CN103446033A - Propolis health care toothpaste - Google Patents
Propolis health care toothpaste Download PDFInfo
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- CN103446033A CN103446033A CN2013103746936A CN201310374693A CN103446033A CN 103446033 A CN103446033 A CN 103446033A CN 2013103746936 A CN2013103746936 A CN 2013103746936A CN 201310374693 A CN201310374693 A CN 201310374693A CN 103446033 A CN103446033 A CN 103446033A
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- propolis
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- care toothpaste
- toothpaste
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Abstract
The invention relates to propolis health care toothpaste. The propolis health care toothpaste comprises the following components in percentage by weight: 0.6 to 1.0% of propolis, 0.4 to 0.8% of D-panthenol, 30 to 40% of silicon dioxide, 8 to 16% of glycerinum, 12 to 16% of sorbitol, 1.6 to 2.4% of sodium lauroyl sarcosine, 0.1 to 0.3% of hydroxyethyl cellulose, 0.4 to 0.8% of hydroxymethyl cellulose and the balance of water. The propolis health care toothpaste has a good protection effect on teeth, can nourish gingiva and prevent gingivitis, and also ensures the comfort of a mouth during use.
Description
Technical field
The present invention relates to a kind of toothpaste, be specifically related to a kind of propolis health care toothpaste.
Background technology
Toothpaste is to be used from cleaning teeth with toothbrush one, and the protection oral hygiene, to a kind of daily necessities of human-body safety.Along with the raising of people's living standard, to the also progressively raising of quality requirement of toothpaste.At aspect of performance General Requirements toothpaste: (1) can remove the thin film of dental surface and bacterial plaque and not damage enamel and dentin; (2) there is good cleaning oral cavity and effect on every side thereof; (3) avirulence, non-stimulated to oral mucosa; (4) comfortable fragrance and taste are arranged, cool and sweet-smelling sensation is arranged after use.
Summary of the invention
For above shortcomings in prior art, technical problem to be solved by this invention is to provide a kind of propolis health care toothpaste.
The present invention seeks to be achieved through the following technical solutions:
A kind of propolis health care toothpaste, by following compositions in weight percentage, formed: the 0.6-1.0% propolis, the 0.4-0.8%D-pantothenylol, 30-40% silicon dioxide, 8-16% glycerol, 12-16% sorbitol, the 1.6-2.4% sodium lauroyl sarcosine, the 0.1-0.3% hydroxyethyl-cellulose, the 0.4-0.8% hydroxy methocel, surplus is water.
Preferably,
A kind of propolis health care toothpaste, by following compositions in weight percentage, formed: the 0.6-1.0% propolis, the 0.4-0.8%D-pantothenylol, 30-40% silicon dioxide, 8-16% glycerol, the 12-16% sorbitol, the 1.6-2.4% sodium lauroyl sarcosine, 0.1-0.3% hydroxyethyl-cellulose, 0.4-0.8% hydroxy methocel, the 1-3% whitening agent, surplus is water.
Described whitening agent is a kind of or its mixture in sodium phytate, aloin, glycyrrhizin and glucoseoxidase.
Best, described whitening agent consists of by weight following component: 40-60 part sodium phytate, 10-20 part aloin, 10-20 part glycyrrhizin and 15-25 part glucoseoxidase.
In the present invention,
Sodium phytate, English name: Sodium phytate, CAS accession number: 14306-25-3.
Aloin, English name: Aloin, CAS accession number: 5133-19-7.
Glycyrrhizin, English name: Glycyrrhizic acid, CAS accession number: 1405-86-3.
Glucoseoxidase, No. CAS: 9001-37-0, name of commodity in English: EC1.1.3.4, EINECS:232-601-0.
Propolis health care toothpaste of the present invention has protective effect preferably for tooth, but also can nourish gingiva, and the generation of prevention of gingivitis disease also can make oral sensation comfortable in the process of using.
The specific embodiment
Embodiment 1
A kind of propolis health care toothpaste is comprised of following compositions in weight percentage: 0.8% propolis, 0.6%D-pantothenylol, 35% silicon dioxide, 12% glycerol, 14% sorbitol, 2% sodium lauroyl sarcosine, 0.2% hydroxyethyl-cellulose, 0.6% hydroxy methocel, 2% whitening agent, surplus is water.
Described whitening agent consists of by weight following component: 50 parts of sodium phytates, 15 parts of aloins, 15 parts of glycyrrhizins and 20 parts of glucoseoxidases.
Propolis health care toothpaste of the present invention can adopt the conventional method preparation of this area fully, as " detergent compositions workshop manual ", (Xu Baocai etc. write, Chemical Industry Press, chemistry and applied chemistry publishing centre, January in 2006 the 1st edition) the disclosed toothpaste production technology of 594-597 page is prepared.Concrete, the preparation method of the present embodiment propolis health care toothpaste is: after the above-mentioned raw materials component is weighed, disperse in pre-dispersed still, mix, open cream still vacuum pump processed and suck above-mentioned liquid material, then open scraper, agitator and colloid mill, close colloid mill, agitator and scraper successively after 50 minutes, vacuum breaker, obtain propolis health care toothpaste.
Obviously, the preparation method of toothpaste is prior art in the present invention, does not have special character, and main improvement of the present invention just is the difference of formula.
Embodiment 2
A kind of propolis health care toothpaste is comprised of following compositions in weight percentage: 0.8% propolis, 0.6%D-pantothenylol, 35% silicon dioxide, 12% glycerol, 14% sorbitol, 2% sodium lauroyl sarcosine, 0.2% hydroxyethyl-cellulose, 0.6% hydroxy methocel, 2% whitening agent, surplus is water.
Described whitening agent consists of by weight following component: 50 parts of sodium phytates, 15 parts of aloins and 20 parts of glucoseoxidases.
According to the preparation method of embodiment 1, obtain the propolis health care toothpaste of embodiment 2.
Embodiment 3
A kind of propolis health care toothpaste is comprised of following compositions in weight percentage: 0.8% propolis, 0.6%D-pantothenylol, 35% silicon dioxide, 12% glycerol, 14% sorbitol, 2% sodium lauroyl sarcosine, 0.2% hydroxyethyl-cellulose, 0.6% hydroxy methocel, 2% whitening agent, surplus is water.
Described whitening agent consists of by weight following component: 50 parts of sodium phytates, 15 parts of glycyrrhizins and 20 parts of glucoseoxidases.
According to the preparation method of embodiment 1, obtain the propolis health care toothpaste of embodiment 3.
Embodiment 4
A kind of propolis health care toothpaste is comprised of following compositions in weight percentage: 0.8% propolis, 0.6%D-pantothenylol, 35% silicon dioxide, 12% glycerol, 14% sorbitol, 2% sodium lauroyl sarcosine, 0.2% hydroxyethyl-cellulose, 0.6% hydroxy methocel, 2% whitening agent, surplus is water.
Described whitening agent consists of by weight following component: 50 parts of sodium phytates, 15 parts of aloins and 15 parts of glycyrrhizins.
According to the preparation method of embodiment 1, obtain the propolis health care toothpaste of embodiment 4.
Embodiment 5
A kind of propolis health care toothpaste is comprised of following compositions in weight percentage: 0.8% propolis, 0.6%D-pantothenylol, 35% silicon dioxide, 12% glycerol, 14% sorbitol, 2% sodium lauroyl sarcosine, 0.2% hydroxyethyl-cellulose, 0.6% hydroxy methocel, 2% whitening agent, surplus is water.
Described whitening agent consists of by weight following component: 15 parts of aloins, 15 parts of glycyrrhizins and 20 parts of glucoseoxidases.
According to the preparation method of embodiment 1, obtain the propolis health care toothpaste of embodiment 5.
Embodiment 6
A kind of propolis health care toothpaste is comprised of following compositions in weight percentage: 0.8% propolis, and the 0.6%D-pantothenylol, 35% silicon dioxide, 12% glycerol, 14% sorbitol, 2% sodium lauroyl sarcosine, 0.2% hydroxyethyl-cellulose, 0.6% hydroxy methocel, surplus is water.
According to the preparation method of embodiment 1, obtain the propolis health care toothpaste of embodiment 6.
Test case
48 adult men and women are divided into to 6 groups, use embodiment 1-5 toothpaste, every day, each was brushed once sooner or later, to reaching the mottle index LSI of use after 3 months continuously before using, tested respectively, method of testing and scoring rule are permitted first 5th～6 pages of 1.4.1 of master thesis " a kind of clinical efficacy evaluation study of novel whitening toothpaste " of son referring to Shanghai Communications University.
The LSI scoring method, concrete scoring rule is as follows:
0 minute-without mottle, exist;
1 minute-mottle size is no more than 1/3 of facing; Degree is slight mottle (yellow or yellowish-brown);
2 minutes-mottle size is no more than 2/3 of facing; Degree is moderate mottle (moderate brown);
3 minutes-mottle size is greater than 2/3 of facing; Degree is severe mottle (dark-brown or black).
LSI value after the statistics experimenter uses front LSI value and uses March, LSI meansigma methods after calculating the front LSI meansigma methods of use and using March, then calculate mottle index LSI rate of descent, the results are shown in Table 1.
Table 1: mottle index LSI test chart
| ? | Mottle index LSI rate of descent, % |
| Embodiment 1 | 25.3 |
| Embodiment 2 | 24.1 |
| Embodiment 3 | 23.8 |
| Embodiment 4 | 20.6 |
| Embodiment 5 | 18.7 |
| Embodiment 6 | 11.4 |
Mottle index LSI rate of descent (%)=[LSI meansigma methods before using-uses is the LSI meansigma methods after March]/use front LSI meansigma methods * 100%.
As seen from the data in Table 1, using embodiment 1-5 toothpaste after 3 months, the obvious decline of LSI value, toothpaste of the present invention has whitening effect preferably.
Claims (4)
1. a propolis health care toothpaste, it is characterized in that, by following compositions in weight percentage, formed: 0.6-1.0% propolis, 0.4-0.8%D-pantothenylol, 30-40% silicon dioxide, 8-16% glycerol, the 12-16% sorbitol, 1.6-2.4% sodium lauroyl sarcosine, 0.1-0.3% hydroxyethyl-cellulose, the 0.4-0.8% hydroxy methocel, surplus is water.
2. a propolis health care toothpaste, it is characterized in that, formed by following compositions in weight percentage: 0.6-1.0% propolis, 0.4-0.8%D-pantothenylol, 30-40% silicon dioxide, 8-16% glycerol, 12-16% sorbitol, 1.6-2.4% sodium lauroyl sarcosine, the 0.1-0.3% hydroxyethyl-cellulose, the 0.4-0.8% hydroxy methocel, the 1-3% whitening agent, surplus is water.
3. propolis health care toothpaste as claimed in claim 2, it is characterized in that: described whitening agent is a kind of or its mixture in sodium phytate, aloin, glycyrrhizin and glucoseoxidase.
4. propolis health care toothpaste as claimed in claim 3, is characterized in that, described whitening agent consists of by weight following component: 40-60 part sodium phytate, 10-20 part aloin, 10-20 part glycyrrhizin and 15-25 part glucoseoxidase.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310374693.6A CN103446033B (en) | 2013-08-24 | 2013-08-24 | Propolis health care toothpaste |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310374693.6A CN103446033B (en) | 2013-08-24 | 2013-08-24 | Propolis health care toothpaste |
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| Publication Number | Publication Date |
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| CN103446033A true CN103446033A (en) | 2013-12-18 |
| CN103446033B CN103446033B (en) | 2016-02-03 |
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| CN201310374693.6A Expired - Fee Related CN103446033B (en) | 2013-08-24 | 2013-08-24 | Propolis health care toothpaste |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105663015A (en) * | 2016-03-24 | 2016-06-15 | 广州健朗医用科技有限公司 | Special propolis toothpaste for pregnant and lying-in women and preparation method of special propolis toothpaste |
| CN105708783A (en) * | 2016-03-21 | 2016-06-29 | 王跃华 | Rose healthcare toothpaste |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1864660A (en) * | 2005-05-20 | 2006-11-22 | 远景生物科技（上海）有限公司 | An anti-cavity toothpaste with natural substances for children and method for making same |
| CN1864661A (en) * | 2005-05-20 | 2006-11-22 | 远景生物科技（上海）有限公司 | A highly effective plaque-removing whitening toothpaste and method for making same |
-
2013
- 2013-08-24 CN CN201310374693.6A patent/CN103446033B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1864660A (en) * | 2005-05-20 | 2006-11-22 | 远景生物科技（上海）有限公司 | An anti-cavity toothpaste with natural substances for children and method for making same |
| CN1864661A (en) * | 2005-05-20 | 2006-11-22 | 远景生物科技（上海）有限公司 | A highly effective plaque-removing whitening toothpaste and method for making same |
Non-Patent Citations (3)
| Title |
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| 宋心仿等: "《蜜蜂产品的应用与检测加工技术》", 31 December 2000, article "蜂胶牙膏", pages: 372 * |
| 王银龙等: "蜂胶保健牙膏防治牙周疾病的研究", 《中国中西医结合杂志》, vol. 17, no. 7, 31 December 1997 (1997-12-31), pages 431 - 432 * |
| 颜红侠等: "《日用化学品制造原理与技术》", 28 February 2011, article "蜂胶牙膏", pages: 244 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105708783A (en) * | 2016-03-21 | 2016-06-29 | 王跃华 | Rose healthcare toothpaste |
| CN105663015A (en) * | 2016-03-24 | 2016-06-15 | 广州健朗医用科技有限公司 | Special propolis toothpaste for pregnant and lying-in women and preparation method of special propolis toothpaste |
| CN105663015B (en) * | 2016-03-24 | 2018-06-29 | 广州健朗医用科技有限公司 | A kind of special bee glue tooth paste of pregnant and lying-in women and preparation method thereof |
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| Publication number | Publication date |
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| CN103446033B (en) | 2016-02-03 |
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Effective date of registration: 20190111 Address after: 510000 Room 413, No. 177, South Second Road, Yuncheng, Sanyuanli Street, Baiyun District, Guangzhou City, Guangdong Province (self-declaration) Patentee after: Senrui Health Technology (Guangzhou) Co.,Ltd. Address before: 510000 B1B2, one, two, three and four floors of the podium building 231 and 233, science Avenue, Guangzhou, Guangdong. Patentee before: BOAO ZONGHENG NETWORK TECHNOLOGY Co.,Ltd. Effective date of registration: 20190111 Address after: 510000 B1B2, one, two, three and four floors of the podium building 231 and 233, science Avenue, Guangzhou, Guangdong. Patentee after: BOAO ZONGHENG NETWORK TECHNOLOGY Co.,Ltd. Address before: 201107 T159 twenty-second, 1-30 Lane 88, min Bei Road, Minhang District, Shanghai. Patentee before: SHANGHAI FANGMU FINE CHEMICAL Co.,Ltd. |
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Granted publication date: 20160203 Termination date: 20200824 |