CN103393060A - Cis-4-heptenal and 5-methyl-2-phenyl-2-hexenal milk-flavor essence and application thereof in candies - Google Patents
Cis-4-heptenal and 5-methyl-2-phenyl-2-hexenal milk-flavor essence and application thereof in candies Download PDFInfo
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- CN103393060A CN103393060A CN2013103505198A CN201310350519A CN103393060A CN 103393060 A CN103393060 A CN 103393060A CN 2013103505198 A CN2013103505198 A CN 2013103505198A CN 201310350519 A CN201310350519 A CN 201310350519A CN 103393060 A CN103393060 A CN 103393060A
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Abstract
The invention discloses a cis-4-heptenal and 5-methyl-2-phenyl-2-hexenal milk-flavor essence and application thereof in candies. The flavors of the essence consist of cream flavor, sour flavor, fat flavor, fruity flavor, bean flavor, grease flavor, vanilla burnt sweet flavor, milk lactone flavor and a solvent; secondly, suitable aromatic raw materials are selected to prepare a milk-flavor essence for candies according to various flavors; then, cis-4-heptenal and 5-methyl-2-phenyl-2-hexenal are added into the milk-flavor essence for candies according to the ratio of 1: (10-20), the added amount is 2-4ppm, and the aroma change of the essence is evaluated; and finally, milk-flavor essences with/without cis-4-heptenal and 5-methyl-2-phenyl-2-hexenal are respectively applied to the candies, and the influence on the aromas and mouth feelings of the candies caused by the essences is evaluated. According to the cis-4-heptenal and 5-methyl-2-phenyl-2-hexenal milk-flavor essence, through adding a small amount of cis-4-heptenal and 5-methyl-2-phenyl-2-hexenal, the aroma of the milk-flavor essence for candies is more mellow and full, the freshness of the initial aroma is improved, and the whole milk sweet flavor and grease feeling are enhanced.
Description
Technical field
The present invention relates to a kind of milk-taste essence, specifically a kind of suitable-4-heptenal and 5-methyl-2-phenyl-2-hexenoic aldehyde milk-taste essence and the application in candy.
Background technology
Fragrance and mouthfeel are to estimate the major criterion of food quality, and be particularly outstanding aspect candy.What determining the candy local flavor is flavoring essence, and candy can increase the fragrance of the strong uniqueness of candy with essence, covers bad smell, makes us producing joyful sensation, promotes appetite, assist digestion.
Diversity due to flavour of food products on market constantly increases at present, and the consumer also no longer is satisfied with single local flavor to the hobby of candy, but more tends to fragrance novelty, uniqueness, and mouthfeel is more abundant, the more lasting product of aftertaste.Milk flavor sugar wherein is wide in variety, and sales volume is large, and people's popular welcome is got well and be subject to prospect.Therefore essence enterprise more and more payes attention to the research and development of milk-taste essence candy.How to show one's talent in the market that milk-taste essence spreads unchecked, improve occupation rate of market, the quality of the uniqueness of milk-taste essence, novelty and quality plays vital effect.Composite essence can reach the purpose of enriching fragrance and mouthfeel, but the style of also very easily bringing some not to be supposed to, workload strengthens concerning producing simultaneously, wastes time and energy.Therefore by adding single or the special perfume material of only a few increases essence uniqueness, novelty, the method that improves the essence quality provides one better to select for the blending worker.
Summary of the invention
The purpose of this invention is to provide a kind of suitable-4-heptenal and 5-methyl-2-phenyl-2-hexenoic aldehyde milk-taste essence and the application in candy, this milk-taste essence improves uniqueness and the novelty of milk-taste essence by adding the perfume material that threshold value is lower or fragrance is special, and makes it show more outstanding quality in the candy application.
The objective of the invention is to be achieved through the following technical solutions:
A kind of suitable-4-heptenal and 5-methyl-2-phenyl-2-hexenoic aldehyde milk-taste essence, it is characterized in that: this milk-taste essence comprises A component and B component, and wherein the A component is: the mass ratio of suitable-4-heptenal and 5-methyl-2-phenyl-2-hexenoic aldehyde is 1:10 ~ 20; The weight portion of B component consists of: 0.01 ~ 0.2 part of cream note, 0.1 ~ 0.8 part of sour note, 0.6 ~ 3 part of fatty note, 1 ~ 3 part of fruital rhythm, 0.01 ~ 0.2 part of beans note, 0.1 ~ 1.5 part of grease note, 1 ~ 5 part of the burnt fragrant and sweet rhythm of vanilla, 0.3 ~ 1 part of milk lactone rhythm, 85 ~ 95 parts of solvents; The addition of A component is 2 ~ 4ppm.
In the present invention, cream note raw material is 0.04 ~ 0.08 part of 3-hydroxy-2-butanone, 0.02 ~ 0.04 part of butyl butyryl lactate; Acid note raw material is 0.08 ~ 0.12 part of n-butyric acie, 0.07 ~ 0.15 part of caproic acid; Fat note raw material is 1 ~ 1.5 part of capric acid, 0.05 ~ 0.1 part of dodecoic acid, 0.15 ~ 0.25 part of tetradecylic acid, 0.4 ~ 0.8 part of hexadecylic acid, 0.1 ~ 0.2 part of stearic acid; Fruital rhythm raw material is 0.05 ~ 0.15 part of ethyl lactate, 0.06 ~ 0.1 part of ethyl laurate, 0.6 ~ 0.8 part of third-nonalactone, 0.2 ~ 0.4 part of third-decalactone, 0.8 ~ 1 part of third-undecalactone; Beans note raw material is 0.03 ~ 0.05 part of third-caprylolactone, 0.02 ~ 0.05 part of dihydrocoumarin; Grease note raw material is 0.1 ~ 0.3 part of ethyl myristate, 0.05 ~ 0.1 part of ethyl palmitate, 0.5 ~ 0.8 part of oleic acid, 0.05 ~ 0.1 part of ethyl oleate; The burnt fragrant and sweet rhythm raw material of vanilla is 0.5 ~ 1 part of ethyl maltol, 0.5 ~ 1 part of Ethyl vanillin, 1.5 ~ 2.5 parts of vanillic aldehydes; Milk lactone rhythm raw material is 0.15 ~ 0.3 part of fourth position-decalactone, 0.3 ~ 0.5 part of fourth position-dodecalactone; Solvent is propane diols.
A kind of suitable-4-heptenal and the 5-methyl-2-phenyl-application of 2-hexenoic aldehyde milk-taste essence in candy.To have or not the suitable-4-heptenal of interpolation and 5-methyl-2-phenyl-2-hexenoic aldehyde milk-taste essence to be applied to respectively in candy, estimate the impact of essence on candy fragrance and mouthfeel
Added the milk-taste essence of suitable-4-heptenal and 5-methyl-2-phenyl-2-hexenoic aldehyde in the present invention, fragrance is more mellow and fuller, full, and a fragrant freshness increases, and whole milk is fragrant and sweet, the grease sense strengthens.Be applied to product fragrance nature in candy, coordinate, the essence style remains intact, and to oral cavity, brings unique sense of taste to experience and lasting aftertaste.
The present invention by add a small amount of suitable-4-heptenal and 5-methyl-2-phenyl-2-hexenoic aldehyde greatly enriched the milk-taste essence style, and improved the quality of candy with milk-taste essence.The method is not only produced simple to operate, and consumption is few.
The specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.
Embodiment 1
A kind of suitable-4-heptenal and 5-methyl-2-phenyl-2-hexenoic aldehyde milk-taste essence, this milk-taste essence comprises A component and B component, the weight portion of B component consists of: 0.09 part of cream note, 0.2 part of sour note, 2.33 parts of fatty notes, 2.08 parts of fruital rhythms, 0.08 part of beans note, 1.01 parts of grease notes, 3.5 parts of the burnt fragrant and sweet rhythms of vanilla, 0.65 part of milk lactone rhythm, 90.06 parts of solvents.The corresponding perfume material of each note consists of: cream note raw material is 0.06 part of 3-hydroxy-2-butanone, 0.03 part of butyl butyryl lactate; Acid note raw material is 0.1 part of n-butyric acie, 0.1 part of caproic acid; Fat note raw material is 1.3 parts of capric acid, 0.08 part of dodecoic acid, 0.2 part of tetradecylic acid, 0.6 part of hexadecylic acid, 0.15 part of stearic acid; Fruital rhythm raw material is 0.1 part of ethyl lactate, 0.08 part of ethyl laurate, 0.7 part of third-nonalactone, 0.3 part of third-decalactone, 0.9 part of third-undecalactone; Beans note raw material is 0.04 part of third-caprylolactone, 0.04 part of dihydrocoumarin; Grease note raw material is 0.2 part of ethyl myristate, 0.08 part of ethyl palmitate, 0.65 part of oleic acid, 0.08 part of ethyl oleate; The burnt fragrant and sweet rhythm raw material of vanilla is 0.75 part of ethyl maltol, 0.75 part of Ethyl vanillin, 2 parts of vanillic aldehydes; Milk lactone rhythm raw material is 0.25 part of fourth position-decalactone, 0.4 part of fourth position-dodecalactone; Solvent is 90.06 parts of propane diols.
The A component is: the mass ratio of suitable-4-heptenal and 5-methyl-2-phenyl-2-hexenoic aldehyde is 1:15, adds in the B component, and the addition of A component is 3ppm.It is carried out sensory evaluation: milk-taste essence fragrance is more mellow and fuller, full, and a fragrant freshness increases, and whole milk is fragrant and sweet, the grease sense strengthens.
A kind of suitable-4-heptenal and the 5-methyl-2-phenyl-application of 2-hexenoic aldehyde milk-taste essence in candy.To have or not the suitable-4-heptenal of interpolation and 5-methyl-2-phenyl-2-hexenoic aldehyde milk-taste essence to be applied to respectively in candy, estimate the impact of essence on candy fragrance and mouthfeel
Concrete scheme is as follows:
(1) the design candy is filled a prescription with milk-taste essence: wherein the cream note is 0.01 ~ 0.2 part, 0.1 ~ 0.8 part of acid note, 0.6 ~ 3 part of fat note, 1 ~ 3 part of fruital rhythm, 0.01 ~ 0.2 part of beans note, 0.1 ~ 1.5 part of grease note, 1 ~ 5 part of the burnt fragrant and sweet rhythm of vanilla, 0.3 ~ 1 part of milk lactone rhythm, 85 ~ 95 parts of solvents.
(2) select the corresponding perfume material of each note to prepare the candy milk-taste essence: cream note raw material is 0.04 ~ 0.08 part of 3-hydroxy-2-butanone, 0.02 ~ 0.04 part of butyl butyryl lactate; Acid note raw material is 0.08 ~ 0.12 part of n-butyric acie, 0.07 ~ 0.15 part of caproic acid; Fat note raw material is 1 ~ 1.5 part of capric acid, 0.05 ~ 0.1 part of dodecoic acid, 0.15 ~ 0.25 part of tetradecylic acid, 0.4 ~ 0.8 part of hexadecylic acid, 0.1 ~ 0.2 part of stearic acid; Fruital rhythm raw material is 0.05 ~ 0.15 part of ethyl lactate, 0.06 ~ 0.1 part of ethyl laurate, 0.6 ~ 0.8 part of third-nonalactone, 0.2 ~ 0.4 part of third-decalactone, 0.8 ~ 1 part of third-undecalactone; Beans note raw material is 0.03 ~ 0.05 part of third-caprylolactone, 0.02 ~ 0.05 part of dihydrocoumarin; Grease note raw material is 0.1 ~ 0.3 part of ethyl myristate, 0.05 ~ 0.1 part of ethyl palmitate, 0.5 ~ 0.8 part of oleic acid, 0.05 ~ 0.1 part of ethyl oleate; The burnt fragrant and sweet rhythm raw material of vanilla is 0.5 ~ 1 part of ethyl maltol, 0.5 ~ 1 part of Ethyl vanillin, 1.5 ~ 2.5 parts of vanillic aldehydes; Milk lactone rhythm raw material is 0.15 ~ 0.3 part of fourth position-decalactone, 0.3 ~ 0.5 part of fourth position-dodecalactone; Solvent is 85 ~ 95 parts of propane diols.
(3) add above-mentioned candy with in milk-taste essence with the ratio of 1:10 ~ 20 suitable-4-heptenal and 5-methyl-2-phenyl-2-hexenoic aldehyde, wherein addition 2 ~ 4ppm.Estimate suitable-4-heptenal and 5-methyl-2-phenyl-2-hexenoic aldehyde to the fragrance impact of candy with milk-taste essence
(4) will have or not the milk-taste essence that adds suitable-4-heptenal and 5-methyl-2-phenyl-2-hexenoic aldehyde to be applied in candy respectively.The effect of milk-taste essence in candy of evaluation has been added suitable-4-heptenal and 5-methyl-2-phenyl-2-hexenoic aldehyde.
Added the milk-taste essence of suitable-4-heptenal and 5-methyl-2-phenyl-2-hexenoic aldehyde in the present invention, fragrance is more mellow and fuller, full, and a fragrant freshness increases, and whole milk is fragrant and sweet, the grease sense strengthens.Be applied to product fragrance nature in candy, coordinate, the essence style remains intact, and to oral cavity, brings unique sense of taste to experience and lasting aftertaste.
Embodiment 2
Another suitable-4-heptenal and 5-methyl-2-phenyl-2-hexenoic aldehyde milk-taste essence, this milk-taste essence comprises A component and B component, the weight portion of B component consists of: 0.06 part of cream note, 0.15 part of sour note, 2.85 parts of fatty notes, 1.71 parts of fruital rhythms, 0.1 part of beans note, 0.7 part of grease note, 4.5 parts of the burnt fragrant and sweet rhythms of vanilla, 0.8 part of milk lactone rhythm, 89.13 parts of solvents.The corresponding perfume material of each note consists of: cream note raw material is 0.04 part of 3-hydroxy-2-butanone, 0.02 part of butyl butyryl lactate; Acid note raw material is 0.08 part of n-butyric acie, 0.07 part of caproic acid; Fat note raw material is 1.5 parts of capric acid, 0.1 part of dodecoic acid, 0.25 part of tetradecylic acid, 0.8 part of hexadecylic acid, 0.2 part of stearic acid; Fruital rhythm raw material is 0.05 part of ethyl lactate, 0.06 part of ethyl laurate, 0.6 part of third-nonalactone, 0.2 part of third-decalactone, 0.8 part of third-undecalactone; Beans note raw material is 0.05 part of third-caprylolactone, 0.05 part of dihydrocoumarin; Grease note raw material is 0.1 part of ethyl myristate, 0.05 part of ethyl palmitate, 0.5 part of oleic acid, 0.05 part of ethyl oleate; The burnt fragrant and sweet rhythm raw material of vanilla is 1 part of ethyl maltol, 1 part of Ethyl vanillin, 2.5 parts of vanillic aldehydes; Milk lactone rhythm raw material is 0.3 part of fourth position-decalactone, 0.5 part of fourth position-dodecalactone; Solvent is 89.13 parts of propane diols.
The A component is: the mass ratio of suitable-4-heptenal and 5-methyl-2-phenyl-2-hexenoic aldehyde is 1:12, adds in the B component, and the addition of A component is 4ppm.It is carried out sensory evaluation: milk-taste essence fragrance is more mellow and fuller, full, and a fragrant freshness increases, and whole milk is fragrant and sweet, the grease sense strengthens.
To have or not the milk-taste essence that adds suitable-4-heptenal and 5-methyl-2-phenyl-2-hexenoic aldehyde to be applied in candy respectively.Confectionary products is carried out sensory evaluation: product fragrance nature, coordination, the essence style remains intact, and to oral cavity, brings unique sense of taste to experience and lasting aftertaste.
Embodiment 3
Another suitable-4-heptenal and 5-methyl-2-phenyl-2-hexenoic aldehyde milk-taste essence, this milk-taste essence comprises A component and B component, the weight portion of B component consists of: 0.12 part of cream note, 0.27 part of sour note, 1.7 parts of fatty notes, 2.45 parts of fruital rhythms, 0.05 part of beans note, 1.3 parts of grease notes, 3.5 parts of the burnt fragrant and sweet rhythms of vanilla, 0.45 part of milk lactone rhythm, 91.16 parts of solvents.The corresponding perfume material of each note consists of: cream note raw material is 0.08 part of 3-hydroxy-2-butanone, 0.04 part of butyl butyryl lactate; Acid note raw material is 0.12 part of n-butyric acie, 0.15 part of caproic acid; Fat note raw material is 1 part of capric acid, 0.05 part of dodecoic acid, 0.15 part of tetradecylic acid, 0.4 part of hexadecylic acid, 0.1 part of stearic acid; Fruital rhythm raw material is 0.15 part of ethyl lactate, 0.1 part of ethyl laurate, 0.8 part of third-nonalactone, 0.4 part of third-decalactone, 1 part of third-undecalactone; Beans note raw material is 0.03 part of third-caprylolactone, 0.02 part of dihydrocoumarin; Grease note raw material is 0.3 part of ethyl myristate, 0.1 part of ethyl palmitate, 0.8 part of oleic acid, 0.1 part of ethyl oleate; The burnt fragrant and sweet rhythm raw material of vanilla is 0.5 part of ethyl maltol, 0.5 part of Ethyl vanillin, 1.5 parts of vanillic aldehydes; Milk lactone rhythm raw material is 0.15 part of fourth position-decalactone, 0.3 part of fourth position-dodecalactone; Solvent is 91.16 parts of propane diols.
The A component is: the mass ratio of suitable-4-heptenal and 5-methyl-2-phenyl-2-hexenoic aldehyde is 1:18, adds in the B component, and the addition of A component is 2ppm.It is carried out sensory evaluation: milk-taste essence fragrance is more mellow and fuller, full, and a fragrant freshness increases, and whole milk is fragrant and sweet, the grease sense strengthens.
To have or not the milk-taste essence that adds suitable-4-heptenal and 5-methyl-2-phenyl-2-hexenoic aldehyde to be applied in candy respectively.Confectionary products is carried out sensory evaluation: product fragrance nature, coordination, the essence style remains intact, and to oral cavity, brings unique sense of taste to experience and lasting aftertaste.
Claims (5)
1. the invention discloses a kind of suitable-4-heptenal and 5-methyl-2-phenyl-2-hexenoic aldehyde milk-taste essence and the application in candy, its note consists of the cream note, sour note, the fat note, fruital rhythm, beans note, the grease note, the burnt fragrant and sweet rhythm of vanilla, milk lactone rhythm and solvent.
2. secondly according to each note, select suitable perfume material to prepare the candy milk-taste essence.
3. then add above-mentioned candy with in milk-taste essence with the ratio of 1:10 ~ 20 suitable-4-heptenal and 5-methyl-2-phenyl-2-hexenoic aldehyde, addition is 2 ~ 4ppm, estimates the aroma change of essence.
4. will have or not the milk-taste essence that adds suitable-4-heptenal and 5-methyl-2-phenyl-2-hexenoic aldehyde to be applied to respectively in candy finally, estimate the impact of essence on candy fragrance and mouthfeel.
The present invention by add a small amount of suitable-4-heptenal and 5-methyl-2-phenyl-2-hexenoic aldehyde, make candy more mellow and fuller, full with the fragrance of milk-taste essence, a fragrant freshness increases, whole milk is fragrant and sweet, the grease sense strengthens.
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Cited By (2)
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| WO2018032526A1 (en) * | 2016-08-18 | 2018-02-22 | 天宁香料（江苏）有限公司 | Viviparidae essence and use thereof in fishing bait |
| CN112368259A (en) * | 2018-06-26 | 2021-02-12 | 三菱瓦斯化学株式会社 | Isobutyrate compound having butyryloxy group or pivaloyloxy group at alpha-position, and fragrance composition |
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Cited By (2)
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| WO2018032526A1 (en) * | 2016-08-18 | 2018-02-22 | 天宁香料（江苏）有限公司 | Viviparidae essence and use thereof in fishing bait |
| CN112368259A (en) * | 2018-06-26 | 2021-02-12 | 三菱瓦斯化学株式会社 | Isobutyrate compound having butyryloxy group or pivaloyloxy group at alpha-position, and fragrance composition |
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Application publication date: 20131120 |