2 hours, obtain product.
embodiment 7 coloured glaze preparation of the present invention (seven)
1) take each raw material: 105 parts of quartz sands, 42 parts of soda ash, 9 parts of aluminium sesquioxides, 50 parts of plumbic oxide, 1.5 parts of cerium dioxides, 4 parts of antimonous oxides, 0.5 part of SODIUMNITRATE, 1 part of CuO mix;
2) raw material is melted in tank furnace, 1600 ℃ of temperature of fusion, 1700 ℃ of clarifying temps, fusing time 12 hours, settling time 7 hours, obtain glass metal;
3) glass metal melted is cooled to 1200 ℃, according to design shape, manually is shaped, the artificial shaping is specially: artificial feeding, by instruments such as scissors, handle, blowpipe, moulds, through processes such as manually blowing, draw, press, turn, squeeze, make coloured glaze become desired shape;
4) goods after being shaped are sent into annealing in annealing furnace, and 480 ℃ of annealing temperatures slowly cool to room temperature after being incubated 2.5 hours, obtain product.
embodiment 8 coloured glaze preparation of the present invention (eight)
1) take each raw material: 93 parts of quartz sands, 46 parts of soda ash, 9 parts of aluminium sesquioxides, 50 parts of plumbic oxide, 1.5 parts of cerium dioxides, 3 parts of antimonous oxides, 0.1 part of SODIUMNITRATE, Cr
2o
31.2 0.3 part of part, CuO, mix;
2) raw material is melted in tank furnace, 1650 ℃ of temperature of fusion, 1660 ℃ of clarifying temps, fusing time 14 hours, settling time 7 hours, obtain glass metal;
3) glass metal melted is cooled to 1200 ℃, according to design shape, manually is shaped, the artificial shaping is specially: artificial feeding, by instruments such as scissors, handle, blowpipe, moulds, through processes such as manually blowing, draw, press, turn, squeeze, make coloured glaze become desired shape;
4) goods after being shaped are sent into annealing in annealing furnace, and 520 ℃ of annealing temperatures slowly cool to room temperature after being incubated 3 hours, obtain product.
comparative Examples 1
1) take each raw material: 99 parts of quartz sands, 45.13 parts of soda ash, 10 parts of aluminium sesquioxides, 49 parts of plumbic oxide, 4.9 parts of cerium dioxides, Cr
2o
30.6 0.6 part of part, CuO, mix;
2) raw material is melted in tank furnace, 1630 ℃ of temperature of fusion, 1680 ℃ of clarifying temps, fusing time 13 hours, settling time 6 hours, obtain glass metal;
3) glass metal melted is cooled to 1100 ℃, according to design shape, manually is shaped, the artificial shaping is specially: artificial feeding, by instruments such as scissors, handle, blowpipe, moulds, through processes such as manually blowing, draw, press, turn, squeeze, make coloured glaze become desired shape;
4) goods after being shaped are sent into annealing in annealing furnace, and 500 ℃ of annealing temperatures slowly cool to room temperature after being incubated 2.5 hours, obtain product.
comparative Examples 2
1) take each raw material: 105 parts of quartz sands, 42 parts of soda ash, 13 parts of aluminium sesquioxides, 45 parts of plumbic oxide, 4.5 parts of antimonous oxides, 0.5 part of SODIUMNITRATE, 0.98 part of CuO, 0.02 part of CoO mix;
2) raw material is melted in tank furnace, 1600 ℃ of temperature of fusion, 1700 ℃ of clarifying temps, fusing time 12 hours, settling time 8 hours, obtain glass metal;
3) glass metal melted is cooled to 1200 ℃, according to design shape, manually is shaped, the artificial shaping is specially: artificial feeding, by instruments such as scissors, handle, blowpipe, moulds, through processes such as manually blowing, draw, press, turn, squeeze, make coloured glaze become desired shape;
4) goods after being shaped are sent into annealing in annealing furnace, and 480 ℃ of annealing temperatures slowly cool to room temperature after being incubated 2 hours, obtain product.
comparative Examples 3
1) take each raw material: 93 parts of quartz sands, 46 parts of soda ash, 9 parts of aluminium sesquioxides, 50 parts of plumbic oxide, 1 part of cerium dioxide, 4.1 parts of antimonous oxides, 0.1 part of SODIUMNITRATE, Cr
2o
31.2 0.3 part of part, CuO, mix;
2) raw material is melted in tank furnace, 1650 ℃ of temperature of fusion, 1660 ℃ of clarifying temps, fusing time 14 hours, settling time 7 hours, obtain glass metal;
3) glass metal melted is cooled to 1200 ℃, according to design shape, manually is shaped, the artificial shaping is specially: artificial feeding, by instruments such as scissors, handle, blowpipe, moulds, through processes such as manually blowing, draw, press, turn, squeeze, make coloured glaze become desired shape;
4) goods after being shaped are sent into annealing in annealing furnace, and 520 ℃ of annealing temperatures slowly cool to room temperature after being incubated 3 hours, obtain product.
comparative Examples 4
1) take each raw material: 93 parts of quartz sands, 46 parts of soda ash, 9 parts of aluminium sesquioxides, 50 parts of plumbic oxide, 1.55 parts of cerium dioxides, 3 parts of antimonous oxides, 0.1 part of SODIUMNITRATE, Cr
2o
31.2 0.3 part of part, CuO, mix;
2) raw material is melted in tank furnace, 1650 ℃ of temperature of fusion, 1660 ℃ of clarifying temps, fusing time 14 hours, settling time 7 hours, obtain glass metal;
3) glass metal melted is cooled to 1200 ℃, according to design shape, manually is shaped, the artificial shaping is specially: artificial feeding, by instruments such as scissors, handle, blowpipe, moulds, through processes such as manually blowing, draw, press, turn, squeeze, make coloured glaze become desired shape;
4) goods after being shaped are sent into annealing in annealing furnace, and 520 ℃ of annealing temperatures slowly cool to room temperature after being incubated 3 hours, obtain product.
embodiment 9 colored glaze product attribute tests
1, with PCY type high-temperature horizontal dilatometer, in 20-30 ℃ of scope, detect coefficient of linear expansion;
2, with the softening point measurement standard method of ASTMC-338-57, BLR-II glass softening point determinator, under normal temperature and pressure conditions, detect softening temperature (10
6.7temperature during Pas);
3, appearance quality detection: randomly draw 100 goods prepared by each embodiment, there is striped goods number in statistics, sense organ evaluation and test goods transparency, bubble degree, glossiness.The evaluation and test of transparency, bubble degree, glossiness all adopts ten point system, by 10 coloured glaze industry personages, each goods is given a mark, and marks higher, and quality is better.
Embodiment 1-8 and Comparative Examples 1-4 colored glaze product attribute test result are as shown in table 1.Result shows, in the coloured glaze preparation process, simple cerium dioxide or the antimonous oxide of using is as finings, its clarifying effect is limited, and goods transparency, bubble degree, glossiness are not satisfactory, and the striped number of articles is more, and the present invention is used in conjunction with cerium dioxide and antimonous oxide, the transparency of goods, bubble degree, glossiness etc. all significantly are better than using merely cerium dioxide or antimonous oxide as finings (P≤0.05), have significantly improved quality product, and have provided cost savings.Find, the ratio control of cerium dioxide and antimonous oxide is at 1:(2-4 simultaneously) best results in scope.
Table 1 embodiment 1-8 and Comparative Examples 1-4 colored glaze product attribute test result
| ? | Coefficient of linear expansion (/ ℃) | Softening temperature (℃) | Striped goods number | Transparency | The bubble degree | Glossiness |
| Embodiment 1 | 106×10 -7 | 525 | 0 | 9.7 | 9.8 | 9.9 |
| Embodiment 2 | 102×10 -7 | 527 | 1 | 9.4 | 9.6 | 9.5 |
| Embodiment 3 | 104×10 -7 | 529 | 2 | 9.3 | 9.5 | 9.4 |
| Embodiment 4 | 103×10 -7 | 529 | 3 | 9.3 | 9.4 | 9.3 |
| Embodiment 5 | 101×10 -7 | 531 | 1 | 9.4 | 9.4 | 9.5 |
| Embodiment 6 | 101×10 -7 | 530 | 2 | 9.5 | 9.4 | 9.5 |
| Embodiment 7 | 103×10 -7 | 528 | 0 | 9.6 | 9.5 | 9.6 |
| Embodiment 8 | 101×10 -7 | 528 | 1 | 9.4 | 9.3 | 9.5 |
| Comparative Examples 1 | 99×10 -7* | 530 | 9* | 7.9* | 7.9* | 8.0* |
| Comparative Examples 2 | 102×10 -7 | 531 | 9* | 7.9* | 8.0* | 7.9* |
| Comparative Examples 3 | 102×10 -7 | 532 | 10* | 8.0* | 7.6* | 7.5* |
| Comparative Examples 4 | 104×10 -7 | 532 | 11* | 7.8* | 7.9* | 7.4* |
Annotate: coefficient of linear expansion, softening temperature, transparency, bubble degree, glossiness are the mean value of 100 product test values; * represent P≤0.05.
The above is only the preferred embodiment of the present invention; it should be pointed out that for those skilled in the art, under the prerequisite that does not break away from the inventive method; can also make some improvement and supplement, these improvement and supplement and also should be considered as protection scope of the present invention.
Claims (4)
1. the coloured glaze that clarifying effect is good, product property is good, it is characterized in that, described coloured glaze is made by the raw material of following weight part: quartz sand 93-105 part, soda ash 42-46 part, aluminium sesquioxide 9-13 part, plumbic oxide 45-50 part, cerium dioxide 1-1.5 part, antimonous oxide 3-4 part, SODIUMNITRATE 0.1-0.5 part, pigment 1-1.5 part.
2. coloured glaze according to claim 2, it is characterized in that, described coloured glaze is made by the raw material of following weight part: quartz sand 98-100 part, soda ash 45-46 part, aluminium sesquioxide 10-12 part, plumbic oxide 48-50 part, cerium dioxide 1-1.2 part, antimonous oxide 3-3.5 part, SODIUMNITRATE 0.1-0.5 part, pigment 1-1.5 part.
3. coloured glaze according to claim 3, it is characterized in that, described coloured glaze formula is made by the raw material of following weight part: 99 parts of quartz sands, 45 parts of soda ash, 10 parts of aluminium sesquioxides, 49 parts of plumbic oxide, 1 part of cerium dioxide, 3.5 parts of antimonous oxides, 0.4 part of SODIUMNITRATE, pigment 1-1.5 part.
4. according to the arbitrary described coloured glaze of claim 1-3, it is characterized in that, described pigment is Cr
2o
3, CuO, CoO, Mn
2o
3and TiO
2in one or more.
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| CN105271739A (en) * | 2015-09-30 | 2016-01-27 | 太仓市双凤镇薄彩工艺品厂 | High-quality colored glaze |
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| CN105198216A (en) * | 2015-10-30 | 2015-12-30 | 太仓市双凤镇薄彩工艺品厂 | Formula for manufacturing colored glaze ornaments |
| CN105254175A (en) * | 2015-10-30 | 2016-01-20 | 太仓市双凤镇薄彩工艺品厂 | Colored glaze formula for producing colored glaze pendant |
| CN105254178A (en) * | 2015-10-30 | 2016-01-20 | 太仓市双凤镇薄彩工艺品厂 | Formula of colored glaze artware |
| CN105254177A (en) * | 2015-10-30 | 2016-01-20 | 太仓市双凤镇薄彩工艺品厂 | Colored glaze formula for firing colored glaze handicraft |
| CN105271732A (en) * | 2015-10-30 | 2016-01-27 | 太仓市双凤镇薄彩工艺品厂 | Colored glaze formula for fabricating colored glaze craftworks |
| CN105271742A (en) * | 2015-10-30 | 2016-01-27 | 太仓市双凤镇薄彩工艺品厂 | High-cleanliness colored glaze |
| CN105271731A (en) * | 2015-10-30 | 2016-01-27 | 太仓市双凤镇薄彩工艺品厂 | Colored glaze recipe |
| CN106045312A (en) * | 2016-08-08 | 2016-10-26 | 太仓市双凤镇薄彩工艺品厂 | High-fineness colored glaze |
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Application publication date: 20131225 |