CN103385823A - Peel-off type Chinese angelica mask and preparation method thereof - Google Patents
Peel-off type Chinese angelica mask and preparation method thereof Download PDFInfo
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- CN103385823A CN103385823A CN2013101971624A CN201310197162A CN103385823A CN 103385823 A CN103385823 A CN 103385823A CN 2013101971624 A CN2013101971624 A CN 2013101971624A CN 201310197162 A CN201310197162 A CN 201310197162A CN 103385823 A CN103385823 A CN 103385823A
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- radix angelicae
- angelicae sinensis
- facial film
- skin
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- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- 241000213006 Angelica dahurica Species 0.000 title abstract 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 35
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 25
- QRYRORQUOLYVBU-VBKZILBWSA-N carnosic acid Chemical compound CC([C@@H]1CC2)(C)CCC[C@]1(C(O)=O)C1=C2C=C(C(C)C)C(O)=C1O QRYRORQUOLYVBU-VBKZILBWSA-N 0.000 claims abstract description 22
- NVNLLIYOARQCIX-MSHCCFNRSA-N Nisin Chemical compound N1C(=O)[C@@H](CC(C)C)NC(=O)C(=C)NC(=O)[C@@H]([C@H](C)CC)NC(=O)[C@@H](NC(=O)C(=C/C)/NC(=O)[C@H](N)[C@H](C)CC)CSC[C@@H]1C(=O)N[C@@H]1C(=O)N2CCC[C@@H]2C(=O)NCC(=O)N[C@@H](C(=O)N[C@H](CCCCN)C(=O)N[C@@H]2C(NCC(=O)N[C@H](C)C(=O)N[C@H](CC(C)C)C(=O)N[C@H](CCSC)C(=O)NCC(=O)N[C@H](CS[C@@H]2C)C(=O)N[C@H](CC(N)=O)C(=O)N[C@H](CCSC)C(=O)N[C@H](CCCCN)C(=O)N[C@@H]2C(N[C@H](C)C(=O)N[C@@H]3C(=O)N[C@@H](C(N[C@H](CC=4NC=NC=4)C(=O)N[C@H](CS[C@@H]3C)C(=O)N[C@H](CO)C(=O)N[C@H]([C@H](C)CC)C(=O)N[C@H](CC=3NC=NC=3)C(=O)N[C@H](C(C)C)C(=O)NC(=C)C(=O)N[C@H](CCCCN)C(O)=O)=O)CS[C@@H]2C)=O)=O)CS[C@@H]1C NVNLLIYOARQCIX-MSHCCFNRSA-N 0.000 claims abstract description 15
- 108010053775 Nisin Proteins 0.000 claims abstract description 15
- 239000004309 nisin Substances 0.000 claims abstract description 15
- 235000010297 nisin Nutrition 0.000 claims abstract description 15
- 239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 9
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000002994 raw material Substances 0.000 claims abstract description 8
- 239000008367 deionised water Substances 0.000 claims abstract description 7
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 7
- 238000007796 conventional method Methods 0.000 claims abstract description 4
- 230000001815 facial effect Effects 0.000 claims description 41
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 claims description 12
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 12
- 239000011630 iodine Substances 0.000 claims description 12
- 229910052740 iodine Inorganic materials 0.000 claims description 12
- KRPAJLYSLFNDOA-UHFFFAOYSA-N mephenesin carbamate Chemical compound CC1=CC=CC=C1OCC(O)COC(N)=O KRPAJLYSLFNDOA-UHFFFAOYSA-N 0.000 claims description 12
- 229950006838 mephenesin carbamate Drugs 0.000 claims description 12
- 239000003755 preservative agent Substances 0.000 claims description 10
- 230000002335 preservative effect Effects 0.000 claims description 10
- 150000001875 compounds Chemical class 0.000 claims description 9
- 244000060011 Cocos nucifera Species 0.000 claims description 7
- 235000013162 Cocos nucifera Nutrition 0.000 claims description 7
- QXNVGIXVLWOKEQ-UHFFFAOYSA-N Disodium Chemical compound [Na][Na] QXNVGIXVLWOKEQ-UHFFFAOYSA-N 0.000 claims description 7
- 125000002252 acyl group Chemical group 0.000 claims description 7
- NBMKJKDGKREAPL-DVTGEIKXSA-N beclomethasone Chemical compound C1CC2=CC(=O)C=C[C@]2(C)[C@]2(Cl)[C@@H]1[C@@H]1C[C@H](C)[C@@](C(=O)CO)(O)[C@@]1(C)C[C@@H]2O NBMKJKDGKREAPL-DVTGEIKXSA-N 0.000 claims description 7
- 229940092705 beclomethasone Drugs 0.000 claims description 7
- JMGZBMRVDHKMKB-UHFFFAOYSA-L disodium;2-sulfobutanedioate Chemical compound [Na+].[Na+].OS(=O)(=O)C(C([O-])=O)CC([O-])=O JMGZBMRVDHKMKB-UHFFFAOYSA-L 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 6
- 239000003643 water by type Substances 0.000 claims description 2
- 230000002421 anti-septic effect Effects 0.000 abstract description 13
- 235000011187 glycerol Nutrition 0.000 abstract description 7
- 239000002131 composite material Substances 0.000 abstract description 6
- WYVVKGNFXHOCQV-UHFFFAOYSA-N 3-iodoprop-2-yn-1-yl butylcarbamate Chemical compound CCCCNC(=O)OCC#CI WYVVKGNFXHOCQV-UHFFFAOYSA-N 0.000 abstract description 5
- 235000017166 Bambusa arundinacea Nutrition 0.000 abstract description 3
- 235000017491 Bambusa tulda Nutrition 0.000 abstract description 3
- 244000082204 Phyllostachys viridis Species 0.000 abstract description 3
- 235000015334 Phyllostachys viridis Nutrition 0.000 abstract description 3
- 239000011425 bamboo Substances 0.000 abstract description 3
- 239000000284 extract Substances 0.000 abstract description 3
- 229940099451 3-iodo-2-propynylbutylcarbamate Drugs 0.000 abstract description 2
- 239000003963 antioxidant agent Substances 0.000 abstract description 2
- 230000003078 antioxidant effect Effects 0.000 abstract description 2
- KJDVLQDNIBGVMR-UHFFFAOYSA-L disodium;3-[2-aminoethyl-[2-(2-carboxylatoethoxy)ethyl]amino]propanoate Chemical compound [Na+].[Na+].[O-]C(=O)CCN(CCN)CCOCCC([O-])=O KJDVLQDNIBGVMR-UHFFFAOYSA-L 0.000 abstract description 2
- QQGISFDJEJMKIL-JAIQZWGSSA-N (5z)-5-[[3-(hydroxymethyl)thiophen-2-yl]methylidene]-10-methoxy-2,2,4-trimethyl-1h-chromeno[3,4-f]quinolin-9-ol Chemical compound C1=CC=2NC(C)(C)C=C(C)C=2C2=C1C=1C(OC)=C(O)C=CC=1O\C2=C/C=1SC=CC=1CO QQGISFDJEJMKIL-JAIQZWGSSA-N 0.000 abstract 1
- 206010015150 Erythema Diseases 0.000 abstract 1
- 239000004166 Lanolin Substances 0.000 abstract 1
- 229940079857 disodium cocoamphodipropionate Drugs 0.000 abstract 1
- 229940039717 lanolin Drugs 0.000 abstract 1
- 235000019388 lanolin Nutrition 0.000 abstract 1
- 239000010408 film Substances 0.000 description 36
- 230000000052 comparative effect Effects 0.000 description 29
- 210000003491 skin Anatomy 0.000 description 23
- WPTUPLITBGLORN-VOTSOKGWSA-N 2-amino-4-oxo-6-[(e)-2-phenylethenyl]-1,7-dihydropyrrolo[2,3-d]pyrimidine-5-carbonitrile Chemical compound N#CC=1C=2C(=O)NC(N)=NC=2NC=1\C=C\C1=CC=CC=C1 WPTUPLITBGLORN-VOTSOKGWSA-N 0.000 description 11
- 238000000034 method Methods 0.000 description 9
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- 230000002159 abnormal effect Effects 0.000 description 6
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- 230000035943 smell Effects 0.000 description 6
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- 239000008280 blood Substances 0.000 description 3
- 210000004369 blood Anatomy 0.000 description 3
- 210000002615 epidermis Anatomy 0.000 description 3
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- 208000003351 Melanosis Diseases 0.000 description 2
- 241000745988 Phyllostachys Species 0.000 description 2
- 230000032683 aging Effects 0.000 description 2
- 238000013019 agitation Methods 0.000 description 2
- 230000017531 blood circulation Effects 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000009931 harmful effect Effects 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 235000010270 methyl p-hydroxybenzoate Nutrition 0.000 description 2
- 239000004292 methyl p-hydroxybenzoate Substances 0.000 description 2
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 description 2
- 229960002216 methylparaben Drugs 0.000 description 2
- 235000013336 milk Nutrition 0.000 description 2
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- 231100000252 nontoxic Toxicity 0.000 description 2
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- 150000002989 phenols Chemical class 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 239000006228 supernatant Substances 0.000 description 2
- 238000002137 ultrasound extraction Methods 0.000 description 2
- 208000002874 Acne Vulgaris Diseases 0.000 description 1
- 241000382455 Angelica sinensis Species 0.000 description 1
- 206010008570 Chloasma Diseases 0.000 description 1
- 229920000832 Cutin Polymers 0.000 description 1
- 208000001840 Dandruff Diseases 0.000 description 1
- 201000004624 Dermatitis Diseases 0.000 description 1
- 108010082495 Dietary Plant Proteins Proteins 0.000 description 1
- 241001529742 Rosmarinus Species 0.000 description 1
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- 206010039792 Seborrhoea Diseases 0.000 description 1
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- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 description 1
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- 150000001413 amino acids Chemical class 0.000 description 1
- 239000009188 angelicae sinensis extract Substances 0.000 description 1
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- SOROIESOUPGGFO-UHFFFAOYSA-N diazolidinylurea Chemical compound OCNC(=O)N(CO)C1N(CO)C(=O)N(CO)C1=O SOROIESOUPGGFO-UHFFFAOYSA-N 0.000 description 1
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- 150000002212 flavone derivatives Chemical class 0.000 description 1
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- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 1
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Abstract
The invention discloses a peel-off type Chinese angelica mask and a preparation method thereof. The peel-off type Chinese angelica mask is prepared by using a conventional method from the following raw materials by weight: 10 to 14 parts of polyvinyl alcohol, 8 to 12 parts of glycerin, 0.8 to 1.2 parts of lanolin alcohol ether-5-disodium sulfosuccinate, 4 to 6 parts of ethanol, 6 to 8 parts of disodium cocoamphodipropionate, 0.8 to 2 parts of a Chinese angelica extract, 0.03 to 0.08 part of a composite antiseptic and 100 parts of deionized water, wherein the composite antiseptic comprises, by weight, 1 to 3 parts of carnosic acid, 3 to 5 parts of a bamboo leaf antioxidant, 1 to 3 parts of nisin and 1 to 3 parts of 3-iodo-2-propynyl butyl carbamate. The peel-off type Chinese angelica mask provided by the invention can make one's face red and glossy, enables the skin to become tender and elastic and is capable of nourishing the skin and preventing roughness.
Description
Technical field
The present invention relates to facial film and preparation method thereof, be specifically related to a kind of exfoliated Radix Angelicae Sinensis facial film and preparation method thereof.
Background technology
Facial film is the important content in skin nursing,, for the regular application facial film of all kinds of skin characteristics, can make the oily skin defat, and thick pore is restrained, and the skin of withered gauffer recovers gloss, and the inflammation of skin sore skin is inhibited.facial film makes skin seem salubrious after using, smooth and pure white delicacy, this is because when facial film is coated on skin, facial film and skin produce affinity, drying gradually along with facial film, the skin temperature rise, blood circulation is accelerated, skin-tightening and tension force are strengthened, the sebum of skin secretion and moisture reverse osmosis are in horny layer, the epidermis softness is unfolded, the pore instinct is opened, effective ingredient in facial film infiltrates skin and is absorbed, facial film tightly is connected with skin simultaneously, when removing facial film, aging cutin on skin, in pore, the deep layer dirt is also by the while leukorrhagia, make skin pure and fresh clean.
When the dry root that is classified as umbelliferae angelica Angelica sinensis (Oliv.) Diels.Autumn end excavates, and removes fibrous root and silt, after moisture slightly evaporates, is bundled into wisp, and upper canopy, with pyrotechnics smoke-dried beancurd slowly.Radix Angelicae Sinensis is traditional medicine for enriching blood and activating blood.Because Radix Angelicae Sinensis can impel QI and blood full, blood flow is unobstructed, thus can make have rosy cheeks, gloss, the delicate high resilience of skin.And contain various trace elements in Radix Angelicae Sinensis, to skin nutrition, prevent coarse playing an important role.Radix Angelicae Sinensis can also be made in acne, chloasma, freckle treatment and black hair, anti-loss etc.The Radix Angelicae Sinensis external has been widely used in protective skin cream, also can decoct, steeps in wine or cook medicated diet for oral administration.Radix Angelicae Sinensis extract can extract and make by water extraction pharmaceutically commonly used or alcohol extracting method, also can be from buying on the market.
Summary of the invention
For above shortcomings in prior art, one of technical problem to be solved by this invention provides a kind of exfoliated Radix Angelicae Sinensis facial film.
Two of technical problem to be solved by this invention provides the preparation method of above-mentioned exfoliated Radix Angelicae Sinensis facial film.
The present invention seeks to be achieved through the following technical solutions:
A kind of exfoliated Radix Angelicae Sinensis facial film is prepared from according to a conventional method by the raw material of following weight parts:
10-14 part polyvinyl alcohol, 8-12 part glycerol, 0.8-1.2 part lanoline alcohol ether-5 sulfosuccinate disodium, 4-6 part ethanol, 6-8 part cocos nucifera oil acyl both sexes base disodium beclomethasone, 0.8-2 part Radix Angelicae Sinensis extracting solution, 0.03-0.08 part compound preservative, 100 parts of deionized waters.
Wherein, described compound preservative consists of by weight following component: 1-3 part carnosic acid, 3-5 part AOB, 1-3 part nisin, 1-3 part iodine propilolic alcohol butyl mephenesin Carbamate.
, with carnosic acid, AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate simple agitation mix homogeneously, can make described compound preservative.
Described exfoliated Radix Angelicae Sinensis facial film can adopt industry conventional method to be prepared from.
Further, the present invention also provides a kind of preparation method of exfoliated Radix Angelicae Sinensis facial film, following step, consists of:
Polyvinyl alcohol is added in deionized water, be heated to 70-90 ℃, dissolve, be cooled to 45-55 ℃, add glycerol, lanoline alcohol ether-5 sulfosuccinate disodium, ethanol, cocos nucifera oil acyl both sexes base disodium beclomethasone to stir, be cooled to 40 ℃, add Radix Angelicae Sinensis extracting solution and compound preservative, stir, can make described exfoliated Radix Angelicae Sinensis facial film.
Concrete, in the present invention:
Described polyvinyl alcohol can be selected the cosmetics-stage polyvinyl alcohol, and specifically can select as the trade mark is the polyvinyl alcohol of PVA1788, PVA1799 or PVA2488.
Glycerol has another name called: propylene glycol, English name: Glycerin, molecular formula C
3H
8O
3.
Lanoline alcohol ether-5 sulfosuccinate disodium, CAS accession number: 68890-92-6.
Cocos nucifera oil acyl both sexes base disodium beclomethasone, CAS accession number: 68411-57-4.
Radix Angelicae Sinensis extracting solution of the present invention can pass through commercially available obtaining.Also can adopt following method preparation and obtain: after Radix Angelicae Sinensis is pulverized, add the deionized water of 6-10 times of weight, soak 1-3 hour, ultrasonic extraction, 10-15 minute, filter, and is centrifugal, discards precipitation with supernatant concentration, makes Radix Angelicae Sinensis extracting solution.Preferably, after concentrating, controlling Radix Angelicae Sinensis extracting solution density is 1.02-1.10g/cm
3.
Carnosic acid, molecular formula: C
20H
28O
4, No. CAS: 3650--09-7, source: Labiatae Rosmarinus plant rosemary Rosmarinus officinalis L.
AOB, No. CNS: 04.019, English name: antioxidant of bamboo leaves.AOB extracts from the tender leaf of Phyllostachys (phyllostachys) bamboo, natural, the nutrition take flavone and phenolic compound as effective ingredient, multi-functional food antioxidant.
Nisin also claims nisin, English name: Nisin, and by the synthetic a kind of polypeptide that is formed by 34 aminoacid of streptococcus acidi lactici metabolism, molecular formula C
143H
228O
37N
42S
7Molecular weight is 3348, and nisin consists of water-wet side and hydrophobic side, is typical surfactant, be efficient, nontoxic biological antiseptic, be widely used in the anticorrosion of milk and milk products, fermented beverage, filling food, vegetable protein food, meat and its products at present.
Iodine propilolic alcohol butyl mephenesin Carbamate, English name: 3-Iodo-2-propynyl butylcarbamate, be abbreviated as IPBC, No. CAS: 55406-53-6, molecular formula: C
8H
12INO
2, molecular weight is 281.10.
The present invention uses carnosic acid, AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate composite as antiseptic, and antiseptic effect is significantly improved, the long shelf-life of facial film.And, use Compositional antiseptic agent, greatly reduce the consumption of iodine propilolic alcohol butyl mephenesin Carbamate, the consumption of iodine propilolic alcohol butyl mephenesin Carbamate is controlled at below 0.03%, meet the IPBC that stipulates in China's cosmetics health standard and European Union's regulatory affairs and limit the use of antiseptic in components of cosmetics, maximum permission working concentration is 0.05% in cosmetics.Carnosic acid, AOB, nisin are the nontoxic biological antiseptic, be widely used in food service industry, in the present invention, it is diverted to cosmetic mask, can't brings ill effect to human body or skin, and can not produce harmful effect to the stability of facial film.
The using method of exfoliated Radix Angelicae Sinensis facial film of the present invention is: before using facial film, first deeply cleaning is facial, again facial film is coated on face, after 15-25 minute, the facial film active substance is absorbed by the skin, the moisture evaporation, form gradually thin film at face, this thin film is peeled off from face, and the dirt on skin of face, scurf also stick on thin film in company with and are eliminated, and it is clean, smooth that face seems.
Exfoliated Radix Angelicae Sinensis facial film of the present invention, can the deep layer cleaning skin of face, desalinates facial microgroove, makes skin elasticity compact, and the water profit is plentiful.Continue to use, skin water profit is flexible, reproduces youthful vigor.
Exfoliated Radix Angelicae Sinensis facial film of the present invention, can make have rosy cheeks, the delicate high resilience of gloss, skin, can skin nutrition, prevent coarse.
Exfoliated Radix Angelicae Sinensis facial film of the present invention, adopt carnosic acid, AOB, nisin, the composite antiseptic of iodine propilolic alcohol butyl mephenesin Carbamate, and shelf life of products is long, and can not produce harmful effect to skin.
The specific embodiment
The invention will be further described below in conjunction with embodiment.
Embodiment 1
Take each raw material according to corresponding embodiment 1 data in table 1,, with carnosic acid, AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate simple agitation mix homogeneously, can make described compound preservative.
Polyvinyl alcohol is added in deionized water, be heated to 70-90 ℃, dissolve, be cooled to 45-55 ℃, add glycerol, lanoline alcohol ether-5 sulfosuccinate disodium, ethanol, cocos nucifera oil acyl both sexes base disodium beclomethasone to stir, be cooled to 40 ℃, add Radix Angelicae Sinensis extracting solution and compound preservative, stir, can make described exfoliated Radix Angelicae Sinensis facial film.
Wherein, the Radix Angelicae Sinensis extracting solution in embodiment 1 and Comparative Examples 1-5 adopts following method to be prepared from: after Radix Angelicae Sinensis is pulverized, add the deionized water of 8 times of weight, soaked 2 hours, ultrasonic extraction, 12 minutes, filter, centrifugal, discard precipitation with supernatant concentration, after concentrating, making density is 1.06g/cm
3Radix Angelicae Sinensis extracting solution.
Table 1: face pack prescription list position: kilogram
| ? | Embodiment 1 | Comparative Examples 1 | Comparative Examples 2 | Comparative Examples 3 | Comparative Examples 4 | Comparative Examples 5 |
| Deionized water | 100 | 100 | 100 | 100 | 100 | 100 |
| PVA-124 88 | 12 | 12 | 12 | 12 | 12 | 12 |
| Glycerol | 10 | 10 | 10 | 10 | 10 | 10 |
| Lanoline alcohol ether-5 sulfosuccinate disodium | 1 | 1 | 1 | 1 | 1 | 1 |
| Ethanol | 5 | 5 | 5 | 5 | 5 | 5 |
| Cocos nucifera oil acyl both sexes base disodium beclomethasone | 7 | 7 | 7 | 7 | 7 | 7 |
| Radix Angelicae Sinensis extracting solution | 1 | 1 | 1 | 1 | 1 | 1 |
| Carnosic acid | 0.01 | / | / | / | / | / |
| AOB | 0.02 | 0.02 | 0.02 | 0.03 | / | / |
| Nisin | 0.01 | 0.01 | 0.02 | 0.01 | / | / |
| Iodine propilolic alcohol butyl mephenesin Carbamate | 0.01 | 0.02 | 0.01 | 0.01 | / | / |
| Methyl parahydroxybenzoate | / | / | / | / | 0.05 | / |
Comparative Examples 1
Take each raw material according to corresponding Comparative Examples 1 data in table 1.Adopt the described method of embodiment 1 to prepare the exfoliated Radix Angelicae Sinensis facial film of Comparative Examples 1.
Comparative Examples 2
Take each raw material according to corresponding Comparative Examples 2 data in table 1.Adopt the described method of embodiment 1 to prepare the exfoliated Radix Angelicae Sinensis facial film of Comparative Examples 2.
Comparative Examples 3
Take each raw material according to corresponding Comparative Examples 3 data in table 1.Adopt the described method of embodiment 1 to prepare the exfoliated Radix Angelicae Sinensis facial film of Comparative Examples 3.
Comparative Examples 4
Take each raw material according to corresponding Comparative Examples 4 data in table 1.Adopt the described method of embodiment 1 to prepare the exfoliated Radix Angelicae Sinensis facial film of Comparative Examples 4.
Comparative Examples 5
Take each component according to Comparative Examples 5 data corresponding in table 1, adopt the described method of embodiment 1, namely obtain the exfoliated Radix Angelicae Sinensis facial film of Comparative Examples 5.
Test case
The exfoliated Radix Angelicae Sinensis facial film that respectively embodiment 1 and Comparative Examples 1-5 is made, carry out fill with the dark brown vial, opens wide bottle cap, is placed under 40 ℃ of ambient temperatures, relative humidity 85% environment, continues to observe and test, and concrete outcome sees the following form.Detect the microorganism level, concrete test item, detection method and examination criteria carry out according to QB/T2872-2007.
| ? | Observe phenomena |
| Embodiment 1 | No abnormality seen after 60 days, abnormal smells from the patient is pure |
| Comparative Examples 1 | After 50 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
| Comparative Examples 2 | After 40 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
| Comparative Examples 3 | After 40 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
| Comparative Examples 4 | After 40 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
| Comparative Examples 5 | After 5 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
The antiseptic methyl parahydroxybenzoate that uses in Comparative Examples 4 is one of the most frequently used cosmetics preservative in this area.Belong to antiseptic phenols, generally effective to mycete, yeast, antibacterial, the effect that suppresses growth of microorganism is arranged, effectively extend the shelf-life (40 days shelf-lifves under test condition of the present invention) of cosmetics after adding, but long-term this antiseptic of excessive use, the Diazolidinyl Urea epidermis cell, cause the epidermis transition aging.
Can significantly be drawn by test data, the embodiment of the present invention 1 is used carnosic acid, AOB, nisin and the composite Synergistic of iodine propilolic alcohol butyl mephenesin Carbamate, and antiseptic effect (60 days shelf-lifves under test condition of the present invention) obviously is better than Comparative Examples 1-3 and only adopts AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate three composite (in the shelf-life under test condition of the present invention below 50 days).
The facial film of the embodiment of the present invention 1 is placed in accelerated test under 40 ℃ of ambient temperatures, relative humidity 85% environment at opening, can reach 60 days antiseptic effects, the long shelf-life of facial film, and conversion shady and cool dry its shelf-life of place under sealing state far surpasses 3 years.
The above; it is only the specific embodiment of the present invention; but protection scope of the present invention is not limited to this; any those of ordinary skill in the art are in the disclosed technical scope of the present invention; variation or the replacement that can expect without creative work, within all should being encompassed in protection scope of the present invention.Therefore, protection scope of the present invention should be as the criterion with the protection domain that claims were limited.
Claims (3)
1. exfoliated Radix Angelicae Sinensis facial film, it is characterized in that, raw material by following weight parts is prepared from according to a conventional method: 10-14 part polyvinyl alcohol, 8-12 part glycerol, 0.8-1.2 part lanoline alcohol ether-5 sulfosuccinate disodium, 4-6 part ethanol, 6-8 part cocos nucifera oil acyl both sexes base disodium beclomethasone, 0.8-2 part Radix Angelicae Sinensis extracting solution, 0.03-0.08 part compound preservative, 100 parts of deionized waters.
2. exfoliated Radix Angelicae Sinensis facial film as claimed in claim 1, it is characterized in that, described compound preservative consists of by weight following component: 1-3 part carnosic acid, 3-5 part AOB, 1-3 part nisin, 1-3 part iodine propilolic alcohol butyl mephenesin Carbamate.
3. the preparation method of exfoliated Radix Angelicae Sinensis facial film as claimed in claim 2, it is characterized in that, formed by following step: polyvinyl alcohol is added in deionized water, be heated to 70-90 ℃, dissolve, be cooled to 45-55 ℃, add glycerol, lanoline alcohol ether-5 sulfosuccinate disodium, ethanol, cocos nucifera oil acyl both sexes base disodium beclomethasone to stir, be cooled to 40 ℃, add Radix Angelicae Sinensis extracting solution and compound preservative, stir.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105055263A (en) * | 2015-10-02 | 2015-11-18 | 王学建 | Traditional Chinese medicine mask with whitening and spot reducing effects and preparation method of traditional Chinese medicine mask |
| CN106214572A (en) * | 2016-08-30 | 2016-12-14 | 陈秀华 | A kind of Chinese medicine composition for skin care and the application in mask product thereof |
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| CN102198062A (en) * | 2011-05-26 | 2011-09-28 | 成都中医药大学 | Red sage root mask and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102198062A (en) * | 2011-05-26 | 2011-09-28 | 成都中医药大学 | Red sage root mask and preparation method thereof |
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| L.V. THOMAS，ET AL: "Nisin synergy with natural antioxidant extracts of the herb rosemary", 《PROC IM IS ON NATURAL PRESERV. IN FOOD SYSTEMS》, 31 December 2006 (2006-12-31), pages 109 - 113 * |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105055263A (en) * | 2015-10-02 | 2015-11-18 | 王学建 | Traditional Chinese medicine mask with whitening and spot reducing effects and preparation method of traditional Chinese medicine mask |
| CN106214572A (en) * | 2016-08-30 | 2016-12-14 | 陈秀华 | A kind of Chinese medicine composition for skin care and the application in mask product thereof |
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| CN103385823B (en) | 2015-05-06 |
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