CN103450710A - Coated flame-retardant iron oxide blue - Google Patents
Coated flame-retardant iron oxide blue Download PDFInfo
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- CN103450710A CN103450710A CN2013103613703A CN201310361370A CN103450710A CN 103450710 A CN103450710 A CN 103450710A CN 2013103613703 A CN2013103613703 A CN 2013103613703A CN 201310361370 A CN201310361370 A CN 201310361370A CN 103450710 A CN103450710 A CN 103450710A
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Abstract
The invention discloses coated flame-retardant iron oxide blue. The coated flame-retardant iron oxide blue is prepared from the following raw materials in parts by weight: 250-300 parts of iron oxide blue, 10-20 parts of coated flame-retardant aluminum hydroxide, 2-4 parts of polytrimethyl dihydroquinoline, 10-15 parts of acetone, 2-4 parts of silicone oil with high hydrogen content, 0.3-0.4 part of coconut oil fatty acid diethanolamide, 2-4 parts of silane coupling agent a171, 1-2 parts of decabromodiphenyl ethane, 0.5-0.8 part of alkylethoxyglucoside, 0.2-0.4 part of sodium lauryl ether sulfate and 0.1-0.2 part of zinc sulfide.
Description
Technical field
The present invention relates to the iron oxide blue field, is exactly the fire-retardant iron oxide blue of a kind of coating.
Background technology
Iron oxide blue is mazarine and light blue powder, lovely luster, and strong coloring force, opacifying power is slightly poor.Opaque is harder.Quality standard: tinting strength 95 ~ 105% oil number 15-30% moisture content 1.0%, screenings (200 mesh sieve)≤1.0%, the water solubles 1.0%.
Summary of the invention
The object of the present invention is to provide the fire-retardant iron oxide blue of a kind of coating
Above-mentioned purpose realizes by following scheme:
The fire-retardant iron oxide blue of a kind of coating, it is characterized in that: it is that raw material by following weight parts makes: iron oxide blue 250-300, coat fire-retardant aluminium hydroxide 10-20, the poly-high containing hydrogen silicone oil 2-4 of trimethyldihydroquinoline 2-4, acetone 10-15., cocoanut fatty acid diethanolamide 0.3-0.4, silane coupling agent a171 2-4, decabromodiphenyl ethane 1-2, alcohol ether glucoside 0.5-0.8, laureth sodium sulfovinate 0.2-0.4, zinc sulphide 0.1-0.2.
The fire-retardant iron oxide blue of described a kind of coating, it is characterized in that: the preparation method comprises the following steps:
(1) get by weight aluminium hydroxide, add again the titanate coupling agent TMC-201 that is equivalent to aluminium hydroxide weight 0.4-0.8%, the epoxy oleum lini of 1.3-1.5%, the aluminum oxide of 0.4-0.5%, and appropriate amount of deionized water, under 1000-1200rpm, after high speed shear 10-15 minute, take out, drying, must coat fire-retardant aluminium hydroxide standby;
(2) will except the oxidation barba hispanica, mix by weight by all the other raw materials, add appropriate amount of deionized water, after stirring, obtain modification liquid standby;
(3) modification liquid and iron oxide blue are mixed by weight, high speed shear 20-30 minute under 800-1000rpm, take out, and dries, and the gained powder utilizes the roller milling machine to carry out wet-milling, and wet grinding media is dehydrated alcohol, and mill ball is sintered carbide ball;
(4) by the slurry vacuum-drying after the gained wet-milling and get final product.
Beneficial effect of the present invention is: the present invention has fire-retardant, acid and alkali-resistance, uvioresistant, chemical solvent resistance.Coat fire-retardant aluminium hydroxide by modification, increased its flame retardant effect, itself and iron oxide blue can combine more closely.
Embodiment
The fire-retardant iron oxide blue of a kind of coating, it is that raw material by following weight parts (kg) makes: iron oxide blue 300, coat fire-retardant aluminium hydroxide 20, poly-trimethyldihydroquinoline 4, the high containing hydrogen silicone oil 4 of acetone 15., cocoanut fatty acid diethanolamide 0.3, silane coupling agent a171 4, decabromodiphenyl ethane 2, alcohol ether glucoside 0.8, laureth sodium sulfovinate 0.4, zinc sulphide 0.2.
The fire-retardant iron oxide blue of described a kind of coating, the preparation method comprises the following steps:
(1) get by weight aluminium hydroxide, add again the titanate coupling agent TMC-201 that is equivalent to aluminium hydroxide weight 0.8%, 1.5% epoxy oleum lini, 0.5% aluminum oxide, and appropriate amount of deionized water, under 1200rpm, high speed shear, after 15 minutes, is taken out, drying, must coat fire-retardant aluminium hydroxide standby;
(2) will except the oxidation barba hispanica, mix by weight by all the other raw materials, add appropriate amount of deionized water, after stirring, obtain modification liquid standby;
(3) modification liquid and iron oxide blue are mixed by weight, under 800rpm, high speed shear is 25 minutes, takes out, and dries, and the gained powder utilizes the roller milling machine to carry out wet-milling, and wet grinding media is dehydrated alcohol, and mill ball is sintered carbide ball;
(4) by the slurry vacuum-drying after the gained wet-milling and get final product.
The iron oxide blue product performance analytical data that the present embodiment is produced is as following table:
| Project | Index | Detected result |
| 105 ℃ of volatile matters (%) | ≤1.0 | 0.82 |
| Oil number (%) | 15-25 | 21.9 |
| Tinctorial strength (%) | 95-105 | 98.7 |
| Anti-200 ℃/30min (△ E) | ≤1.0 | 0.83 |
Claims (2)
1. one kind coats fire-retardant iron oxide blue, it is characterized in that: it is that raw material by following weight parts makes: iron oxide blue 250-300, coat fire-retardant aluminium hydroxide 10-20, the poly-high containing hydrogen silicone oil 2-4 of trimethyldihydroquinoline 2-4, acetone 10-15., cocoanut fatty acid diethanolamide 0.3-0.4, silane coupling agent a171 2-4, decabromodiphenyl ethane 1-2, alcohol ether glucoside 0.5-0.8, laureth sodium sulfovinate 0.2-0.4, zinc sulphide 0.1-0.2.
2. the fire-retardant iron oxide blue of a kind of coating according to claim 1, it is characterized in that: the preparation method comprises the following steps:
(1) get by weight aluminium hydroxide, add again the titanate coupling agent TMC-201 that is equivalent to aluminium hydroxide weight 0.4-0.8%, the epoxy oleum lini of 1.3-1.5%, the aluminum oxide of 0.4-0.5%, and appropriate amount of deionized water, under 1000-1200rpm, after high speed shear 10-15 minute, take out, drying, must coat fire-retardant aluminium hydroxide standby;
(2) will except the oxidation barba hispanica, mix by weight by all the other raw materials, add appropriate amount of deionized water, after stirring, obtain modification liquid standby;
(3) modification liquid and iron oxide blue are mixed by weight, high speed shear 20-30 minute under 800-1000rpm, take out, and dries, and the gained powder utilizes the roller milling machine to carry out wet-milling, and wet grinding media is dehydrated alcohol, and mill ball is sintered carbide ball;
(4) by the slurry vacuum-drying after the gained wet-milling and get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310361370.3A CN103450710B (en) | 2013-08-19 | 2013-08-19 | A kind of coated fire-retardant iron oxide blue |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310361370.3A CN103450710B (en) | 2013-08-19 | 2013-08-19 | A kind of coated fire-retardant iron oxide blue |
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| Publication Number | Publication Date |
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| CN103450710A true CN103450710A (en) | 2013-12-18 |
| CN103450710B CN103450710B (en) | 2016-05-18 |
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| CN201310361370.3A Active CN103450710B (en) | 2013-08-19 | 2013-08-19 | A kind of coated fire-retardant iron oxide blue |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1103088A (en) * | 1993-07-09 | 1995-05-31 | 拜尔公司 | Thermally stable iron oxide pigments, a process for their preparation and their use |
| CN103012854A (en) * | 2012-12-31 | 2013-04-03 | 青岛海诺中天节能科技有限公司 | Inorganic flame retardant for wrapping polystyrene granules |
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| DE3038328A1 (en) * | 1980-10-10 | 1982-05-06 | Degussa Ag, 6000 Frankfurt | IRON BLUE PIGMENT, METHOD FOR PRODUCING THE SAME AND USE |
| CN1252191C (en) * | 2004-07-14 | 2006-04-19 | 山西大学 | Process for the preparation of iron blue |
| CN1314778C (en) * | 2005-03-04 | 2007-05-09 | 北京化工大学 | Process for preparing nano inorganic compound flame retardant by transfer method |
| DE102006008244A1 (en) * | 2006-02-22 | 2007-09-06 | Giesecke & Devrient Gmbh | Printing ink for security printing |
| CN101760083B (en) * | 2009-03-20 | 2012-04-11 | 苏州世名科技股份有限公司 | Water and oil applicable iron oxide color paste |
| CN101942273B (en) * | 2010-08-19 | 2013-03-20 | 福建瑞森化工有限公司 | Anti-explosive splattering paint and preparation method thereof |
| CN102443285B (en) * | 2011-09-05 | 2013-07-24 | 福州坤彩精化有限公司 | Prussian blue pearlescent pigment and preparation method thereof |
| CN102924978A (en) * | 2012-10-19 | 2013-02-13 | 福州坤彩精化有限公司 | Magnetic Prussian blue pigment and preparation method thereof |
| CN102942895B (en) * | 2012-11-15 | 2016-03-02 | 烟台德邦科技有限公司 | A kind of heat conductive electronic pouring sealant and preparation method thereof |
| CN103131298B (en) * | 2013-02-03 | 2016-03-02 | 倪进培 | A kind of Flame Retardant Powder Coatings containing hydration zinc borate |
| CN103102134B (en) * | 2013-02-20 | 2015-08-05 | 上海宏胜电线电缆有限公司 | Fire protection flame retarding mineral chemical combination inserts and the cable containing this mineral chemical combination inserts |
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2013
- 2013-08-19 CN CN201310361370.3A patent/CN103450710B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1103088A (en) * | 1993-07-09 | 1995-05-31 | 拜尔公司 | Thermally stable iron oxide pigments, a process for their preparation and their use |
| CN103012854A (en) * | 2012-12-31 | 2013-04-03 | 青岛海诺中天节能科技有限公司 | Inorganic flame retardant for wrapping polystyrene granules |
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| CN103450710B (en) | 2016-05-18 |
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