CN103343491A - Raw paper of on-machine coating type mosquito-proofing non-woven wallpaper and preparation method thereof - Google Patents
Raw paper of on-machine coating type mosquito-proofing non-woven wallpaper and preparation method thereof Download PDFInfo
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- CN103343491A CN103343491A CN2013102862997A CN201310286299A CN103343491A CN 103343491 A CN103343491 A CN 103343491A CN 2013102862997 A CN2013102862997 A CN 2013102862997A CN 201310286299 A CN201310286299 A CN 201310286299A CN 103343491 A CN103343491 A CN 103343491A
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Abstract
The invention relates to raw paper of on-machine coating type mosquito-proofing non-woven wallpaper and a preparation method thereof. The raw paper of the wallpaper is prepared by mixed papermaking of functional fiber and wood pulp cellulose and on-machine coating by adopting an adhesive composition, and comprises the following components in percentage by weight: 60-95 percent of adhesive, and 0.5-20 percent of mosquito-proofing pesticide, wherein the coating amount of the adhesive composition is 1-30 percent of the paper quantity. By adopting the technical scheme, the knock down rate of the mosquito-proofing type non-woven wallpaper produced by the raw material in 60 minutes can be 97 percent, and the wallpaper product does not shrink in the processing process, does not have wet feeling, can be released completely, is good in toughness, and has a function of knock down mosquitoes attached to the surface of the water paper.
Description
Technical field
The present invention relates to a kind of wallpaper base stock, relate in particular to mosquito-proof nonwoven wallpaper base stock of application type and preparation method thereof in a kind of machine.
Background technology
Nonwoven wallpaper is a kind of novel decorative material for wall surface.It has rich color, the myoplasm sense is strong, pattern is gorgeous, environmental protection, easy construction, price suitable, and characteristics such as the noble elegance of decorative effect are that other multiple indoor ornament materials is incomparable.But wallpaper base stock in the past all is basic material with the wood pulp fibre, this wallpaper low price, shortcoming be poor performance, not water-fast, be not easy to clean, be not easy to construction, because wood pulp fibre can absorb airborne moisture content in a large number, the surface can have damp, time to grow often can existing stain.When changing wallpaper base stock, owing to himself intensity difference, cause and peel off not exclusively, sticking wall phenomenon appears.
Chinese invention patent (the application number: 200810060243.9 applyings date: 2008-03-31) disclose nonwoven wallpaper base stock of applicant's application, comprise fibre stuff and adhesive, fibre stuff comprises wood pulp fibre and functional fibre, wood pulp fibre and functional fibre are 0～95%:5～100% by part by weight between the two, and adhesive accounts for 1～10% of body paper gross weight.Wallpaper base stock product of the present invention adds in process and does not shrink man-hour, the free from dampness sense, and it is complete to take off paper, and the pliability of paper is very good.
Chinese invention patent (the application number: 200810063378.0 applyings date: 2008-08-12) disclose nonwoven wallpaper base stock of applicant's application, this body paper comprises fibre stuff and adhesive, fibre stuff comprises wood pulp fibre and functional fibre, wood pulp fibre and functional fibre are 0～95%: 5～100% by part by weight between the two, and adhesive accounts for 1～10% of body paper gross weight; It is 0.8～25D that described functional fibre contains a kind of fineness at least, and length is the functional fibre of 15～60MM.The surface of wallpaper base stock of the present invention can show the striped of nature, and good looking appearance does not need to handle in addition.Simultaneously, the wallpaper base stock product adds in process and does not shrink man-hour, the free from dampness sense, and it is complete to take off paper, and the pliability of paper is very good.
Nonwoven wallpaper base stock can't reach effect mosquito-proof, that kill mosquito in above-mentioned two patents.For this reason, 2013102008215,2013102008003,2013102007458, the patent of invention of 201310200822X the applicant has applied for that number of patent application is:, these patents disclose respectively and have adopted the mosquito-proof type nonwoven wallpaper base stock of mosquito-proof fiber production, the mosquito-proof fiber price that adopts in this method is higher, caused the rising of production cost like this, only be suitable for expensive goods, for mill run, then still need consider production cost.
Summary of the invention
In order to solve above-mentioned technical problem, an object of the present invention is to provide the mosquito-proof nonwoven wallpaper base stock of application type in a kind of machine, this wallpaper base stock has reduced production cost, this wallpaper base stock can mosquito-proof, anti-water, mildew-resistant, anti-wiping, easily peel off, good processability, second purpose of the present invention provides the preparation method of above-mentioned mosquito-proof type nonwoven wallpaper base stock, it adopts copies the preparation of paper method, and this method technology is simple, enforcement is convenient.
In order to realize first above-mentioned purpose, the present invention has adopted following technical scheme:
The mosquito-proof nonwoven wallpaper base stock of application type in a kind of machine, this wallpaper base stock are mixed to copy to adopt to be coated with in the adhesive compound machine behind the paper by functional fibre, wood pulp fibre to be made; Described adhesive compound comprises adhesive 60% ~ 95% and mosquito-proof pesticide 0.5 ~ 20% by weight percentage, the coating weight of described adhesive compound be paper quantitative 1 ~ 30%.
As preferably, described adhesive compound comprises adhesive 90% ~ 99% and mosquito-proof pesticide 1 ~ 10% by weight percentage.
As preferably, the coating weight of described adhesive compound is 5 ~ 20%.
The mosquito-proof nonwoven wallpaper base stock of application type in a kind of machine according to claim 1, it is characterized in that: mosquito-proof pesticide is pyrethroid or the mosquito-proof pesticide of extracted form natural plant, is preferably decis or lambda-cyhalothrin.
As preferably, described functional fibre is one or more mixing in animal fiber, synthetic fiber and the artificial fibre.
As preferably, described functional fibre is one or more in collagenous fibres, keratin fiber, fibroin fiber, regenerated celulose fibre and the azlon; As preferred again, keratin fiber is wool, regenerated celulose fibre is one or more in viscose, copper ammonia fibre, the acetic ester fiber, and azlon is one or more in casein fibre, Zein fibers, ground nut fiber, the soybean fiber.
As preferably, described functional fibre is one or more in polyacrylonitrile fibre, polypropylene fibre, polyethylene fiber, polyvinyl acetal fiber, polyvinyl chloride fibre, polytetrafluoroethylene fibre, polyester fiber, polyamide fiber, polyurethane elastomeric fiber, polyimide fiber, polybenzimidazole fiber and the polyhenylene three nitrine fibers.
As preferably, described adhesive comprises one or more in natural adhesive and the synthetic adhesive; As preferably, described natural adhesive is one or more in shellac, gelatinized corn starch, specimens of one's blood and the natural rubber adhesive; Synthetic adhesive is one or more in thermosetting adhesive, thermoplastic adhesive, rubber based adhesives and the inorganic adhesive; As preferred again, described thermosetting adhesive comprises one or more in phenolic aldehyde, urea aldehyde, epoxy, polyester, organosilicon, the polyurethane; The thermoplastic adhesive comprises one or more in vinyl esters, esters of acrylic acid, phenylethylene, cellulose family, the alkyd resins class; Rubber based adhesives comprises one or more in reclaimed rubber, butadiene-styrene rubber, neoprene, cyano group rubber, butyl rubber, silicon rubber, the polyurethane rubber.
As preferably, described adhesive compound also comprises Cypres, and the consumption of Cypres is 0.5% ~ 5% of adhesive consumption; As preferably, described adhesive adopts polyvinyl alcohol and starch, and by solution oven dry weight vinyl alcohol: starch: Cypres is 2～8:0.5～2:0.04～0.15, and use amount accounts for 5～15% of body paper gross weight.
In order to realize second above-mentioned purpose, the present invention has adopted following technical scheme:
A kind of preparation method of described mosquito-proof type nonwoven wallpaper base stock, this wallpaper base stock is mixed to copy to adopt to be coated with in the adhesive compound machine behind the paper by functional fibre, wood pulp fibre to be made; Described adhesive compound comprises adhesive 60% ~ 95% and mosquito-proof pesticide 0.5 ~ 20% by weight percentage, the coating weight of described adhesive compound be paper quantitative 1 ~ 20%.
Nonwoven wallpaper base stock of the present invention can adopt Chinese invention patent (application number: 200810060243.9 applyings date: 2008-03-31) and Chinese invention patent (application number: 200810063378.0 applyings date: any one technical scheme is added mosquito-proof pesticide and is prepared 2008-08-12) in adhesive.
The present invention is owing to adopted above technical scheme, and with the mosquito-proof type nonwoven wallpaper that the present invention produces, the rate of knockdown of mosquito can reach 97% in its product 60min.And the wallpaper product adds in process and does not shrink man-hour, the free from dampness sense, and it is complete to take off paper, and the pliability of paper is very good, has to knock down the function that is attached to wallpaper surface mosquito.
The specific embodiment
Embodiment 1
Fibre furnish: softwood pulp 50%, broad-leaved slurry 30% mixes the degree of beating 20
0SR, polyster fibre 20%, 1.5 * 10mm, the quantitative 122g/m of basic paper
2, dip-coating polyvinyl alcohol, starch, decis and Cypres in the machine, coating fluid concentration 4%, coating weight 13g/m
2Polyvinyl alcohol: decis: starch: Cypres=5:1:2:0.8(all refers to the solution oven dry weight), get quantitative 135 g/m of body paper
2
The outer coating of machine 15 g/m
2Coating fluid prescription: 70 parts of 90 coarse whitings, 25 parts of 95 fine particle calcium carbonates, 25 parts of china clay, 50 parts in water, CMC1 part, 1 part of dispersant (solid content 40%), 2 parts of lubricants, 1.5 parts of water repellent agents, 40 parts in latex, paper basis weight 150 g/m
2, become the paper index as follows: quantitative 150 g/m
2, tightness 0.45g/cm
3, tensile strength 9.5kn/m, wet strength 2.5 kn/m, surface absorption 30 g/m
2, opacity 86%, the vertical 5100mn of tearability, horizontal 6300mn, expansion and contraction 0.3%.Has mosquito-proof effect.Page has placed the mosquito environment, and above mosquito can not be attached to, it had the mosquito of knocking down down.
Embodiment 2
Fibre furnish: softwood pulp 40%, broad-leaved slurry 30%, the degree of beating 18
0SR, soybean fiber 30%, 3.5D * 5mm, the quantitative 83g/m of basic paper
2, dip-coating epoxy resin, lambda-cyhalothrin, Cypres in the machine, epoxy resin: lambda-cyhalothrin: Cypres=10:1:0.5(all refers to the solution oven dry weight), coating fluid concentration 4%, coating weight 5g/m
2Get the quantitative 89g/m of body paper
2
The outer coating of machine 20 g/m
2, coating fluid prescription, 70 parts of 90 coarse whitings, 25 parts of 95 fine particle calcium carbonates, 25 parts of china clay, 50 parts in water, CMC1 part, 1 part of dispersant (solid content 40%), 2 parts of lubricants, 1.5 parts of water repellent agents, 40 parts in latex, paper basis weight 109g/m
2Become the paper index as follows: quantitative 109 g/m
2, tightness 0.56g/cm
3, tensile strength 7.8kn/m, wet strength 1.7 kn/m, surface absorption 28g/m
2, opacity 78%, the vertical 2500mn of tearability, horizontal 3200mn, expansion and contraction 0.6%.Has mosquito-proof effect.Page has placed the mosquito environment, above mosquito can not be attached to, down and out mosquito is arranged under it.
Embodiment 3
Fibre furnish: softwood pulp 20%, the degree of beating 25
0SR, viscose 80%, 5D * 2mm, the quantitative 100g/m of basic paper
2, dip-coating butadiene-styrene rubber in the machine: lambda-cyhalothrin: Cypres=20:5:1(all refers to the solution oven dry weight); Coating fluid concentration 4%, coating weight 20g/m
2, get quantitative 120 g/m of body paper
2, machine is coated with 15 g/m outward
2
The coating fluid prescription, 70 parts of 90 coarse whitings, 25 parts of 95 fine particle calcium carbonates, 25 parts of china clay, 50 parts in water, CMC1 part, 1 part of dispersant (solid content 40%), 2 parts of lubricants, 1.5 parts of water repellent agents, 40 parts in latex, paper basis weight 135g/m
2, become the paper index as follows: quantitative 135 g/m
2, tightness 0.38g/cm
3, tensile strength 3.5kn/m, wet strength 1.2 kn/m, surface absorption 35 g/m
2, opacity 89%, the vertical 2300mn of tearability, horizontal 2900mn, expansion and contraction 0.2%.Has mosquito-proof effect.Page has placed the mosquito environment, above mosquito can not be attached to, down and out mosquito is arranged under it.
Embodiment 4
Fibre furnish: softwood pulp 60%, the degree of beating 31
0SR, aramid fiber 40%, 25D * 40mm, the quantitative 100g/m of basic paper
2, dip-coating polyvinyl alcohol, lambda-cyhalothrin, starch and Cypres in the machine; Coating fluid concentration 4%, coating weight 20g/m
2, polyvinyl alcohol: lambda-cyhalothrin: starch: Cypres=4:0.5:1:0. 8(all refers to the solution oven dry weight), get quantitative 120 g/m of body paper
2
The outer coating of machine 15 g/m
2, coating fluid prescription, 70 parts of 90 coarse whitings, 25 parts of 95 fine particle calcium carbonates, 25 parts of china clay, 50 parts in water, CMC1 part, 1 part of dispersant (solid content 40%), 2 parts of lubricants, 1.5 parts of water repellent agents, 40 parts in latex, paper basis weight 135g/m
2, become the paper index as follows: quantitative 135 g/m
2, tightness 0.41g/cm
3, tensile strength 6.1kn/m, wet strength 1.8 kn/m, surface absorption 21 g/m
2, opacity 79%, the vertical 5600mn of tearability, horizontal 7400mn, expansion and contraction 0.23%.Has mosquito-proof effect.Page has placed the mosquito environment, above mosquito can not be attached to, down and out mosquito is arranged under it.
Embodiment 5
Fibre furnish: softwood pulp 40%, broad-leaved slurry 40%, the degree of beating 27
0SR, nylon fibre 20%, 15D * 10mm, the quantitative 90g/m of basic paper
2, dip-coating polyvinyl alcohol, decis and Cypres in the machine, coating fluid concentration 4%, coating weight 15g/m
2, polyvinyl alcohol: decis: Cypres=4:1:0.8(all refers to the solution oven dry weight), get quantitative 105 g/m of body paper
2
Become the paper index as follows: quantitative 105 g/m
2, tightness 0.45g/cm
3, tensile strength 7.7kn/m, wet strength 1.7 kn/m, surface absorption 22 g/m
2, opacity 83%, the vertical 3500mn of tearability, horizontal 4700mn, expansion and contraction 0.5%.Has mosquito-proof effect.Page has placed the mosquito environment, above mosquito can not be attached to, down and out mosquito is arranged under it.
Embodiment 6
Fibre furnish: softwood pulp 70%, the degree of beating 25
0SR, polyvinyl alcohol fibre 20%, 4D * 15mm, carbon fiber 10%, powdery, 200 orders filter, the quantitative 120g/m of basic paper
2, dip-coating polyvinyl alcohol, lambda-cyhalothrin, starch and Cypres in the machine, coating fluid concentration 10%, coating weight 20g/m
2, polyvinyl alcohol: lambda-cyhalothrin: starch: Cypres=4:0.5:1:0.8(all refers to the solution oven dry weight), get quantitative 140 g/m of body paper
2
Become the paper index as follows: quantitative 140 g/m
2, tightness 0.36g/cm
3, tensile strength 5.7kn/m, wet strength 1.2 kn/m, surface absorption 26 g/m
2, opacity 88%, the vertical 6700mn of tearability, laterally 5100mn.Has mosquito-proof effect.Page has placed the mosquito environment, above mosquito can not be attached to, down and out mosquito is arranged under it.
Embodiment 7
Fibre furnish: softwood pulp 30%, the degree of beating 20
0SR, polypropylene fiber 70%, 15D * 10mm, the quantitative 122g/m of basic paper
2, dip-coating polyvinyl alcohol, decis, starch and Cypres in the machine, coating fluid concentration 10%, coating weight 20g/m
2, polyvinyl alcohol: decis: starch: Cypres=4:0.5:1:0.8(all refers to the solution oven dry weight), get the quantitative 142g/m of body paper
2
Become the paper index as follows: quantitative 142 g/m
2, tightness 0.35g/cm
3, tensile strength 4.7kn/m, wet strength 1.2 kn/m, surface absorption 18 g/m
2, opacity 77%, the vertical 6200mn of tearability, laterally 4800mn.Has mosquito-proof effect.Page has placed the mosquito environment, above mosquito can not be attached to, down and out mosquito is arranged under it.
Embodiment 8
Fibre furnish: softwood pulp 20%, broad-leaved slurry 60% mixes the degree of beating 20
0SR, polyster fibre 10%, 1.5 * 6mm, 10%, 1.5 * 12mm, the quantitative 85g/m of basic paper
2, the water-soluble acrylic acid resin of dip-coating, decis and Cypres in the machine, coating fluid concentration 4%, coating weight 13g/m
2Water-soluble acrylic acid resin: Cypres=4:0.8(all refers to the solution oven dry weight), get quantitative 87.5 g/m of body paper
2
The outer coating of machine 15 g/m
2Coating fluid prescription: 90 coarse whitings: 70 parts, 95 fine particle calcium carbonates: 25 parts, china clay: 25 parts, water: 50 parts, CMC:1 part, dispersant (solid content 40%): 1 part, 2 parts of lubricants, water repellent agent: 1.5 parts, latex: 40 parts.Paper basis weight 108.7 g/m
2, become the paper index as follows: quantitative 110 g/m
2, tightness 0.55g/cm
3, tensile strength 8.5kn/m, wet strength 2.5 kn/m, surface absorption 25 g/m
2, opacity 86%, the vertical 3100mn of tearability, horizontal 4830mn, expansion and contraction 0.3%.Has mosquito-proof effect.Page has placed the mosquito environment, above mosquito can not be attached to, down and out mosquito is arranged under it.
Method of testing:
Quantitative GB/T451.2 paper and the quantitative determination method of cardboard
The determination method of thickness G B/T451.3 paper and cal(l)iper
The determination method of tearability GB/T455.1 paper tearability
The determination method of expansion and contraction GB/T451.3 paper retractility
The determination method of tensile strength after wet strength GB/T465.2 paper and cardboard soak in required time
The absorptive determination method of surface absorption GB/T1540 paper and cardboard
The determination method of thickness G B/T1543 paper opacity
The determination method of tensile strength GB/T12914 paper and cardboard tensile strength
The fire resistance method of testing: U.S.'s fire proofing standard is the ANSI/UL-94-2003 standard.
Claims (10)
1. the mosquito-proof nonwoven wallpaper base stock of application type in the machine, this wallpaper base stock are mixed to copy to adopt to be coated with in the adhesive compound machine behind the paper by functional fibre, wood pulp fibre to be made; It is characterized in that: described adhesive compound comprises adhesive 60% ~ 95% and mosquito-proof pesticide 0.5 ~ 20% by weight percentage, the coating weight of described adhesive compound be paper quantitative 1 ~ 30%.
2. the mosquito-proof nonwoven wallpaper base stock of application type in a kind of machine according to claim 1, it is characterized in that: adhesive compound comprises adhesive 90% ~ 99% and mosquito-proof pesticide 1 ~ 10% by weight percentage.
3. the mosquito-proof nonwoven wallpaper base stock of application type in a kind of machine according to claim 1, it is characterized in that: the coating weight of adhesive compound is 5 ~ 20%.
4. the mosquito-proof nonwoven wallpaper base stock of application type in a kind of machine according to claim 1, it is characterized in that: mosquito-proof pesticide is pyrethroid or the mosquito-proof pesticide of extracted form natural plant, is preferably decis or lambda-cyhalothrin.
5. according to the mosquito-proof nonwoven wallpaper base stock of application type in the described a kind of machine of any claim of claim 1 ~ 4, it is characterized in that: functional fibre is one or more mixing in animal fiber, synthetic fiber and the artificial fibre.
6. the mosquito-proof nonwoven wallpaper base stock of application type in a kind of machine according to claim 5, it is characterized in that: functional fibre is one or more in collagenous fibres, keratin fiber, fibroin fiber, regenerated celulose fibre and the azlon; As preferred again, keratin fiber is wool, regenerated celulose fibre is one or more in viscose, copper ammonia fibre, the acetic ester fiber, and azlon is one or more in casein fibre, Zein fibers, ground nut fiber, the soybean fiber.
7. the mosquito-proof nonwoven wallpaper base stock of application type in a kind of machine according to claim 5, it is characterized in that: functional fibre is one or more in polyacrylonitrile fibre, polypropylene fibre, polyethylene fiber, polyvinyl acetal fiber, polyvinyl chloride fibre, polytetrafluoroethylene fibre, polyester fiber, polyamide fiber, polyurethane elastomeric fiber, polyimide fiber, polybenzimidazole fiber and the polyhenylene three nitrine fibers.
8. according to the mosquito-proof nonwoven wallpaper base stock of application type in the described a kind of machine of any claim of claim 1 ~ 4, it is characterized in that: adhesive comprises one or more in natural adhesive and the synthetic adhesive; As preferably, described natural adhesive is one or more in shellac, gelatinized corn starch, specimens of one's blood and the natural rubber adhesive; Synthetic adhesive is one or more in thermosetting adhesive, thermoplastic adhesive, rubber based adhesives and the inorganic adhesive; As preferred again, described thermosetting adhesive comprises one or more in phenolic aldehyde, urea aldehyde, epoxy, polyester, organosilicon, the polyurethane; The thermoplastic adhesive comprises one or more in vinyl esters, esters of acrylic acid, phenylethylene, cellulose family, the alkyd resins class; Rubber based adhesives comprises one or more in reclaimed rubber, butadiene-styrene rubber, neoprene, cyano group rubber, butyl rubber, silicon rubber, the polyurethane rubber.
9. according to the mosquito-proof nonwoven wallpaper base stock of application type in the described a kind of machine of any claim of claim 1 ~ 4, it is characterized in that: described adhesive compound also comprises Cypres, and the consumption of Cypres is 0.5% ~ 5% of adhesive consumption; As preferably, described adhesive adopts polyvinyl alcohol and starch, and by solution oven dry weight vinyl alcohol: mosquito-proof pesticide: starch: Cypres is 2～8:0.5～2:0.5～2:0.04～0.15, and use amount accounts for 5～15% of body paper gross weight.
10. the preparation method of the mosquito-proof nonwoven wallpaper base stock of application type in the described a kind of machine of any claim of claim 1 ~ 4 is characterized in that this wallpaper base stock is mixed to copy to adopt to be coated with in the adhesive compound machine behind the paper by functional fibre, wood pulp fibre to make; Described adhesive compound comprises adhesive 60% ~ 95% and mosquito-proof pesticide 0.5 ~ 20% by weight percentage, the coating weight of described adhesive compound be paper quantitative 1 ~ 20%.
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| CN107988805A (en) * | 2017-12-01 | 2018-05-04 | 周昭金 | The preparation method of flame-retardant heat insulating anti-corrosion wallpaper |
| CN109112896A (en) * | 2018-10-16 | 2019-01-01 | 求秋平 | A kind of synthesis wallpaper base paper and preparation method improving anti-flammability and printability |
| CN109610219A (en) * | 2018-10-29 | 2019-04-12 | 浙江凯丰新材料股份有限公司 | A kind of preparation method and its mashing agitating device of top grade matt pure paper wallpaper |
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| CN103343491B (en) | 2015-12-09 |
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