CN103207101A - Outdoor shale gas collecting tank and method - Google Patents

Outdoor shale gas collecting tank and method Download PDF

Info

Publication number
CN103207101A
CN103207101A CN2013101207423A CN201310120742A CN103207101A CN 103207101 A CN103207101 A CN 103207101A CN 2013101207423 A CN2013101207423 A CN 2013101207423A CN 201310120742 A CN201310120742 A CN 201310120742A CN 103207101 A CN103207101 A CN 103207101A
Authority
CN
China
Prior art keywords
gas
tank body
shale
outdoor
air
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN2013101207423A
Other languages
Chinese (zh)
Inventor
薛晓辉
丁安徐
孙齐
高和群
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Petroleum and Chemical Corp
Original Assignee
China Petroleum and Chemical Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Petroleum and Chemical Corp filed Critical China Petroleum and Chemical Corp
Priority to CN2013101207423A priority Critical patent/CN103207101A/en
Publication of CN103207101A publication Critical patent/CN103207101A/en
Pending legal-status Critical Current

Links

Images

Landscapes

  • Sampling And Sample Adjustment (AREA)

Abstract

The invention relates to an outdoor shale gas collecting tank and method, which aim to prevent air from being mixed into shale gas to reduce the purity of the gas in an outdoor shale gas collecting process, are favorable to improve the precision of a gas experiment, and belong to the technical field of outdoor shale gas collecting experiments. The outdoor shale gas collecting tank provided by the invention is characterized in that the hemisphere shape of the top of the outdoor shale gas collecting tank can guarantee the gathering direction of gas and the collecting capacity of gas under small gas capacity, and generated gas extrude water in the hemisphere shape part to discharge the water out of a tank body through drain holes of a balance water pipe; in the whole process, a cavity is filled by water, air is not mixed through sealing, and thus the purity of gas is guaranteed; and the balance water pipe has important meaning for pressure and an exhaust process in a sample desorbing process. The outdoor shale gas collecting tank provided by the invention can guarantee that gas is gathered on the top of the tank body, air is prevented from mixing to cause a collecting error, and thus a precision result of an experiment is improved. The gas collecting tank and the gas collecting method applying the gas collecting tank provided by the invention are simple and useful, reduce collecting errors and guarantee outdoor shale gas collection and follow-up experiments.

Description

Open-air shale gas gas production jar and gas production method
Technical field
The present invention relates to a kind of open-air shale gas gas production jar and gas production method, is for fear of to sneaking into the purity that reduces gas because of air in the open-air shale gas gas production process, is conducive to improve the degree of accuracy of gas experiment, belongs to open-air shale gas gas production experimental technique field.
Background technology
Shale gas is as a kind of novel natural gas source, obtained success in the exploitation of countries such as the U.S., Canada, and China's shale gas distribution area is wide, it is many to grow series of strata, and resource potential is big, can fill up the shortage of China's conventional energy resources to a certain extent.Shale gas stores with ADSORPTION STATE and other mode in reservoir, the about 0.5-3m3/t of absorption tolerance.After the shale sample takes out under the reservoir conditions, because temperature, pressure changes, be adsorbed on the shale surface and intrapore gas generation desorb, migration, and discharge.Often reason makes air inevitably sneak into to general gas producing device because complicated operation, pipeline be too many etc., and particularly under the lower situation of shale gas tolerance, the field acquisition error is too big, has influenced experimental result.
Summary of the invention
The purpose of this invention is to provide a kind of open-air shale gas gas production jar and gas production method, solving existing shale gas gas producing device causes Acquisition Error too big because of easy entrained air, influence the problem of experimental result, the present invention has reduced Acquisition Error, for open-air shale gas gas collecting and subsequent experimental provide safeguard.
The objective of the invention is to realize in the following manner, a kind of open-air shale gas gas production jar, it is characterized in that, described gas production jar is the cylindric tank body of semi-spherical shape by the top, the gland bonnet that tank base connects, be arranged on tank body one side, one end connect tank body and with tank body in the balancing pipeline that communicates, the gland bonnet of the gas outlet at semi-spherical shape top and gas outlet port constitutes.
The gland bonnet of described tank base connects through the equidistant buckle that arranges, and the button in gland bonnet and the buckle is one, and the card in the buckle and tank body are one, and O-ring seal is set in the gland bonnet.
Described balancing pipeline and tank body axially parallel, the height of balancing pipeline is a little more than the height of gas outlet.
Described tank body adopts PP GRANULES and silica gel resin to make, and is the transparent body.
Described method is that the tank body with the shale sample of packing into submerges in the water of associated vessel, after being full of water in the jar bottom gland bonnet and top gas outlet is sealed with gland bonnet, takes out the tank body after the sealing then from water, carries out desorb at normal temperatures and takes pictures; By the time when assembling a certain amount of gas in the tank body, again tank body is not had in the entry, open the gland bonnet of gas outlet, utilize drainage with the gas collecting of discharging to gas-sample bottle.
The semi-spherical shape at top of the present invention can guarantee the gathering direction of gas, and under the less situation of tolerance, guarantee the collection capacity of gas, the water at the gas extruding semi-spherical shape position that produces, make its osculum through balancing pipeline discharge tank body, the overall process water enriches cavity and sealing can guarantee that air can't sneak into, improve the purity of gas, the setting of balancing pipeline has great importance for the pressure in the sample desorption process and exhaust process.The present invention guarantees that gas assembles at the tank body top, isolate air to be sneaked into and caused Acquisition Error, improved the degree of accuracy result of experiment, the gas production method of gas production jar of the present invention and application gas production jar is simple and practical, the present invention has reduced Acquisition Error, for open-air shale gas gas collecting and subsequent experimental provide guarantee.
Description of drawings
Fig. 1 is master's TV structure synoptic diagram of the present invention;
Fig. 2 is plan structure synoptic diagram of the present invention,
Among the figure, 1 gas outlet, 2 tank bodies, 3 balancing pipelines, 4 osculums, 5 buckles, 6 gland bonnets, 7 gland bonnets.
Embodiment
Further specify the present invention in conjunction with the accompanying drawings and embodiments, as shown in Figure 1, 2, gas production jar of the present invention is the tank body 2 of semi-spherical shape by the top, the gland bonnet 6 of tank body 2 bottoms, be arranged on tank body 2 one sides, one end connect tank body 2 and with tank body 2 in the balancing pipeline 3 that communicates, the gland bonnet 7 of the gas outlet 1 at semi-spherical shape top and gas outlet 1 port constitutes.The gland bonnet 6 of tank body 2 bottoms connects through the equidistant buckle that arranges 5, button in gland bonnet 6 and the buckle 5 is one, and the card in the buckle 5 and tank body 2 are one, in the gland bonnet 6 O-ring seal are set, balancing pipeline 3 and tank body 2 axially parallels, the height of balancing pipeline 3 is a little more than the height of gas outlet 1.
The gas production method of utilizing the gas production jar of the present invention, the shale sample packed into not to be had in the entry behind the tank body 2, is full of water and connects bottom gland bonnets 6 by some buckles 5 in tank body 2, and gas outlet 1 top is through gland bonnet 7 sealings, take out the tank body 2 after the sealing then, carry out desorb at normal temperatures and take pictures; By the time when assembling a certain amount of gas in the tank body 2, in the water in the associated vessel that again tank body 2 submerged, open the gland bonnet 7 of gas outlet 1, utilize drainage with the gas collecting of discharging to gas-sample bottle, deliver to the laboratory and detect.
Tank body 2 of the present invention adopts PP GRANULES and silica gel resin to make, and can guarantee stability, and transparent tank body also can satisfy the needs of visual observation.

Claims (5)

1. open-air shale gas gas production jar, it is characterized in that, described gas production jar is a cylindric tank body of semi-spherical shape by the top, the gland bonnet that tank base connects, be arranged on tank body one side, one end connect tank body and with tank body in the balancing pipeline that communicates, the gland bonnet of the gas outlet at semi-spherical shape top and gas outlet port constitutes.
2. open-air shale gas gas production jar according to claim 1 is characterized in that, the gland bonnet of described tank base connects through the equidistant buckle that arranges, and the button in gland bonnet and the buckle is one, and the card in the buckle and tank body are one, and O-ring seal is set in the gland bonnet.
3. open-air shale gas gas production jar according to claim 1 is characterized in that, described balancing pipeline and tank body axially parallel, and the height of balancing pipeline is a little more than the height of gas outlet.
4. open-air shale gas gas production jar according to claim 1 is characterized in that, described tank body adopts PP GRANULES and silica gel resin to make, and is the transparent body.
5. the gas production method of an open-air shale gas gas production jar, it is characterized in that, described method is that the tank body with the shale sample of packing into does not have in the entry, after being full of water in the jar, bottom gland bonnet and top gas outlet are sealed through gland bonnet, from water, take out the tank body after the sealing then, carry out desorb at normal temperatures and take pictures; By the time when assembling a certain amount of gas in the tank body, again tank body is not had in the entry, open the gland bonnet of gas outlet, utilize drainage with the gas collecting of discharging to gas-sample bottle.
CN2013101207423A 2013-04-09 2013-04-09 Outdoor shale gas collecting tank and method Pending CN103207101A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2013101207423A CN103207101A (en) 2013-04-09 2013-04-09 Outdoor shale gas collecting tank and method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2013101207423A CN103207101A (en) 2013-04-09 2013-04-09 Outdoor shale gas collecting tank and method

Publications (1)

Publication Number Publication Date
CN103207101A true CN103207101A (en) 2013-07-17

Family

ID=48754393

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2013101207423A Pending CN103207101A (en) 2013-04-09 2013-04-09 Outdoor shale gas collecting tank and method

Country Status (1)

Country Link
CN (1) CN103207101A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105092314A (en) * 2014-05-23 2015-11-25 中国石油化工股份有限公司 Apparatus for collecting head-space gas, and method using apparatus
CN107314919A (en) * 2017-07-18 2017-11-03 贵州大学 A kind of sampling sampling and testing device for shale gas exploitation
CN110631951A (en) * 2018-06-22 2019-12-31 中国石油化工股份有限公司 On-site detection device and method for shale desorption gas

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU1700433A1 (en) * 1990-01-10 1991-12-23 Уфимский Нефтеперерабатывающий Завод Им.Ххп Съезда Кпсс Gas sampling probe
JPH079433A (en) * 1993-06-24 1995-01-13 Zenkoku Nama Concrete Kogyo Kumiai Rengokai Method and apparatus for measuring amount of admixture uncured concrete
JP2601735B2 (en) * 1991-07-04 1997-04-16 新コスモス電機株式会社 Method and apparatus for measuring the amount of admixture in uncured concrete
CN1614388A (en) * 2003-11-06 2005-05-11 哈尔滨工业大学 Measuring equipment for gas content of fresh concrete
CN101318150A (en) * 2007-12-14 2008-12-10 王庆良 Gas collection apparatus with water discharge method
CN201653760U (en) * 2010-04-01 2010-11-24 张金川 Seal pot
CN203203839U (en) * 2013-04-09 2013-09-18 中国石油化工股份有限公司 Field shale gas collecting tank

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU1700433A1 (en) * 1990-01-10 1991-12-23 Уфимский Нефтеперерабатывающий Завод Им.Ххп Съезда Кпсс Gas sampling probe
JP2601735B2 (en) * 1991-07-04 1997-04-16 新コスモス電機株式会社 Method and apparatus for measuring the amount of admixture in uncured concrete
JPH079433A (en) * 1993-06-24 1995-01-13 Zenkoku Nama Concrete Kogyo Kumiai Rengokai Method and apparatus for measuring amount of admixture uncured concrete
CN1614388A (en) * 2003-11-06 2005-05-11 哈尔滨工业大学 Measuring equipment for gas content of fresh concrete
CN101318150A (en) * 2007-12-14 2008-12-10 王庆良 Gas collection apparatus with water discharge method
CN201653760U (en) * 2010-04-01 2010-11-24 张金川 Seal pot
CN203203839U (en) * 2013-04-09 2013-09-18 中国石油化工股份有限公司 Field shale gas collecting tank

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105092314A (en) * 2014-05-23 2015-11-25 中国石油化工股份有限公司 Apparatus for collecting head-space gas, and method using apparatus
CN105092314B (en) * 2014-05-23 2020-01-24 中国石油化工股份有限公司 Apparatus for headspace collection and method of using the same
CN107314919A (en) * 2017-07-18 2017-11-03 贵州大学 A kind of sampling sampling and testing device for shale gas exploitation
CN110631951A (en) * 2018-06-22 2019-12-31 中国石油化工股份有限公司 On-site detection device and method for shale desorption gas
CN110631951B (en) * 2018-06-22 2021-11-09 中国石油化工股份有限公司 On-site detection device and method for shale desorption gas

Similar Documents

Publication Publication Date Title
CN107860681B (en) Gas adsorption and desorption characteristic testing device and method for pre-adsorbing moisture coal sample
CN102053141B (en) Method for testing desorption characteristic of externally added water on gas-containing coal body
CN102120161B (en) Testing simulation system for generation process of diffusion hydrates in precipitates and testing method thereof
CN104360021A (en) Testing device for simulating exploitation of natural gas hydrate from deep-sea energy soil
CN103148888B (en) A kind of coalbed methane reservoir bilayer closes adopts High Temperature High Pressure mining dynamic estimation system
CN102162779B (en) Triaxial test device for in-situ generation and decomposition of natural gas hydrate
CN102967525A (en) Experiment device for replacing CH4 in adsorption storage layer by multi-phase-state CO2 and mixed gas
CN203133063U (en) Laboratory simulation device of undisturbed soil column
CN108844850A (en) Shale adsorption-desorption and decompression exploitation simulator and method based on dynamic equilibrium
CN103207101A (en) Outdoor shale gas collecting tank and method
CN203203897U (en) Shale residual gas determining sample tank
CN107202736A (en) A kind of multifunctional water compound characteristic test experimental device
CN104316428A (en) Shale adsorbed gas content analysis system
CN106769507B (en) Seal simulation experiment method up for safekeeping in multi- scenarios method condition carbon dioxide coal seam
CN102562011A (en) Experiment system for high-pressure outcrop plane model
CN204439490U (en) A kind of parsing tank testing shale air content
CN203203839U (en) Field shale gas collecting tank
CN203083991U (en) Endogenous release device for nutritive salt of sediment
CN204165857U (en) Based on the system analyzed shale gas adsorbed gas content
CN102478467B (en) Physical absorption gas degassing cylinder, degasser and degassing method
CN203203849U (en) Gas extractor for extracting core gas in vacuum gas collector in natural gas hydrate exploration field
CN204462114U (en) A kind of nitrogen fracturing coal seam energy variation and permeability proving installation
CN207336285U (en) A kind of water filling is to desorption of mash gas characteristic experimental apparatus
CN209559604U (en) A kind of coal petrography sample negative-pressure saturation device
CN102980973A (en) Water rock chemical action device

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C02 Deemed withdrawal of patent application after publication (patent law 2001)
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20130717