CN103371424A - Method for preparing traditional Chinese medicine beverage concentrated liquor - Google Patents
Method for preparing traditional Chinese medicine beverage concentrated liquor Download PDFInfo
- Publication number
- CN103371424A CN103371424A CN2012101139775A CN201210113977A CN103371424A CN 103371424 A CN103371424 A CN 103371424A CN 2012101139775 A CN2012101139775 A CN 2012101139775A CN 201210113977 A CN201210113977 A CN 201210113977A CN 103371424 A CN103371424 A CN 103371424A
- Authority
- CN
- China
- Prior art keywords
- parts
- chinese medicine
- traditional chinese
- concentrate
- extract
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Medicines Containing Plant Substances (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
Abstract
The invention relates to a membrane separation technology for beverage concentrated liquor containing traditional Chinese medicine components. The key preparation process is as follows: the problems of large energy consumption, long production period, effective component loss of medical liquor and the like of the existing traditional Chinese medicine beverage in the prior art are successfully solved through comprehensive utilization of an inorganic ceramic membrane filter refining method and an organic reverse osmosis membrane concentration method. According to the invention, low-carbon and environment-friendly industrial development need of traditional Chinese medicine beverage production can be met, inherent quality of products can be remarkably improved, and transportation and storage of the product can be facilitated at the same time.
Description
Technical field
The present invention relates to a kind of membrane separation technique that contains the beverage concentrate of traditional Chinese medicine ingredients, particularly, the inorganic ceramic membrane that relates to a kind of herbal mixture composition water extract filters the integrated use of process for purification and organic reverse osmosis membrane method for concentration, it can be deployed into liquid or semi-solid beverage by interpolation water or thickener in this concentrate.
Background technology
The production technology that present stage contains the functional beverage of traditional Chinese medicine ingredients all adopts the extracting mode of the direct boiling of medicinal material, be transfer and the enrichment of guaranteeing the active ingredient composition, remove impurity mainly with polarity difference between component (solvent deposition or extraction, adsorbing separation etc.) for basic principle.As everyone knows, above-mentioned traditional handicraft Main Problems has: energy consumption is large, the production cycle is long, liquid repeatedly concentrated or turn molten meeting and make loss of effective components or destruction, especially the rate of transform of fragrance ingredient is significantly descended the many defectives of degradation.And membrane separation technique is as one of at present the most promising separation technology, it mainly is according to " screening " theory, then permeability is different according to the material molecule diameter difference in certain membrane aperture scope inner penetration, utilize pressure differential to be motive force, realize the separation between the different sized molecules materials.
Yet, because the complicated components of Chinese medicine extract, the multiple macromolecular substances such as polysaccharide, cellulose, starch, pigment and protein that contain higher concentration adopt conventional membrane separation technique easily to produce the problems such as the pollution of film material and obstruction, are unfavorable for industrial-scale production.
The present invention adopts inorganic ceramic membrane to substitute Chinese medicine tradition process for purification, reduces production costs, simplifies preparation technology on the one hand, can significantly improve on the other hand the rate of transform of active ingredient, and product is environment friendly and pollution-free.On this basis, and then adopt the reverse osmosis membrane concentration technique to realize that the low temperature of this product is concentrated, be applicable to Chinese medicinal drink concentrate " color " processing principle.
Further add on this basis the thickeners such as agar, carragheen, pectin and it can be deployed into semi-solid beverage, the transportation of sonvenient beverage product and storage.
Summary of the invention
Main purpose of the present invention is the problems such as the traditional processing technology energy consumption for existing Chinese medicinal drink is large, the production cycle long, the liquid loss of effective components is large, provides a kind of not only low carbon ring to protect, be convenient to transportation, but also can keep " color " various Chinese medicinal drink concentrate preparation method.
Chinese medicinal drink of the present invention mainly is comprised of the medicinal material of following weight proportioning:
20～40 parts of radix polygonati officinalis, 20～40 parts of the roots of kudzu vine, 10～20 parts of the tubers of dwarf lilyturf, 10～20 parts of ginsengs, 10～20 parts of the living Radixs Astragali, 5～15 parts in the fruit of Chinese magnoliavine, 5～15 parts of dark plums, 2～10 parts of honey-fried licorice roots.
Radix polygonati officinalis is nourishing Yin and moistening lung in the side, and nourishing the stomach to improve the production of body fluid is monarch drug in a prescription; The root of kudzu vine rises sends out the taste yang-energy, promotes the production of body fluid to quench thirst, and the tuber of dwarf lilyturf, Yin nourishing and lung moistening was ministerial drug altogether; Radix Codonopsis, living Radix Astragali nourishing generate fluid; Fruit of Chinese magnoliavine invigorating heart and kidney has the merit that promotes the production of body fluid to quench thirst concurrently, and dark plum closes the Radix Glycyrrhizae sour-sweet herbs nourishing yin, is adjutant; The honey-fried licorice root coordinating the drug actions of a prescription, full side's giving consideration to both the incidental and fundamental is played nourish yin and benefit qi altogether, and the merit that promotes the production of body fluid to quench thirst has the effect that reduces blood sugar, moist skin simultaneously.
The preparation method of Chinese medicinal drink extract of the present invention is as follows:
Take by weighing whole eight flavor medicinal material boiling secondaries such as radix polygonati officinalis, the root of kudzu vine, the tuber of dwarf lilyturf by above-mentioned weight proportion, add the water of 6～10 times of medicinal material amounts for the first time, decocted 1～3 hour, add the water of 6～10 times of medicinal material amounts for the second time, decocted 1～2 hour, merge decocting liquid twice, filter; Be lower than 10 ℃ of condition stand at low temperature 12 hours, get its supernatant, and get final product.
The removal of impurities fine filtering method of Chinese medicinal drink extract of the present invention is as follows:
Water intaking extract supernatant adopts inorganic ceramic membrane to filter, and under general condition gets final product effective removal of impurities, can obtain smart filtrate.
Its preferred working condition is: pore size of inorganic ceramic membrane is 200nm, and the extract temperature is 50～60 ℃ during filtration, and operation pressure reduction is 0.08～0.12Mpa, and crossflow velocity is respectively 2.2～3m
3/ S.
The method for concentration of the smart filtrate of Chinese medicinal drink of the present invention is as follows:
Getting above-mentioned smart filtrate, to adopt organic reverse osmosis membrane to carry out the liquid body concentrated, and namely getting relative density is the Chinese medicinal drink concentrate of 1.05～1.15 (60 ℃).
Its preferred working condition is: the film specification is the 0R level, and the extract temperature is 30～40 ℃ during filtration, and operation pressure reduction is 1.4～1.6Mpa, and crossflow velocity is respectively 3～5m
3/ S.
It can be deployed into semi-solid beverage, the wherein optional agar of thickener, carragheen, pectin, gelatin, sodium alginate, starch and derivative, cellulose and derivative thereof by the thickener that in above-mentioned concentrate, adds mass fraction 0.5～20%.
Preparation method of the present invention need adopt following index of correlation to investigate:
1, adopt full-automatic turbidimetry that the liquid that film separates front and back is carried out turbidimetric analysis turbidimetry;
2, according to flow and timing and calculating membrane flux.
3, index components is measured;
Puerarin: take octadecylsilane chemically bonded silica as filler; Take methanol-water (25: 75) as mobile phase; The detection wavelength is 250nm.
Ginsenoside: take octadecylsilane chemically bonded silica as filler; Take the second eyeball as mobile phase A, take water as Mobile phase B, the regulation in the according to the form below is carried out gradient elution; The detection wavelength is 203nm.
| Time (minute) | Mobile phase A (%) | Mobile phase B (%) |
| 0～35 | 19 | 81 |
| 35～55 | 19→29 | 81→71 |
| 55～70 | 29 | 71 |
| 70～100 | 29→40 | 71→60 |
The specific embodiment
Embodiment 1:
The Chinese medicinal drink prescription is:
Radix polygonati officinalis 30g, root of kudzu vine 30g, the tuber of dwarf lilyturf 15g, ginseng 15g, give birth to Radix Astragali 15g, fruit of Chinese magnoliavine 10g, dark plum 10g, honey-fried licorice root 6g;
Process for purification is:
A, get above-mentioned medicinal material boiling secondary, add the water of 8 times of medicinal material amounts for the first time, decocted 1.5 hours, add the water of 6 times of medicinal material amounts for the second time, decocted 1 hour, merge decocting liquid twice, filtration; Be lower than 10 ℃ of condition stand at low temperature 12 hours, get its supernatant, stand-by;
B, water intaking extract supernatant adopt inorganic ceramic membrane to filter, under general condition get final product effective removal of impurities, its preferred working condition is: pore size of inorganic ceramic membrane is 200nm, and the extract temperature is 55 ℃ during filtration, operation pressure reduction is 0.11Mpa, and crossflow velocity is respectively 2.5m
3/ S;
It is concentrated that C, the extract after getting ceramic membrane and filtering adopt organic reverse osmosis membrane to carry out the liquid body, and shut-down operation when treating that its relative density is 1.06 (60 ℃) namely gets this Chinese medicinal drink concentrate.Its preferred working condition is: the film specification is the OR level, and the extract temperature is 35 ℃ during filtration, and operation pressure reduction is 1.4Mpa, and crossflow velocity is respectively 4m
3/ S.
Implementation result:
Refining and the concentrated effect of table 1 Chinese medicinal drink
The concentrate curing is: after the concentrated liquid of tradition Chinese medicine being pressed the agar heating for dissolving of mass fraction 2%, mixes, and packing, sterilization, and get final product.
Embodiment 2:
The Chinese medicinal drink prescription is:
Radix polygonati officinalis 25g, root of kudzu vine 20g, the tuber of dwarf lilyturf 10g, ginseng 15g, give birth to Radix Astragali 18g, fruit of Chinese magnoliavine 12g, dark plum 12g, honey-fried licorice root 6g; Process for purification is:
A, get above-mentioned medicinal material boiling secondary, add the water of 8 times of medicinal material amounts for the first time, decocted 1.5 hours, add the water of 6 times of medicinal material amounts for the second time, decocted 1 hour, merge decocting liquid twice, filtration; Be lower than 10 ℃ of condition stand at low temperature 12 hours, get its supernatant, stand-by;
B, water intaking extract supernatant adopt inorganic ceramic membrane to filter, under general condition get final product effective removal of impurities, its preferred working condition is: pore size of inorganic ceramic membrane is 200nm, and the extract temperature is 52 ℃ during filtration, operation pressure reduction is 0.09Mpa, and crossflow velocity is respectively 2.3m
3/ S;
It is concentrated that C, the extract after getting ceramic membrane and filtering adopt organic reverse osmosis membrane to carry out the liquid body, and shut-down operation when treating that its relative density is 1.10 (60 ℃) namely gets this Chinese medicinal drink concentrate.Its preferred working condition is: the film specification is the OR level, and the extract temperature is 38 ℃ during filtration, and operation pressure reduction is 1.5Mpa, and crossflow velocity is respectively 4.5m
3/ S.
Implementation result:
Refining and the concentrated effect of table 2 Chinese medicinal drink
The concentrate curing is: after the concentrated liquid of tradition Chinese medicine being pressed the pectin heating for dissolving of mass fraction 1%, mixes, and packing, sterilization, and get final product.
Claims (3)
1. beverage concentrate that contains traditional Chinese medicine ingredients is characterized in that punishment forms and proportioning:
20～40 parts of radix polygonati officinalis, 20～40 parts of the roots of kudzu vine, 10～20 parts of the tubers of dwarf lilyturf, 10～20 parts of ginsengs, 10～20 parts of the living Radixs Astragali, 5～15 parts in the fruit of Chinese magnoliavine, 5～15 parts of dark plums, 2～10 parts of honey-fried licorice roots.
2. described a kind of beverage concentrate that contains traditional Chinese medicine ingredients according to claim 1 is characterized in that process for preparing medicine is as follows:
(1) preparation of Chinese medicinal drink extract: take by weighing whole eight flavor medicinal material boiling secondaries such as radix polygonati officinalis, the root of kudzu vine, the tuber of dwarf lilyturf by above-mentioned weight proportion, the water that adds for the first time 6～10 times of medicinal material amounts, decocted 1～3 hour, the water that adds for the second time 6～10 times of medicinal material amounts, decocted 1～2 hour, merge decocting liquid twice, filter; Be lower than 10 ℃ of condition stand at low temperature 12 hours, get its supernatant, and get final product.
(2) preparation of the smart filtrate of Chinese medicinal drink: water intaking extract supernatant adopts inorganic ceramic membrane to filter, and under general condition gets final product effective removal of impurities, can obtain smart filtrate.Its preferred working condition is: pore size of inorganic ceramic membrane is 200nm, and the extract temperature is 50～60 ℃ during filtration, and operation pressure reduction is 0.08～0.12Mpa, and crossflow velocity is respectively 2.2～3m
3/ S.
(3) preparation of Chinese medicinal drink concentrate: getting above-mentioned smart filtrate, to adopt organic reverse osmosis membrane to carry out the liquid body concentrated, and namely getting relative density is the Chinese medicinal drink concentrate of 1.05～1.15 (60 ℃).Its preferred working condition is: the film specification is the OR level, and the extract temperature is 30～40 ℃ during filtration, and operation pressure reduction is 1.4～1.6Mpa, and crossflow velocity is respectively 3～5m
3/ S.
3. it can be deployed into semi-solid beverage, the wherein optional agar of thickener, carragheen, pectin, gelatin, sodium alginate, starch and derivative, cellulose and derivative thereof by the thickener that in this concentrate, adds mass fraction 0.5～20%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012101139775A CN103371424A (en) | 2012-04-18 | 2012-04-18 | Method for preparing traditional Chinese medicine beverage concentrated liquor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012101139775A CN103371424A (en) | 2012-04-18 | 2012-04-18 | Method for preparing traditional Chinese medicine beverage concentrated liquor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103371424A true CN103371424A (en) | 2013-10-30 |
Family
ID=49457741
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2012101139775A Pending CN103371424A (en) | 2012-04-18 | 2012-04-18 | Method for preparing traditional Chinese medicine beverage concentrated liquor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103371424A (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103637340A (en) * | 2013-11-29 | 2014-03-19 | 李伟杰 | Honey beverage and preparation method thereof |
| CN104084047A (en) * | 2014-07-17 | 2014-10-08 | 新疆鹏弘生物科技有限公司 | Glycyrrhiza extracting solution clarification and concentration membrane system |
| CN106166227A (en) * | 2016-08-27 | 2016-11-30 | 桂林七星粉业有限责任公司 | A kind of processing technique of the fragrant solomonseal health-care powder with blood sugar decreasing effect |
| CN108850774A (en) * | 2018-07-04 | 2018-11-23 | 于银行 | One compound health-preserving beverage of seed ginseng Rui and preparation method thereof |
| CN109223977A (en) * | 2018-11-14 | 2019-01-18 | 吉林省九圣源生物科技有限公司 | A kind of health beverages and preparation method thereof |
| CN111991525A (en) * | 2020-09-02 | 2020-11-27 | 中国药科大学 | Effective component group of Simiao pills and preparation method and application thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1565272A (en) * | 2003-06-26 | 2005-01-19 | 罗宪章 | Tea containing fragrant solomonseal rhizome and honey, and its preparation method |
| CN1600118A (en) * | 2004-10-12 | 2005-03-30 | 范继余 | 'Yuge' milk and preparation method |
| CN1788622A (en) * | 2004-12-16 | 2006-06-21 | 肖自力 | Health drink possessing liver harmonization and qi dredging function |
| CN1823908A (en) * | 2005-12-29 | 2006-08-30 | 广州星群（药业）股份有限公司 | New technology for refining xiasanju extract using membrane separation technique |
| CN101574471A (en) * | 2008-05-08 | 2009-11-11 | 天津中新药业集团股份有限公司隆顺榕制药厂 | Medicament for treating diabetes and preparation method thereof |
-
2012
- 2012-04-18 CN CN2012101139775A patent/CN103371424A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1565272A (en) * | 2003-06-26 | 2005-01-19 | 罗宪章 | Tea containing fragrant solomonseal rhizome and honey, and its preparation method |
| CN1600118A (en) * | 2004-10-12 | 2005-03-30 | 范继余 | 'Yuge' milk and preparation method |
| CN1788622A (en) * | 2004-12-16 | 2006-06-21 | 肖自力 | Health drink possessing liver harmonization and qi dredging function |
| CN1823908A (en) * | 2005-12-29 | 2006-08-30 | 广州星群（药业）股份有限公司 | New technology for refining xiasanju extract using membrane separation technique |
| CN101574471A (en) * | 2008-05-08 | 2009-11-11 | 天津中新药业集团股份有限公司隆顺榕制药厂 | Medicament for treating diabetes and preparation method thereof |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103637340A (en) * | 2013-11-29 | 2014-03-19 | 李伟杰 | Honey beverage and preparation method thereof |
| CN104084047A (en) * | 2014-07-17 | 2014-10-08 | 新疆鹏弘生物科技有限公司 | Glycyrrhiza extracting solution clarification and concentration membrane system |
| CN106166227A (en) * | 2016-08-27 | 2016-11-30 | 桂林七星粉业有限责任公司 | A kind of processing technique of the fragrant solomonseal health-care powder with blood sugar decreasing effect |
| CN108850774A (en) * | 2018-07-04 | 2018-11-23 | 于银行 | One compound health-preserving beverage of seed ginseng Rui and preparation method thereof |
| CN109223977A (en) * | 2018-11-14 | 2019-01-18 | 吉林省九圣源生物科技有限公司 | A kind of health beverages and preparation method thereof |
| CN111991525A (en) * | 2020-09-02 | 2020-11-27 | 中国药科大学 | Effective component group of Simiao pills and preparation method and application thereof |
| CN111991525B (en) * | 2020-09-02 | 2022-05-03 | 中国药科大学 | Effective component group of Simiao pills and preparation method and application thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103371424A (en) | Method for preparing traditional Chinese medicine beverage concentrated liquor | |
| CN105248785B (en) | A kind of dendrobium candidum antipyretic beverage and its production technology | |
| CN103462010B (en) | Lycium ruthenicum oral solution and production method thereof | |
| CN105168285B (en) | A kind of ginsenoside extracting solution and its extracting method | |
| CN102579576B (en) | Chuanxiongchatiao granule extracts and preparations thereof | |
| CN105166913A (en) | Preparation method of dendrobe nutrition powder | |
| CN103609784A (en) | Green tea beverage with effects of calming nerves and reinforcing intelligence as well as nourishing brain | |
| CN104206576B (en) | A kind of preparation method of the instant tea powder being enriched with tea polyphenols | |
| CN104666369B (en) | A kind of extracting method of fuling peel | |
| CN107890524A (en) | A kind of CHUANBEI PIPA GAO and preparation method thereof | |
| CN103550285B (en) | Astragalus extractive grading preparation method | |
| CN104083617A (en) | Method for preparing child-strengthening digestion-promoting oral solution | |
| CN104001033A (en) | Preparation process of roxburgh anoectochilus terminal bud concentrated solution | |
| CN104642603A (en) | Cistanche green tea beverage | |
| CN103843925B (en) | A kind of health care instant molecular Radix Et Rhizoma Fagopyri Tatarici tea | |
| CN103652158B (en) | A kind of lotus leaf Sang Ju Yin tea instant molecular cold tea | |
| CN103609773A (en) | Green tea beverage containing polygala root | |
| CN100482196C (en) | An extraction preparation method of effective ingredients of Chinese medicine | |
| CN106119429A (en) | A kind of production method of Radix Notoginseng sugar | |
| CN104814215A (en) | Instant chrysanthemum flower tea and preparation method thereof | |
| CN205473493U (en) | Glycyrrhizic acid production system and glycyrrhizic acid waste water's processing system | |
| CN113633714A (en) | Preparation method of golden fruit beverage | |
| CN105685740A (en) | Method for preparing concentrated clear rabdosia rubescens juice | |
| CN103141844A (en) | Food capable of increasing immunity and preparation method thereof | |
| CN107232366A (en) | The preparation technology of dandelion centella nutrition sifting tea |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20131030 |