CN103265908A - Transparent glue for hard plastic, and preparation method thereof - Google Patents
Transparent glue for hard plastic, and preparation method thereof Download PDFInfo
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- CN103265908A CN103265908A CN2013102411615A CN201310241161A CN103265908A CN 103265908 A CN103265908 A CN 103265908A CN 2013102411615 A CN2013102411615 A CN 2013102411615A CN 201310241161 A CN201310241161 A CN 201310241161A CN 103265908 A CN103265908 A CN 103265908A
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- hard plastic
- transparent glue
- toluene
- ethylene
- ethyl acetate
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Abstract
The invention relates to the technical field of glue, and particularly relates to transparent glue for hard plastic, and a preparation method thereof. The transparent glue for hard plastic comprises the following components in percentage by weight: 10%-20% of chlorinated rubber, 10%-20% of vinyl-vinyl acetate, 25%-40% of nitrocellulose, 5-15% of phenolic resin, 0.1%-0.5% of polyethylene wax, 5%-12% of methylbenzene, and 10%-30% of ethyl acetate. The preparation method for the transparent glue for hard plastic comprises the following steps: a. weighting each component; b. preparing mixed solvent; and c. mixing materials to obtain the transparent glue for hard plastic. The transparent glue for hard plastic has the clarified and transparent effects after being coated on a gold-stamped film, thus having good effects on decorating, interspersing and setting off stamped objects. Furthermore, the transparent glue for hard plastic has no after-tack phenomenon during storage process.
Description
Technical field
The present invention relates to the glue technical field, be specifically related to a kind of hard plastic transparent glue and preparation method thereof.
Background technology
Behind gold stamping film coating transparent glue, gold stamping film is bonded in is scalded on the thing again, just can impressed out golden literal or pattern by boiling hot thing, thereby played decoration, intersperse and setting off effect attractive in appearance to scalding thing.
In the thermoprint industry, gold stamping film is widely used on various transparent or nontransparent hard plastics.But in the prior art, transparent glue is coated and can be presented white vaporificly on the gold stamping film, does not have clarification, thorough effect, makes therefore, to make original pattern crested of being scalded thing after the thermoprint by boiling hot thing to be difficult to reach decoration, intersperse and set off effect attractive in appearance.
Transparent glue of the prior art is owing to contain silicon-dioxide or other dyestuff in the prescription, thereby makes transparent glue coat to present on the gold stamping film white vaporific.But if transparent glue prescription of the prior art does not use silicon-dioxide or other dyestuff, then transparent glue can produce " after-tacking " phenomenon in the process of depositing, thereby has had a strong impact on the quality of product.
Summary of the invention
One of purpose of the present invention is at the deficiencies in the prior art, a kind of hard plastic transparent glue is provided, this hard plastic coated with transparent glue have clarification on the gold stamping film, thorough effect, and this hard plastic can not produce " after-tacking " phenomenon with transparent glue in the process of depositing.
Two of purpose of the present invention is at the deficiencies in the prior art, the preparation method of a kind of hard plastic with transparent glue is provided, this preparation method is simple, easy handling, coat with transparent glue by the prepared hard plastic of the present invention simultaneously have clarification on the gold stamping film, thorough effect, and this hard plastic can not produce " after-tacking " phenomenon with transparent glue in the process of depositing.
To achieve these goals, the present invention adopts following technical scheme:
A kind of hard plastic transparent glue, it is made up of following raw materials by weight percent:
Chlorinated rubber 10% ~ 20%
Ethylene-vinyl acetate resin 10% ~ 20%
Soluble cotton 25% ~ 40%
Resol 5% ~ 15%
Polyethylene wax 0.1% ~ 0.5%
Toluene 5% ~ 12%
Ethyl acetate 10% ~ 30%;
Wherein, described resol is the p-tert-butylphenol mela mine-formaldehyde resin, and the trade names of p-tert-butylphenol mela mine-formaldehyde resin are 2402 resol.
Wherein, the used ethyl acetate of the present invention is as solvent, and its function is for to play dissolved dilution to other raw material.
Preferably, a kind of hard plastic transparent glue, it is made up of following raw materials by weight percent:
Chlorinated rubber 10% ~ 18%
Ethylene-vinyl acetate resin 10% ~ 18%
Soluble cotton 25% ~ 38%
Resol 5% ~ 12%
Polyethylene wax 0.1% ~ 0.4%
Toluene 5% ~ 10%
Ethyl acetate 10% ~ 25%.
Preferably, a kind of hard plastic transparent glue, it is made up of following raw materials by weight percent:
Chlorinated rubber 10% ~ 16%
Ethylene-vinyl acetate resin 10% ~ 16%
Soluble cotton 25% ~ 37%
Resol 5% ~ 10%
Polyethylene wax 0.1% ~ 0.2%
Toluene 5% ~ 10%
Ethyl acetate 10% ~ 23%.
Preferably, a kind of hard plastic transparent glue, it is made up of following raw materials by weight percent:
Chlorinated rubber 15%
Ethylene-vinyl acetate resin 15%
Soluble cotton 31.3%
Resol 9%
Polyethylene wax 0.2%
Toluene 9.5%
Ethyl acetate 20%.
Preferably, a kind of hard plastic transparent glue, it is made up of following raw materials by weight percent:
Chlorinated rubber 13.9%
Ethylene-vinyl acetate resin 13%
Soluble cotton 30%
Resol 10%
Polyethylene wax 0.1%
Toluene 10%
Ethyl acetate 23%.
In the technique scheme, resol is the p-tert-butylphenol mela mine-formaldehyde resin, and the trade names of p-tert-butylphenol mela mine-formaldehyde resin are 2402 resol.
The above-mentioned hard plastic preparation method of transparent glue, it may further comprise the steps:
A, weighing each component: according to the composition of raw materials amount of described hard plastic with transparent glue, the component of weighing chlorinated rubber, ethylene-vinyl acetate resin, soluble cotton, resol, polyethylene wax, toluene and ethyl acetate respectively;
The preparation of b, mixed solvent: the toluene of weighing among the step a is added earlier in the container, add the ethyl acetate of weighing among the step a again in the container, be stirred to evenly then, namely obtain mixed solvent;
C, spice: chlorinated rubber, ethylene-vinyl acetate resin, soluble cotton, resol and the polyethylene wax of weighing among the step a are joined in the mixed solvent of step b, stir while adding simultaneously, after adding finishes, continue to stir 10min ~ 15min, namely obtain the hard plastic transparent glue.
The present invention compared with prior art, beneficial effect is:
1) the prepared hard plastic of the present invention coat with transparent glue have clarification on the gold stamping film, thorough effect, make that the original pattern that is scalded thing after the thermoprint can crested, thus make the decoration that scalded thing, intersperse and set off attractive in appearance effective.
2) the prepared hard plastic of the present invention can not produce " after-tacking " phenomenon with transparent glue in the process of depositing, thereby has improved the quality of product.
3) a kind of hard plastic of the present invention is simple with the preparation method of transparent glue.
Embodiment
The present invention is further illustrated below in conjunction with embodiment.
Embodiment 1.
The hard plastic transparent glue, it is made up of the raw material of following weight:
Chlorinated rubber 15g, ethylene-vinyl acetate resin 15g, soluble cotton 31.3g, p-tert-butylphenol mela mine-formaldehyde resin 9g, polyethylene wax 0.2g, toluene 9.5g, ethyl acetate 20g.
Above-mentioned hard plastic is as follows with the preparation method of transparent glue:
Weighing chlorinated rubber 15g, ethylene-vinyl acetate resin 15g, soluble cotton 31.3g, p-tert-butylphenol mela mine-formaldehyde resin 9g, polyethylene wax 0.2g, toluene 9.5g, ethyl acetate 20g, add above-mentioned load weighted toluene in the container earlier, in container, add above-mentioned load weighted ethyl acetate again, be stirred to then evenly, namely obtain mixed solvent; Chlorinated rubber, ethylene-vinyl acetate resin, soluble cotton, p-tert-butylphenol mela mine-formaldehyde resin and polyethylene wax with above-mentioned weighing joins in the mixed solvent then, stir while adding simultaneously, after adding finishes, continue to stir 15min, namely obtain the hard plastic transparent glue.
Embodiment 2.
The hard plastic transparent glue, it is made up of the raw material of following weight:
Chlorinated rubber 13.9g, ethylene-vinyl acetate resin 13g, soluble cotton 30g, p-tert-butylphenol mela mine-formaldehyde resin 10g, polyethylene wax 0.1g, toluene 10g, ethyl acetate 23g.
Above-mentioned hard plastic is as follows with the preparation method of transparent glue:
Weighing chlorinated rubber 13.9g, ethylene-vinyl acetate resin 13g, soluble cotton 30g, p-tert-butylphenol mela mine-formaldehyde resin 10g, polyethylene wax 0.1g, toluene 10g, ethyl acetate 23g, add above-mentioned load weighted toluene in the container earlier, in container, add above-mentioned load weighted ethyl acetate again, be stirred to then evenly, namely obtain mixed solvent; Chlorinated rubber, ethylene-vinyl acetate resin, soluble cotton, p-tert-butylphenol mela mine-formaldehyde resin and polyethylene wax with above-mentioned weighing joins in the mixed solvent then, stir while adding simultaneously, after adding finishes, continue to stir 10min, namely obtain the hard plastic transparent glue.
Embodiment 3.
The hard plastic transparent glue, it is made up of the raw material of following weight:
Chlorinated rubber 10g, ethylene-vinyl acetate resin 16g, soluble cotton 37g, p-tert-butylphenol mela mine-formaldehyde resin 8g, polyethylene wax 0.4g, toluene 9g, ethyl acetate 19.6g.
Above-mentioned hard plastic is as follows with the preparation method of transparent glue:
Weighing chlorinated rubber 10g, ethylene-vinyl acetate resin 16g, soluble cotton 37g, p-tert-butylphenol mela mine-formaldehyde resin 8g, polyethylene wax 0.4g, toluene 9g, ethyl acetate 19.6g, add above-mentioned load weighted toluene in the container earlier, in container, add above-mentioned load weighted ethyl acetate again, be stirred to then evenly, namely obtain mixed solvent; Chlorinated rubber, ethylene-vinyl acetate resin, soluble cotton, p-tert-butylphenol mela mine-formaldehyde resin and polyethylene wax with above-mentioned weighing joins in the mixed solvent then, stir while adding simultaneously, after adding finishes, continue to stir 12min, namely obtain the hard plastic transparent glue.
Embodiment 4.
The hard plastic transparent glue, it is made up of the raw material of following weight:
Chlorinated rubber 16g, ethylene-vinyl acetate resin 10g, soluble cotton 38g, p-tert-butylphenol mela mine-formaldehyde resin 7g, polyethylene wax 0.3g, toluene 8g, ethyl acetate 20.7g.
Above-mentioned hard plastic is as follows with the preparation method of transparent glue:
Weighing chlorinated rubber 16g, ethylene-vinyl acetate resin 10g, soluble cotton 38g, p-tert-butylphenol mela mine-formaldehyde resin 7g, polyethylene wax 0.3g, toluene 8g, ethyl acetate 20.7g, add above-mentioned load weighted toluene in the container earlier, in container, add above-mentioned load weighted ethyl acetate again, be stirred to then evenly, namely obtain mixed solvent; Chlorinated rubber, ethylene-vinyl acetate resin, soluble cotton, p-tert-butylphenol mela mine-formaldehyde resin and polyethylene wax with above-mentioned weighing joins in the mixed solvent then, stir while adding simultaneously, after adding finishes, continue to stir 13min, namely obtain the hard plastic transparent glue.
Embodiment 5.
The hard plastic transparent glue, it is made up of the raw material of following weight:
Chlorinated rubber 18g, ethylene-vinyl acetate resin 15g, soluble cotton 25g, p-tert-butylphenol mela mine-formaldehyde resin 5g, polyethylene wax 0.5g, toluene 11.5g, ethyl acetate 25g.
Above-mentioned hard plastic is as follows with the preparation method of transparent glue:
Weighing chlorinated rubber 18g, ethylene-vinyl acetate resin 15g, soluble cotton 25g, p-tert-butylphenol mela mine-formaldehyde resin 5g, polyethylene wax 0.5g, toluene 11.5g, ethyl acetate 25g, add above-mentioned load weighted toluene in the container earlier, in container, add above-mentioned load weighted ethyl acetate again, be stirred to then evenly, namely obtain mixed solvent; Chlorinated rubber, ethylene-vinyl acetate resin, soluble cotton, p-tert-butylphenol mela mine-formaldehyde resin and polyethylene wax with above-mentioned weighing joins in the mixed solvent then, stir while adding simultaneously, after adding finishes, continue to stir 11min, namely obtain the hard plastic transparent glue.
Embodiment 6.
The hard plastic transparent glue, it is made up of the raw material of following weight:
Chlorinated rubber 12g, ethylene-vinyl acetate resin 18g, soluble cotton 35g, p-tert-butylphenol mela mine-formaldehyde resin 12g, polyethylene wax 0.2g, toluene 12g, ethyl acetate 10.8g.
Above-mentioned hard plastic is as follows with the preparation method of transparent glue:
Weighing chlorinated rubber 12g, ethylene-vinyl acetate resin 18g, soluble cotton 35g, p-tert-butylphenol mela mine-formaldehyde resin 12g, polyethylene wax 0.2g, toluene 12g, ethyl acetate 10.8g, add above-mentioned load weighted toluene in the container earlier, in container, add above-mentioned load weighted ethyl acetate again, be stirred to then evenly, namely obtain mixed solvent; Chlorinated rubber, ethylene-vinyl acetate resin, soluble cotton, p-tert-butylphenol mela mine-formaldehyde resin and polyethylene wax with above-mentioned weighing joins in the mixed solvent then, stir while adding simultaneously, after adding finishes, continue to stir 14min, namely obtain the hard plastic transparent glue.
Embodiment 7.
The hard plastic transparent glue, it is made up of the raw material of following weight:
Chlorinated rubber 20g, ethylene-vinyl acetate resin 12g, soluble cotton 40g, p-tert-butylphenol mela mine-formaldehyde resin 6g, polyethylene wax 0.1g, toluene 5g, ethyl acetate 16.9g.
Above-mentioned hard plastic is as follows with the preparation method of transparent glue:
Weighing chlorinated rubber 20g, ethylene-vinyl acetate resin 12g, soluble cotton 40g, p-tert-butylphenol mela mine-formaldehyde resin 6g, polyethylene wax 0.1g, toluene 5g, ethyl acetate 16.9g, add above-mentioned load weighted toluene in the container earlier, in container, add above-mentioned load weighted ethyl acetate again, be stirred to then evenly, namely obtain mixed solvent; Chlorinated rubber, ethylene-vinyl acetate resin, soluble cotton, p-tert-butylphenol mela mine-formaldehyde resin and polyethylene wax with above-mentioned weighing joins in the mixed solvent then, stir while adding simultaneously, after adding finishes, continue to stir 10min, namely obtain the hard plastic transparent glue.
Embodiment 8.
The hard plastic transparent glue, it is made up of the raw material of following weight:
Chlorinated rubber 13g, ethylene-vinyl acetate resin 20g, soluble cotton 28g, p-tert-butylphenol mela mine-formaldehyde resin 15g, polyethylene wax 0.3g, toluene 8.7g, ethyl acetate 15g.
Above-mentioned hard plastic is as follows with the preparation method of transparent glue:
Weighing chlorinated rubber 13g, ethylene-vinyl acetate resin 20g, soluble cotton 28g, p-tert-butylphenol mela mine-formaldehyde resin 15g, polyethylene wax 0.3g, toluene 8.7g, ethyl acetate 15g, add above-mentioned load weighted toluene in the container earlier, in container, add above-mentioned load weighted ethyl acetate again, be stirred to then evenly, namely obtain mixed solvent; Chlorinated rubber, ethylene-vinyl acetate resin, soluble cotton, p-tert-butylphenol mela mine-formaldehyde resin and polyethylene wax with above-mentioned weighing joins in the mixed solvent then, stir while adding simultaneously, after adding finishes, continue to stir 10min, namely obtain the hard plastic transparent glue.
Should be noted that at last; above embodiment is only in order to illustrate technical scheme of the present invention; but not limiting the scope of the invention; although with reference to preferred embodiment the present invention has been done to explain; those of ordinary skill in the art is to be understood that; can make amendment or be equal to replacement technical scheme of the present invention, and not break away from essence and the scope of technical solution of the present invention.
Claims (6)
1. hard plastic transparent glue, it is characterized in that: it is made up of following raw materials by weight percent:
Chlorinated rubber 10% ~ 20%
Ethylene-vinyl acetate resin 10% ~ 20%
Soluble cotton 25% ~ 40%
Resol 5% ~ 15%
Polyethylene wax 0.1% ~ 0.5%
Toluene 5% ~ 12%
Ethyl acetate 10% ~ 30%;
Wherein, described resol is the p-tert-butylphenol mela mine-formaldehyde resin, and the trade names of p-tert-butylphenol mela mine-formaldehyde resin are 2402 resol.
2. a kind of hard plastic transparent glue according to claim 1, it is characterized in that: it is made up of following raw materials by weight percent:
Chlorinated rubber 10% ~ 18%
Ethylene-vinyl acetate resin 10% ~ 18%
Soluble cotton 25% ~ 38%
Resol 5% ~ 12%
Polyethylene wax 0.1% ~ 0.4%
Toluene 5% ~ 10%
Ethyl acetate 10% ~ 25%.
3. a kind of hard plastic transparent glue according to claim 1, it is characterized in that: it is made up of following raw materials by weight percent:
Chlorinated rubber 10% ~ 16%
Ethylene-vinyl acetate resin 10% ~ 16%
Soluble cotton 25% ~ 37%
Resol 5% ~ 10%
Polyethylene wax 0.1% ~ 0.2%
Toluene 5% ~ 10%
Ethyl acetate 10% ~ 23%.
4. a kind of hard plastic transparent glue according to claim 1, it is characterized in that: it is made up of following raw materials by weight percent:
Chlorinated rubber 15%
Ethylene-vinyl acetate resin 15%
Soluble cotton 31.3%
Resol 9%
Polyethylene wax 0.2%
Toluene 9.5%
Ethyl acetate 20%.
5. a kind of hard plastic transparent glue according to claim 1, it is characterized in that: it is made up of following raw materials by weight percent:
Chlorinated rubber 13.9%
Ethylene-vinyl acetate resin 13%
Soluble cotton 30%
Resol 10%
Polyethylene wax 0.1%
Toluene 10%
Ethyl acetate 23%.
6. any described a kind of hard plastic of claim 1 to 5 is with the preparation method of transparent glue, and it is characterized in that: it may further comprise the steps:
A, weighing each component: according to the composition of raw materials amount of described hard plastic with transparent glue, the component of weighing chlorinated rubber, ethylene-vinyl acetate resin, soluble cotton, resol, polyethylene wax, toluene and ethyl acetate respectively;
The preparation of b, mixed solvent: the toluene of weighing among the step a is added earlier in the container, add the ethyl acetate of weighing among the step a again in the container, be stirred to evenly then, namely obtain mixed solvent;
C, spice: chlorinated rubber, ethylene-vinyl acetate resin, soluble cotton, resol and the polyethylene wax of weighing among the step a are joined in the mixed solvent of step b, stir while adding simultaneously, after adding finishes, continue to stir 10min ~ 15min, namely obtain the hard plastic transparent glue.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013102411615A CN103265908A (en) | 2012-06-19 | 2013-06-18 | Transparent glue for hard plastic, and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210202856.8 | 2012-06-19 | ||
| CN 201210202856 CN102690614A (en) | 2012-06-19 | 2012-06-19 | Transparent glue water for hard plastics and preparation method of transparent glue water |
| CN2013102411615A CN103265908A (en) | 2012-06-19 | 2013-06-18 | Transparent glue for hard plastic, and preparation method thereof |
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| CN103265908A true CN103265908A (en) | 2013-08-28 |
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| CN 201210202856 Pending CN102690614A (en) | 2012-06-19 | 2012-06-19 | Transparent glue water for hard plastics and preparation method of transparent glue water |
| CN2013102411615A Pending CN103265908A (en) | 2012-06-19 | 2013-06-18 | Transparent glue for hard plastic, and preparation method thereof |
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| CN 201210202856 Pending CN102690614A (en) | 2012-06-19 | 2012-06-19 | Transparent glue water for hard plastics and preparation method of transparent glue water |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112358828A (en) * | 2020-09-01 | 2021-02-12 | 江西吉润花炮新材料科技有限公司 | Preparation method of nitrified bamboo cellulose adhesive |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102690614A (en) * | 2012-06-19 | 2012-09-26 | 东莞光群雷射科技有限公司 | Transparent glue water for hard plastics and preparation method of transparent glue water |
| CN107474456A (en) * | 2017-08-10 | 2017-12-15 | 青阳县吉祥塑胶有限公司 | A kind of ethylene vinyl acetate modification by copolymerization resins synthesis plastic cement and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102618188A (en) * | 2012-04-06 | 2012-08-01 | 上海加富橡胶制品有限公司 | Adhesive sticker for rubber products and rubber non-drying tape |
| CN102690614A (en) * | 2012-06-19 | 2012-09-26 | 东莞光群雷射科技有限公司 | Transparent glue water for hard plastics and preparation method of transparent glue water |
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2012
- 2012-06-19 CN CN 201210202856 patent/CN102690614A/en active Pending
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- 2013-06-18 CN CN2013102411615A patent/CN103265908A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102618188A (en) * | 2012-04-06 | 2012-08-01 | 上海加富橡胶制品有限公司 | Adhesive sticker for rubber products and rubber non-drying tape |
| CN102690614A (en) * | 2012-06-19 | 2012-09-26 | 东莞光群雷射科技有限公司 | Transparent glue water for hard plastics and preparation method of transparent glue water |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112358828A (en) * | 2020-09-01 | 2021-02-12 | 江西吉润花炮新材料科技有限公司 | Preparation method of nitrified bamboo cellulose adhesive |
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| CN102690614A (en) | 2012-09-26 |
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