CN103276437B - A kind of inner wall of kettle electrolytic polishing method - Google Patents

A kind of inner wall of kettle electrolytic polishing method Download PDF

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Publication number
CN103276437B
CN103276437B CN201310148511.3A CN201310148511A CN103276437B CN 103276437 B CN103276437 B CN 103276437B CN 201310148511 A CN201310148511 A CN 201310148511A CN 103276437 B CN103276437 B CN 103276437B
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kettle
wall
electrolytic solution
polishing method
electrolytic
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CN103276437A (en
Inventor
杨春辉
李勇
赵振钢
罗忠新
张艳秋
张涛
陆晓峰
闫玉良
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Huludao Huayuan Chemical Machinery Equipment Co Ltd
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Huludao Huayuan Chemical Machinery Equipment Co Ltd
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  • Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)

Abstract

The present invention is to provide a kind of inner wall of kettle electrolytic polishing method.Under the effect of power supply, carry out electrolytic solution polishing by arranging electrode and add electrolytic solution in kettle, realize the electropolishing of inner wall of kettle.Method of the present invention can improve inner wall of kettle electropolishing efficiency, and planeness is good, and surface smoothness is high, reduces costs.Be suitable for applying as the method for still class implements internal surface electropolishing.

Description

A kind of inner wall of kettle electrolytic polishing method
Technical field
The present invention is to provide the inner wall of kettle finishing method of oil, chemical industry, chemical fertilizer, field of medicaments use, specifically a kind of inner wall of kettle electrolytic polishing method.
Background technology
Electropolishing is that the surperficial selectivity anode in the electrolytic solution of applied metal melts and reaches a kind for the treatment of process of polishing and smooth appearance.When processing, by the control to current density, electrolytic solution viscosity and electrolyte temperature, metal is melted in the electrolytic solution, pocket enters passive state and melts, and boss activity melts, finally reach certain balance, by adding light agent and anodic polarization effect in electrolytic solution, reach the object of leveling polishing, surface brightness can reach extreme value.Main electropolishing mechanism has mucous membrane theory and passivation film theory.Smoothness and the thick liquid film of metallic surface electropolishing are closely related, and luminance brightness and solids passivation film closely related.Metallic surface electropolishing can be subdivided into macroscopic view leveling and microcosmic flattens two processes, and the change of these two processes and anode potential is closely related, and when it reaches a kind of dynamic balance state, surface brightness can reach extreme value.Compared with mechanical polishing, electropolishing can reduce the stress on metal inside and surface, and smooth finish after electropolishing and planeness keep more permanent than mechanical polishing.
At present, along with the development of domestic and international electropolishing technology, the research of the domestic electrolytic polishing process to metal works is more and more ripe, but can't realize the disposable integral electropolishing of cylindrical kettle and ellipsoidal head, especially main equipment, not yet has correlation technique at home.
Summary of the invention
In order to realize inner wall of kettle polishing, the present invention proposes a kind of inner wall of kettle electrolytic polishing method.The method pumps in kettle after being heated by electrolytic solution, and passes into direct current between pole plate and electrode axis, by the effect of electric current and the electrolytic reaction between pole plate and electrode axis, solves the technical problem of inner wall of kettle electropolishing.
The scheme that technical solution problem of the present invention adopts is:
Electropolishing equipment: kettle is arranged on and is equipped with on the carrying roller turning tank machine of drive-motor, and kettle rotation axis is arranged on the support at kettle two ends; At kettle built with insulcrete, insulcrete is fixed with pole plate, is fixed with electrode axis in kettle centre; Kettle one end is provided with electrolyte reservoir, in the side of electrolyte reservoir, temperature control unit is housed, and the side of electrolyte reservoir is provided with transferpump, and transferpump is communicated with second mouth of pipe by pipeline, and pipeline is equipped with under meter; First mouth of pipe is provided with at kettle opposite side; Kettle opposite side is provided with housing, and housing is connected with direct supply by wire, and direct supply is connected with pole plate and electrode axis respectively by first mouth of pipe, forms electrolysis loop.
Electrolytic polishing method: the electrolytic solution prepared is poured in electrolyte reservoir, start temperature control unit to heat electrolytic solution, after electrolyte temperature reaches design temperature scope, starting transferpump pumps in electrolyte reservoir by electrolytic solution, start housing and power supply, the drive-motor turning tank machine is started working, and rotates kettle and makes electrolytic solution carry out electropolishing reaction in still.
Electrolytic solution forms: phosphoric acid quality mark 56%, sulfuric acid massfraction 40%, glycerine additive 4%, solution density 1.76-1.82g/cm 3.
Electrolyte temperature: 55 ~ 65 DEG C;
Kettle rotating speed: >=0.05 ~ 0.1RPM;
Direct current power source voltage: 8V;
Direct supply electric current: 15 ~ 50 amperes/square decimeter;
Plate material: stereotype;
Electrode axis material: stainless steel or tetrafluoroethylene.
Positively effect, method of the present invention can realize the polishing of kettle Inner electrolysis, and efficiency is high, and planeness is good, and surface smoothness is high, reduces costs.Be suitable for applying as the method for still class implements internal surface electropolishing.
Accompanying drawing explanation
Fig. 1 is structure iron of the present invention
In figure, 1. electrolyte reservoir, 2. transferpump, 3. under meter, 4. kettle, 5. insulcrete, 6. pole plate, 7. electrode axis, 8. direct supply, 9. housing, 10. support, 11. turns of tank machines, 12. drive-motor, 13. first mouths of pipe, 14. second mouths of pipe, 15. temperature control units.
Embodiment
Electropolishing equipment: as shown in the figure, kettle 4 is arranged on and is equipped with on the carrying roller turning tank machine 11 of drive-motor 12, and kettle rotation axis is arranged on the support 10 at kettle two ends; At kettle built with insulcrete 5, insulcrete is fixed with pole plate 6, is fixed with electrode axis 7 in kettle centre; Kettle one end is provided with electrolyte reservoir 1, in the side of electrolyte reservoir, temperature control unit 15 is housed, and the side of electrolyte reservoir is provided with transferpump 2, and transferpump is communicated with second mouth of pipe 14 by pipeline, and pipeline is equipped with under meter 3; First mouth of pipe 13 is provided with at kettle opposite side; Kettle opposite side is provided with housing 9, and housing is connected with direct supply 8 by wire, and direct supply is connected with pole plate and electrode axis respectively by first mouth of pipe, forms electrolysis loop.
Electrolytic polishing method: the electrolytic solution prepared is poured in electrolyte reservoir, start temperature control unit to heat electrolytic solution, after electrolyte temperature reaches design temperature scope, starting transferpump pumps in electrolyte reservoir by electrolytic solution, start housing and power supply, the drive-motor turning tank machine is started working, and rotates kettle and makes electrolytic solution carry out electropolishing reaction in still.
Electrolytic solution forms: phosphoric acid quality mark 56%, sulfuric acid massfraction 40%, glycerine additive 4%, solution density 1.76-1.82g/cm 3.
Electrolyte temperature: 55 ~ 65 DEG C;
Kettle rotating speed: >=0.05 ~ 0.1RPM;
Direct current power source voltage: 8V;
Direct supply electric current: 15 ~ 50 amperes/square decimeter;
Plate material: stereotype;
Electrode axis material: stainless steel or tetrafluoroethylene.
Feature:
The present invention is by carrying out electropolishing to kettle right cylinder and two ends elipse head internal surface, the disposable electropolishing of main equipment or complicated inner surface can be realized, there is high-level efficiency, high-precision advantage, and electrolytic solution can repeated multiple timesly use, reduce costs and labour intensity, enhance productivity and quality of finish, reduce pollution emissions.

Claims (4)

1. an inner wall of kettle electrolytic polishing method, kettle one end is provided with electrolyte reservoir (1), temperature control unit (15) is housed in the side of electrolyte reservoir, transferpump (2) is provided with in the side of electrolyte reservoir, transferpump is communicated with second mouth of pipe (14) by pipeline, and pipeline is equipped with under meter (3); First mouth of pipe (13) is provided with at reactor opposite side; It is characterized in that:
Electropolishing equipment: kettle (4) be arranged on drive-motor (12) is housed the carrying roller turning tank machine (11) on, kettle rotation axis is arranged on the support (10) at kettle two ends; At kettle built with insulcrete (5), insulcrete is fixed with pole plate (6), is fixed with electrode axis (7) in kettle centre; Reactor opposite side is provided with housing (9), and housing is connected with direct supply (8) by wire, and direct supply is connected with pole plate and electrode axis respectively by first mouth of pipe, forms electrolysis loop;
Electrolytic polishing method: the electrolytic solution prepared is poured in electrolyte reservoir, start temperature control unit to heat electrolytic solution, after electrolyte temperature reaches design temperature scope, starting transferpump pumps in electrolyte reservoir by electrolytic solution, start housing and power supply, the drive-motor turning tank machine is started working, and rotates kettle and makes electrolytic solution carry out electropolishing reaction in still.
2. a kind of inner wall of kettle electrolytic polishing method according to claim 1, is characterized in that: electrolytic solution forms: phosphoric acid quality mark 56%, sulfuric acid massfraction 40%, glycerine additive 4%, solution density 1.76-1.82g/cm 3.
3. a kind of inner wall of kettle electrolytic polishing method according to claim 1, is characterized in that: electrolyte temperature: 55 ~ 65 DEG C; Reactor rotating speed: >=0.05rpm.
4. a kind of inner wall of kettle electrolytic polishing method according to claim 1, is characterized in that: the material of pole plate is stereotype; Electrode axis material is tetrafluoroethylene.
CN201310148511.3A 2013-04-26 2013-04-26 A kind of inner wall of kettle electrolytic polishing method Active CN103276437B (en)

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Publication number Priority date Publication date Assignee Title
CN105297128A (en) * 2015-11-05 2016-02-03 佛山市南海区鑫恒力五金机械厂 Horizontal electrolytic decoating line production device
CN106048706B (en) * 2016-08-17 2018-05-04 沈阳航天新光集团有限公司 Stainless steel parts endoporus electrochemical polish frock
CN106400100B (en) * 2016-10-18 2018-10-23 湖北帕尔森机电设备有限公司 Full-automatic electrolytic polissoir
CN109056048B (en) * 2018-07-05 2020-10-20 刘素兰 Electrochemical polishing system for inner surface of stainless steel pipe and using method thereof

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4156637A (en) * 1977-03-15 1979-05-29 Jumer John F Method for electro-processing large vessels
JPS57198299A (en) * 1981-05-29 1982-12-04 Hitachi Ltd Electrolytic polishing method for inside surface of vessel
JP2003266246A (en) * 2002-03-12 2003-09-24 Kansan Corp Electrolytic composite polishing device, electrolytic composite polishing tool, and electrolytic composite polishing method
CN201581151U (en) * 2009-12-01 2010-09-15 广州中国科学院工业技术研究院 Electrochemical polishing treatment device for internal surface and external surface of metal workpiece
CN102586855A (en) * 2012-03-30 2012-07-18 河北省安装工程公司 Electrochemical and mechanical composite polishing device
CN102703963A (en) * 2011-03-28 2012-10-03 上海迈诺光洁工贸有限公司 Movable electrode (cathode) for stainless steel inner tube electropolishing
CN202572021U (en) * 2012-03-30 2012-12-05 河北省安装工程公司 Electrochemical and mechanical compound polishing device

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4156637A (en) * 1977-03-15 1979-05-29 Jumer John F Method for electro-processing large vessels
JPS57198299A (en) * 1981-05-29 1982-12-04 Hitachi Ltd Electrolytic polishing method for inside surface of vessel
JP2003266246A (en) * 2002-03-12 2003-09-24 Kansan Corp Electrolytic composite polishing device, electrolytic composite polishing tool, and electrolytic composite polishing method
CN201581151U (en) * 2009-12-01 2010-09-15 广州中国科学院工业技术研究院 Electrochemical polishing treatment device for internal surface and external surface of metal workpiece
CN102703963A (en) * 2011-03-28 2012-10-03 上海迈诺光洁工贸有限公司 Movable electrode (cathode) for stainless steel inner tube electropolishing
CN102586855A (en) * 2012-03-30 2012-07-18 河北省安装工程公司 Electrochemical and mechanical composite polishing device
CN202572021U (en) * 2012-03-30 2012-12-05 河北省安装工程公司 Electrochemical and mechanical compound polishing device

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