CN103463284A - Gynecological cleaning liquid and preparation method thereof - Google Patents
Gynecological cleaning liquid and preparation method thereof Download PDFInfo
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- CN103463284A CN103463284A CN2013104167432A CN201310416743A CN103463284A CN 103463284 A CN103463284 A CN 103463284A CN 2013104167432 A CN2013104167432 A CN 2013104167432A CN 201310416743 A CN201310416743 A CN 201310416743A CN 103463284 A CN103463284 A CN 103463284A
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Abstract
The invention discloses gynecological cleaning liquid and a preparation method thereof. The cleaning liquid is prepared from the following raw materials in parts by weight: 7-13 parts of radix sophorae flavescentis, 7-13 parts of fructus cnidii, 6-12 parts of cortex phellodendri, 5-9 parts of senecio, 1-5 parts of savatier monochasma herb, 2-6 parts of folium artemisiae argyi, 0.1-0.5 part of menthol, 0.3-0.8 part of borneol, 0.06-0.15 part of chlorhexidine acetate and 0.1-0.3 part of vitamin E. By means of reasonable compatibility and mutual cooperation of traditional Chinese medicine and Western medicine, the gynecological cleaning liquid has no irritation or side effect, and not only has the functions of being antimicrobial and insecticidal, dispelling pathogenic wind, removing dampness, clearing away heat and toxic materials, relieving itching, diminishing inflammation, cooling blood to remove stasis, and the like, but also capable of treating both manifestation and root cause of disease to prevent easy relapse after cure;,the gynecological cleaning liquid has a humectation function and can greatly reduce the dry and burning feelings generated after the medicine is adopted and improve the use comfort.
Description
Technical field
The present invention relates to a kind of cleaning fluid for gynecology and preparation method thereof.
Background technology
At present, the prevalence of gynaecopathia is higher, such as the gynaecopathias such as vaginitis, cervicitis, cervical erosion are the women of child-bearing age's commonly encountered diseases, frequently-occurring disease, and the trend risen arranged year by year now, though gynaecopathia is so not serious than sexually transmitted disease (STD), but brought painful topic to the women, had a strong impact on people's quality of life and family harmony.At present, the washing liquid that is used for the treatment of gynaecopathia is more, mainly comprises Chinese medicine lotion and the large class of Western medicine lotion two, but all there is shortcoming separately in two kinds of lotions, for example the Chinese medicine lotion efficacy of a drug a little less than, treatment time is long, and Western medicine lotion drug component is few, acts on single, easily produce zest, and Chinese medicine lotion and Western medicine lotion all are easy to cause recurrence, and all have the longer shortcoming course for the treatment of after drug withdrawal.
Application publication number: CN102697961A, the Chinese patent of Shen Qing Publication day: 2012.10.03 discloses a kind of cleaning fluid for gynecology, this cleanout fluid is made by following raw material: Radix Sophorae Flavescentis, Cortex Phellodendri, Indigo Naturalis, Borax, Fructus Forsythiae, Pericarpium Zanthoxyli, Radix Scutellariae, Herba Solani Nigri, Fructus Cnidii, Cortex Dictamni, the Fructus Kochiae, Borneolum Syntheticum, hibitane, by the Radix Sophorae Flavescentis in above-mentioned raw materials, Cortex Phellodendri, Indigo Naturalis, Borax, Fructus Forsythiae, Pericarpium Zanthoxyli, Radix Scutellariae, Herba Solani Nigri, Fructus Cnidii, Cortex Dictamni, the Fructus Kochiae is put into container, add water, then be heated to boiling, decoct 50-60 minute with little fire again, finally filter out decoction liquor, cooling to room temperature adds Borneolum Syntheticum and hibitane to dissolve and mix homogeneously, obtain described cleaning fluid for gynecology.This cleaning fluid for gynecology strengthens drug effect by the mode of Chinese medicine and western medicine compatibility, although can reach fast the purpose for the treatment of, western medicine composition wherein can produce zest to pathogenic site, after use, can make vagina produce burning sensation, and cause dry and astringent; In addition, this cleaning fluid for gynecology only has the effect of sterilization, antipruritic, antiinflammatory, and the effect of conditioning, namely just do not cure the symptoms, not the disease, once drug withdrawal is easy to cause the recurrence of gynaecopathia.
Summary of the invention
The present invention is the existing the problems referred to above of the cleaning fluid for gynecology in order to solve prior art, and a kind of cleaning fluid for gynecology is provided, and this cleaning fluid for gynecology compatibility is reasonable, and drug effect is long, evident in efficacy, has opsonic action simultaneously, and nonirritant is difficult for recurrence after treatment.
The present invention also provides a kind of preparation method of cleaning fluid for gynecology, and this preparation method processing step is simple, is applicable to suitability for industrialized production, and the cleaning fluid for gynecology drug effect and the result of use that make are good.
To achieve these goals, the present invention is by the following technical solutions:
A kind of cleaning fluid for gynecology, described cleanout fluid is made by the raw material of following weight portion:
7～13 parts of Radix Sophorae Flavescentiss, 7～13 parts of Fructus Cnidiis, 6～12 parts of Cortex Phellodendris, Herba Senecionis Scandentis 5-9 part, 1～5 part of Herba monochasmatis, 2～6 parts of Folium Artemisiae Argyis,
0.1～0.5 part of Mentholum, 0.3～0.8 part of Borneolum Syntheticum, 0.06～0.15 part of chlorhexidine acetate, 0.1～0.3 part of vitamin E.
Preferably, described cleanout fluid is made by the raw material of following weight portion:
10 parts of Radix Sophorae Flavescentiss, 10 parts of Fructus Cnidiis, 9 parts of Cortex Phellodendris, 7 parts of Herba Senecionis Scandentiss, 1 part of Herba monochasmatis, 3 parts of Folium Artemisiae Argyis,
0.25 part of Mentholum, 0.625 part of Borneolum Syntheticum, 0.125 part of chlorhexidine acetate, 0.2125 part of vitamin E.Adopt the prescription of this proportioning to there is optimum properties and resultant effect.
Plant material in the present invention is Radix Sophorae Flavescentis, Fructus Cnidii, Cortex Phellodendri, Herba Senecionis Scandentis, Herba monochasmatis, Folium Artemisiae Argyi, wherein Cortex Phellodendri heat clearing and damp drying, eliminating fire and detoxication; The Radix Sophorae Flavescentis anti-inflammation, Propiobacterium, staphylococcus aureus, escherichia coli are all had to inhibitory action; Fructus Cnidii removing toxic substances parasite killing, dampness are dispeled the wind, Herba Senecionis Scandentis heat-clearing and toxic substances removing, antibacterial parasite killing, Herba monochasmatis heat-clearing and toxic substances removing, cooling blood and removing stasis, swelling diuretic, wind-expelling pain-stopping; Folium Artemisiae Argyi is a kind of natural plants of broad-spectrum antibacterial antiviral, in the present invention, the medicine source of each raw material is abundant, component compatibility is reasonable, and Synergistic, without any side effect and zest, there is heat-clearing and toxic substances removing, the effect of kill virus antipruritic, anti-inflammation, mildew-resistant deodorization, promote the production of body fluid yin nourishing and leukorrhagia stopping, can stimulate the impaired mucosa regeneration of histiocyte or vagina, improve self repair ability and resistance, effectively the immunity of enhancing body self, treating both the principal and secondary aspects of a disease, make the rear difficult recurrence for the treatment of.
Other raw materials in the present invention are Borneolum Syntheticum, Mentholum, chlorhexidine acetate, strengthen drug effect by the mutual synergism with above-mentioned plant material, reach the purpose of fast treating: Borneolum Syntheticum has the refreshment of having one's ideas straightened out, the effect of clearing away heat to alleviate pain, Mentholum has refrigerant skin smoothing, the effect of bactericidal antiphlogistic, chlorhexidine acetate is cationic surfactant, has a broad antifungal spectrum, most Grain-positives and negative bacteria are had to killing action, in addition, also added vitamin E in the present invention, vitamin E plays the effect that reaches skin protection of moistening, can significantly reduce the dry and astringent and burning sensation produced after medication, improve comfort, can also accelerate the reparation of damaged tissues cell and the impaired mucosa of vagina, also skin is had to protective effect simultaneously.
A kind of preparation method of cleaning fluid for gynecology comprises the following steps:
(1) take raw material by described weight portion proportioning, standby;
(2) Radix Sophorae Flavescentis, Fructus Cnidii, Cortex Phellodendri, Herba Senecionis Scandentis, Herba monochasmatis, Folium Artemisiae Argyi are added to 6～8 times of decoctings after mixing and boil 2～6h, filter, obtain the first filtering residue and the first decoction liquor; It is here said that to add 6～8 times of water be in the gross mass of Radix Sophorae Flavescentis, Fructus Cnidii, Cortex Phellodendri, Herba Senecionis Scandentis, Herba monochasmatis, Folium Artemisiae Argyi.
(3) first filtering residues add 3～5 times of decoctings and boil 1～3h, filter, and obtain the second filtering residue and the second decoction liquor; Here said 3～5 times of water are in the first filtering residue quality.
(4) merge the first decoction liquor and the second decoction liquor, after filtration, filtrate being concentrated into to relative density is 1.01～1.02g/cm
3, add 95% ethanol, making containing the alcohol amount is 50～60%, standing over night filters, and after recovery ethanol, obtains refined liquid;
(5) after Borneolum Syntheticum, Mentholum, chlorhexidine acetate, vitamin E are used respectively to 95% dissolve with ethanol, with refined liquid, mix homogeneously, add 95% ethanol dilution to the 1.2-1.5 of concentrated solution doubly, obtain described cleaning fluid for gynecology.
Preferably, in step (2), described Radix Sophorae Flavescentis, Fructus Cnidii, Cortex Phellodendri, Herba Senecionis Scandentis, Herba monochasmatis, Folium Artemisiae Argyi mix after pulverizing and cross 40 mesh sieves.Decocted after pulverizing, be conducive to the extraction of effective ingredient in Chinese medicine.
In sum, beneficial effect of the present invention is: the present invention is by the reasonable compatibility of Chinese medicine and western medicine with mutually collaborative, and nonirritant and side effect, not only have the effects such as antibacterial parasite killing, dispeiling pathogenic wind and removing dampness, heat-clearing and toxic substances removing, itch stopping and diminish inflammation, cooling blood and removing stasis, can reach treating both the principal and secondary aspects of a disease, be difficult for recurrence after treatment; There is humidification, can significantly reduce the dry and astringent and burning sensation produced after medication, improve comfort;
Below effect of the present invention will be described by the result of vaginal mucosa irritation test and clinical trial.
One, vaginal mucosa irritation test
Set up test group, matched group, 10 every group adult healthy SD rats.
Test group: after soaking cleaning fluid for gynecology of the present invention with cotton sliver, cotton sliver is placed in the SD rat vagina and contacts 24h with vaginal mucosa;
Matched group: do not give any processing.
Put to death the SD rat after 24 hours, take out whole vagina, observe hyperemia, the edema reacting phenomenon of local vagina tissue, carry out the irritant reaction evaluation.
Experimental result: the local vagina tissue of test group and matched group SD rat is not all found the abnormal responses such as hyperemia, edema, does not find other symptoms yet, illustrates that the present invention belongs to nonirritant to the vaginal mucosa irritation of SD rat.
Two, clinical trial
1. case is selected
Selected case 216 examples, the patient is all without the other system disease, and do not use antifungal drug in 1 month, and at 23～60 years old age, medical history did not wait to 1 week in 2 years.Cardinal symptom is pruritus vulvae, leucorrhoea grow in quantity, pain, visible pudendum and vaginal mucosa hyperemia during inspection, visible infusorian or fungus when infusorian property or colpitis mycotica patient vaginal secretions microscopy, bacterial vaginitis BV checks positive, the patient of every kind of case is divided into to two groups, wherein one group is used cleaning fluid for gynecology of the present invention as test group, and the gynaecologic washing lotion " woman's inflammation is clean " that the commercially available Renhe Pharmaceutical of another group use is produced as a control group.
2. using method
Vaginadouche, directly pour into vaginal douche by cleaning fluid for gynecology of the present invention, then inserts the vagina extrusion bottle and rinsed, rinse every day 2 times, and each 2～3min, continuous 5 days is a course for the treatment of, uses a post-evaluation course for the treatment of curative effect.
3. curative effect judgement
Recovery from illness: subjective symptoms disappears, vagina cleanness degree (I), and vaginal swab is cultivated and is turned out cloudy, and after 4 menstruations, check is all negative;
Effectively: subjective symptoms alleviates, vagina cleanness degree (II), and vaginal swab is cultivated only has the minority bacterial growth, and accidental infusorian or mycete, be no more than at most 10, and 2 positives of check after 4 menstruations;
Invalid: subjective symptoms is without improvement, and vagina cleanness degree is unchanged, and vaginal swab is cultivated unchanged.
4. therapeutic outcome
From the therapeutic outcome of clinical trial, the present invention all has good curative effect to various vaginitiss, and its curative effect will obviously be better than commercially available to product, in addition, sufferer has no obvious untoward reaction during medication, non-stimulated to vaginal mucosa, also has no anaphylaxis, and after on probation, the patient feels comfortable, the affected part healing is fast, and only need 6 days the course for the treatment of, with existing like product, compares the course for the treatment of of at least 12 days, shorten the course for the treatment of, takes effect faster.
Below will by the specific embodiment, the present invention is described further.
The specific embodiment
Method in following embodiment, if no special instructions, be this area conventional method, and all raw materials are all commercially available.
Embodiment 1:
The proportioning raw materials of described cleanout fluid is: Radix Sophorae Flavescentis 100g, Fructus Cnidii 100g, Cortex Phellodendri 90g, Herba Senecionis Scandentis 70g, Herba monochasmatis 10g, Folium Artemisiae Argyi 30g; Borneolum Syntheticum 6.25g, Mentholum 2.5g, chlorhexidine acetate 1.25g, vitamin E2 .125g.Lab scale craft amplifies 50 times according to this proportional quantity and carries out.
Its preparation method comprises the following steps:
(1) take raw material by said ratio, standby;
(2) Radix Sophorae Flavescentis, Fructus Cnidii, Cortex Phellodendri, Herba Senecionis Scandentis, Herba monochasmatis, Folium Artemisiae Argyi are added to 8 times of decoctings after mixing and boil 2h, filter, obtain the first filtering residue and the first decoction liquor; It is here said that to add 8 times of water be in the gross mass of Radix Sophorae Flavescentis, Fructus Cnidii, Cortex Phellodendri, Herba Senecionis Scandentis, Herba monochasmatis, Folium Artemisiae Argyi.
(3) first filtering residues add 5 times of decoctings and boil 1h, filter, and obtain the second filtering residue and the second decoction liquor; Here said 5 times of water are in the first filtering residue quality.
(4) merge the first decoction liquor and the second decoction liquor, after filtration, filtrate being concentrated into to the 1000ml(relative density is 1.01～1.02g/cm
3), add 95% ethanol, making containing the alcohol amount is 50～60%, standing over night filters, and after recovery ethanol, obtains refined liquid;
(5) after Borneolum Syntheticum, Mentholum, chlorhexidine acetate, vitamin E are used respectively to 95% dissolve with ethanol, with refined liquid, mix homogeneously, add 95% ethanol to be diluted to 1250ml.Obtain described cleaning fluid for gynecology.
Embodiment 2-6 is the different of proportioning raw materials and concrete technology parameter from the difference of embodiment 1, refers to following table 1 and table 2:
Proportioning raw materials (the unit: g) of cleaning fluid for gynecology in table 1 embodiment 2-6
| Raw material | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Embodiment 6 |
| Radix Sophorae Flavescentis | 70 | 80 | 90 | 110 | 130 |
| Fructus Cnidii | 90 | 70 | 80 | 130 | 120 |
| Cortex Phellodendri | 80 | 60 | 70 | 110 | 120 |
| Herba Senecionis Scandentis | 50 | 60 | 70 | 80 | 90 |
| Herba monochasmatis | 20 | 30 | 40 | 45 | 50 |
| Folium Artemisiae Argyi | 20 | 40 | 50 | 60 | 58 |
| Borneolum Syntheticum | 3 | 4.2 | 5 | 7.3 | 8 |
| Mentholum | 2 | 1 | 3.2 | 4.2 | 5 |
| Chlorhexidine acetate | 0.6 | 0.8 | 1 | 1.3 | 1.5 |
| Vitamin E | 1 | 1.9 | 3 | 1.5 | 2.5 |
The technological parameter of production method in table 2 embodiment 2-6
Above-described embodiment is just in order at length to set forth the present invention; and can not be interpreted as limiting the scope of the invention, in field known in this field, it exists multiple replacement scheme or variation; under the prerequisite without prejudice to essential meaning of the present invention, all fall into protection scope of the present invention.
Claims (4)
1. a cleaning fluid for gynecology, it is characterized in that, described cleanout fluid is made by the raw material of following weight portion: 7～13 parts of Radix Sophorae Flavescentiss, 7～13 parts of Fructus Cnidiis, 6～12 parts of Cortex Phellodendris, 5～9 parts of Herba Senecionis Scandentiss, 1～5 part of Herba monochasmatis, 2～6 parts of Folium Artemisiae Argyis, 0.1～0.5 part of Mentholum, 0.3～0.8 part of Borneolum Syntheticum, 0.06～0.15 part of chlorhexidine acetate, 0.1～0.3 part of vitamin E.
2. a kind of cleaning fluid for gynecology as claimed in claim 1, it is characterized in that, described cleanout fluid is made by the raw material of following weight portion: 10 parts of Radix Sophorae Flavescentiss, 10 parts of Fructus Cnidiis, 9 parts of Cortex Phellodendris, 7 parts of Herba Senecionis Scandentiss, 1 part of Herba monochasmatis, 3 parts of Folium Artemisiae Argyis, 0.25 part of Mentholum, 0.625 part of Borneolum Syntheticum, 0.125 part of chlorhexidine acetate, 0.2125 part of vitamin E.
3. the preparation method of a cleaning fluid for gynecology, is characterized in that, comprises the following steps:
(1) take raw material by described weight portion proportioning, standby;
(2) Radix Sophorae Flavescentis, Fructus Cnidii, Cortex Phellodendri, Herba Senecionis Scandentis, Herba monochasmatis, Folium Artemisiae Argyi are added to 6～8 times of decoctings after mixing and boil 2～6h, filter, obtain the first filtering residue and the first decoction liquor;
(3) first filtering residues add 3～5 times of decoctings and boil 1～3h, filter, and obtain the second filtering residue and the second decoction liquor;
(4) merge the first decoction liquor and the second decoction liquor, after filtration, filtrate being concentrated into to relative density is 1.01～1.02g/cm
3, add 95% ethanol, making containing the alcohol amount is 50～60%, standing over night filters, and after recovery ethanol, obtains refined liquid;
(5) after Borneolum Syntheticum, Mentholum, chlorhexidine acetate, vitamin E are used respectively to 95% dissolve with ethanol, with refined liquid, mix homogeneously, add 95% ethanol dilution to the 1.2-1.5 of concentrated solution doubly, obtain described cleaning fluid for gynecology.
4. the preparation method of as claimed in claim 3 kind of cleaning fluid for gynecology, is characterized in that, in step (2), described Radix Sophorae Flavescentis, Fructus Cnidii, Cortex Phellodendri, Herba Senecionis Scandentis, Herba monochasmatis, Folium Artemisiae Argyi mix after pulverizing and cross 40 mesh sieves.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105031077A (en) * | 2015-09-08 | 2015-11-11 | 南京正亮医药科技有限公司 | Liquid medicine used for nursing and cleaning gynaecological vulva |
| CN105311328A (en) * | 2015-11-19 | 2016-02-10 | 南方医科大学 | Traditional Chinese medicine composition for treating gynecological inflammation and application thereof |
| CN105326950A (en) * | 2015-12-04 | 2016-02-17 | 武汉璟泓万方堂医药科技股份有限公司 | Lotion for treating gynecologic inflammation |
| CN105521385A (en) * | 2016-01-13 | 2016-04-27 | 山东康富森生物科技有限公司 | Gel for department of gynecology and preparation method of gel |
| CN106511568A (en) * | 2016-12-21 | 2017-03-22 | 南通华津医药保健品有限公司 | Antibacterial lotion achieving skin and vagina cleanliness and preparation method and application thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105031077A (en) * | 2015-09-08 | 2015-11-11 | 南京正亮医药科技有限公司 | Liquid medicine used for nursing and cleaning gynaecological vulva |
| CN105311328A (en) * | 2015-11-19 | 2016-02-10 | 南方医科大学 | Traditional Chinese medicine composition for treating gynecological inflammation and application thereof |
| CN105311328B (en) * | 2015-11-19 | 2019-03-05 | 南方医科大学 | A kind of Chinese medicine composition that treating gynaecological imflammation and its application |
| CN105326950A (en) * | 2015-12-04 | 2016-02-17 | 武汉璟泓万方堂医药科技股份有限公司 | Lotion for treating gynecologic inflammation |
| CN105521385A (en) * | 2016-01-13 | 2016-04-27 | 山东康富森生物科技有限公司 | Gel for department of gynecology and preparation method of gel |
| CN106511568A (en) * | 2016-12-21 | 2017-03-22 | 南通华津医药保健品有限公司 | Antibacterial lotion achieving skin and vagina cleanliness and preparation method and application thereof |
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| CN103463284B (en) | 2015-04-08 |
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