CN107314919A - A kind of sampling sampling and testing device for shale gas exploitation - Google Patents

A kind of sampling sampling and testing device for shale gas exploitation Download PDF

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Publication number
CN107314919A
CN107314919A CN201710585879.4A CN201710585879A CN107314919A CN 107314919 A CN107314919 A CN 107314919A CN 201710585879 A CN201710585879 A CN 201710585879A CN 107314919 A CN107314919 A CN 107314919A
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CN
China
Prior art keywords
sampling
connecting tube
housing
steel cylinder
valve
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Pending
Application number
CN201710585879.4A
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Chinese (zh)
Inventor
张义平
陈奕羲
李波波
史正璞
张磊
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Guizhou University
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Guizhou University
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Priority to CN201710585879.4A priority Critical patent/CN107314919A/en
Publication of CN107314919A publication Critical patent/CN107314919A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/22Devices for withdrawing samples in the gaseous state
    • G01N1/2202Devices for withdrawing samples in the gaseous state involving separation of sample components during sampling

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Biomedical Technology (AREA)
  • Molecular Biology (AREA)
  • Physics & Mathematics (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

A kind of sampling sampling and testing device for shale gas exploitation of the invention, including housing, first pressure table and cover plate, the probe are fixedly connected in the naked section connecting tube outside housing, and probe and the junction of connecting tube are socketed with flange ring;The deep cooling stop valve is arranged on connecting tube and entered at housing;Electrical heating pressure regulator valve is provided with the connecting tube of the enclosure interior;Connecting tube between the surge tank and sampling steel cylinder taps out two connecting tubes respectively, and two connecting tubes separated are both connected on outlet connecting pipe;Safety valve is provided with the connecting tube that described first separates;Second pressure table is provided with the connecting tube that described second separates;The outlet connecting pipe outer end is connected with second pressure table;Present invention buffering tank field is two regions separated with sampling steel cylinder region, and there is the setting at stainless steel separator interval centre, is conducive to avoiding outside air contaminated samples, can completely cut off air, total system is not in contact with external environment.

Description

A kind of sampling sampling and testing device for shale gas exploitation
Technical field
The present invention relates to gas detection technology field, more particularly to a kind of sampling sampling and testing for shale gas exploitation Device.
Background technology
Shale gas refers to preservation in rich organic matter mud shale and its interlayer, to adsorb with free state as the side of being primarily present The Unconventional gas of formula, composition is a kind of cleaning, efficient energy resources and industrial chemicals, is mainly used in based on methane Resident's combustion gas, city heat supply, generating, motor vehicle fuel and Chemical Manufacture etc., it is widely used.Typically need not in shale gas production process Draining, the production cycle is long, generally 30 years~50 years, and exploration and development success rate is high, is worth with higher industrial economy.China Shale gas resource potential is big, and China's shale gas mining resources amount is in 36.1 tcms according to a preliminary estimate, with conventional gas phase When about 36.8 tcms of slightly less than shallow coal bed gas geological resources.
The inventors discovered that, it is difficult to solution source of the gas more existing shale gas gas production sampler and easily contacts general context Problem, and gas production flow is complicated, and the waste gas after collection cannot be focused on, and easily cause problem of environmental pollution.
Then, inventor in view of this, adhere to the relevant industries for many years it is abundant design and develop and actual fabrication experience, Improvement is studied there is provided a kind of sampling sampling and testing device for shale gas exploitation for existing structure and missing, To reach the purpose for having more more practical value.
The content of the invention
It is above-mentioned to solve it is an object of the invention to provide a kind of sampling sampling and testing device for shale gas exploitation The gas producing device complex operation that is proposed in background technology, easily cause the problem of sample and environmental pollution.
Purpose and effect of the present invention for the sampling sampling and testing device of shale gas exploitation, by technology hand in detail below Section is reached:
A kind of sampling sampling and testing device for shale gas exploitation, wherein, this is used for the sampling of shale gas exploitation Sampling and testing device includes:
Housing, probe, connecting tube, deep cooling stop valve, electrical heating pressure regulator valve, surge tank, sampling steel cylinder, second pressure table, Generator, gas sampling tank, safety valve, first pressure table and cover plate;
The probe is fixedly connected in the exposed connecting tube outside housing, and probe and the junction of connecting tube are socketed with Flange ring;The deep cooling stop valve is arranged on connecting tube and entered at housing;Electrical heating is provided with the connecting tube of the enclosure interior Pressure regulator valve;The electrical heating pressure regulator valve is connected with being arranged on the generator of hull outside right-hand member;Under the electrical heating pressure regulator valve Side is connected with surge tank by connecting tube;The surge tank is seated in the bottom in housing;First is provided with the surge tank Pressure gauge, and first pressure table extends outwardly into hull outside;The surge tank top right side is connected with sampling steel cylinder, and sampling Steel cylinder accumbency is in housing inner bottom part;Connecting tube between the surge tank and sampling steel cylinder taps out two connecting tubes respectively, and Two connecting tubes separated are both connected on outlet connecting pipe;Safety valve is provided with the connecting tube that described first separates;Institute State and be provided with second pressure table in second connecting tube separated;The outlet connecting pipe outer end is connected with second pressure table;Institute Gas sampling tank is stated to be seated in the supporting plate of housing;The cover plate is hinged on housing by hinge.
Further, the surge tank region is two regions separated with sampling steel cylinder region, and centre has stainless Steel diaphragm interval.
Further, the sampling steel cylinder two ends, which are provided between stop valve, and stop valve and sampling steel cylinder, passes through Flange links together.
Further, the take-off when spring in the safety valve is the active force of compression 2MPa atmospheric pressure.
With existing structure in comparison, the invention has the advantages that:
1. surge tank region of the present invention is two regions separated with sampling steel cylinder region, and there is stainless steel separator centre The setting at interval, is conducive to avoiding outside air contaminated samples, can completely cut off air, total system is not connected with external environment Touch.
Connected 2. sampling steel cylinder two ends of the present invention are provided between stop valve, and stop valve and sampling steel cylinder by flange The setting being connected together, is conducive to the simplicity of operation, and the gas in pipe can be disconnected when carrying out and taking sampling steel cylinder Source, it is to avoid cause danger.
The setting of take-off, is conducive to avoiding when 3. the spring in safety valve of the present invention is the active force of compression 2MPa atmospheric pressure System pressure, which jumps, causes danger, and can carry out pressure release in time when pressure reaches limit value.
Brief description of the drawings
Fig. 1 is structure schematic cross-sectional view of the present invention;
Fig. 2 is schematic structural view of the invention.
In figure:1st, housing, 2, probe, 3, connecting tube, 4, deep cooling stop valve, 5, electrical heating pressure regulator valve, 6, surge tank, 7, take Sample steel cylinder, 8, second pressure table, 9, generator, 10, gas sampling tank, 11, safety valve, 12, first pressure table, 13, cover plate.
Embodiment
Below, embodiments of the invention are will be explained in, the example is shown in the accompanying drawings and the description below.Although will combine The exemplary embodiment description present invention, it is to be understood that the description is not really wanted to limit the invention to the exemplary implementation Example.On the contrary, the present invention will not only cover the exemplary embodiment, but also cover various replacements, change, it is equivalent and Other embodiment, it can be included in the spirit and scope of the present invention that appended claims are limited.
Referring to Fig. 1 to accompanying drawing 2, a kind of sampling sampling and testing device for shale gas exploitation includes:
Housing 1, probe 2, connecting tube 3, deep cooling stop valve 4, electrical heating pressure regulator valve 5, surge tank 6, sampling steel cylinder 7, second Pressure gauge 8, generator 9, gas sampling tank 10, safety valve 11, first pressure table 12 and cover plate 13;
Probe 2 is fixedly connected in the exposed connecting tube 3 outside housing 1, and probe 2 and the junction of connecting tube 3 are socketed There is flange ring;Deep cooling stop valve 4 is arranged on connecting tube 3 and entered at housing 1;Electrical heating tune is provided with connecting tube 3 inside housing 1 Pressure valve 5;Electrical heating pressure regulator valve 5 is connected with being arranged on the generator 9 of the outside right-hand member of housing 1;The lower section of electrical heating pressure regulator valve 5 passes through Connecting tube 3 is connected with surge tank 6;Surge tank 6 is seated in the bottom in housing 1;First pressure table 12 is provided with surge tank 6, And first pressure table 12 extends outwardly into the outside of housing 1;The top right side of surge tank 6 is connected with sampling steel cylinder 7, and sampling steel cylinder 7 Accumbency is in the inner bottom part of housing 1;Connecting tube 3 between surge tank 6 and sampling steel cylinder 7 taps out two connecting tubes 3 respectively, and separates Two connecting tubes 3 be both connected on outlet connecting pipe 3;Safety valve 11 is provided with the connecting tube 3 that first separates;Second Second pressure table 8 is provided with the connecting tube 3 separated;The outer end of outlet connecting pipe 3 is connected with second pressure table 8;Gas sampling tank 10 are seated in the supporting plate of housing 1;Cover plate 13 is hinged on housing 1 by hinge;Connecting tube 3 is led to each several part equipment room Cross flange connection.
The preferred embodiment of the sampling sampling and testing device for being used for shale gas exploitation as described above, wherein, buffering The region of tank 6 is two regions separated with the region of sampling steel cylinder 7, and there is stainless steel separator interval centre, using sealing and circulating The mode of sampling avoids outside air contaminated samples, can completely cut off air, total system is not in contact with external environment;
The preferred embodiment of the sampling sampling and testing device for being used for shale gas exploitation as described above, wherein, sampling The two ends of steel cylinder 7 are provided between stop valve, and stop valve and sampling steel cylinder 7 and linked together by flange, make operation more Simply, the source of the gas in pipe 3 can be disconnected when carrying out and taking sampling steel cylinder 7, it is to avoid cause danger;
The preferred embodiment of the sampling sampling and testing device for being used for shale gas exploitation as described above, wherein, safety Take-off when spring in valve 11 is the active force of compression 2MPa atmospheric pressure, it is to avoid system pressure, which jumps, causes danger, and is reached in pressure To pressure release can be carried out during limit value in time.
The operation principle of the present embodiment:
When being used for the sampling sampling and testing device of shale gas exploitation using this, the device is promoted first to shale gas production Pipeline is reserved at, and probe 2 and shale flowline are connected by flange, checks each good pipeline switch shape State, confirm it is errorless after, open generator 9, opening deep cooling stop valve 4 makes source of the gas enter surge tank 6, shale gas passes through one section of device After time, talent will be proceeded by again after the impurity emptying in device, seen by the exposed first pressure table 12 in the outside of housing 1 Pressure in surge tank 6 is examined, by controlling electrical heating pressure regulator valve 5 to adjust temperature, and then the purpose of control pressure, steel to be sampled is reached After gas is full of in bottle 7, the stop valve at the two ends of sampling steel cylinder 7 is closed, by-pass valve is opened, shale gas is passed through by by-pass useless In gas collecting tank 10, the lower sampling steel cylinder 7 of dismounting send laboratory to be tested, the shale gas collected in gas sampling tank 10 is through inspection It can continue to use in access subsequent pipeline after survey is qualified, and then complete a series of operating process.
It should be noted that the standardized element that the present invention is used can commercially, shaped piece is according to explanation Book and accompanying drawing record can carry out customized, and the specific connected mode of each part is using spiral shell ripe in the prior art The conventional meanses such as bolt, rivet, welding, machinery, part and equipment are used in the prior art, conventional model, and inventor is herein No longer it is described in detail.
In summary, although the present invention is described in detail with reference to the foregoing embodiments, for the technology of this area For personnel, it can still modify to the technical scheme described in foregoing embodiments, or to which part technology Feature carries out equivalent substitution, within the spirit and principles of the invention, any modification, equivalent substitution and improvements made etc., It should be included within protection scope of the present invention.

Claims (4)

1. a kind of sampling sampling and testing device for shale gas exploitation, it is characterised in that:Described is used for shale gas exploitation Sampling sampling and testing device includes:
Housing, probe, connecting tube, deep cooling stop valve, electrical heating pressure regulator valve, surge tank, sampling steel cylinder, second pressure table, generating Machine, gas sampling tank, safety valve, first pressure table and cover plate;
The probe is fixedly connected in the exposed connecting tube outside housing, and probe and the junction of connecting tube are socketed with flange Ring;The deep cooling stop valve is arranged on connecting tube and entered at housing;Electrical heating pressure regulation is provided with the connecting tube of the enclosure interior Valve;The electrical heating pressure regulator valve is connected with being arranged on the generator of hull outside right-hand member;It is logical below the electrical heating pressure regulator valve Cross connecting tube and be connected with surge tank;The surge tank is seated in the bottom in housing;First pressure is provided with the surge tank Table, and first pressure table extends outwardly into hull outside;The surge tank top right side is connected with sampling steel cylinder, and sampling steel cylinder Accumbency is in housing inner bottom part;Connecting tube between the surge tank and sampling steel cylinder taps out two connecting tubes respectively, and separates Two connecting tubes be both connected on outlet connecting pipe;Safety valve is provided with the connecting tube that described first separates;Described Second pressure table is provided with the connecting tube that two separate;The outlet connecting pipe outer end is connected with second pressure table;It is described useless Gas collecting tank is seated in the supporting plate of housing;The cover plate is hinged on housing by hinge.
2. the sampling sampling and testing device according to claim 1 for shale gas exploitation, it is characterised in that:It is described slow It is two regions separated that tank field domain, which is rushed, with sampling steel cylinder region, and there is stainless steel separator interval centre.
3. the sampling sampling and testing device according to claim 1 for shale gas exploitation, it is characterised in that:It is described to take Sample steel cylinder two ends are provided between stop valve, and stop valve and sampling steel cylinder to be linked together by flange.
4. the sampling sampling and testing device according to claim 1 for shale gas exploitation, it is characterised in that:The peace Take-off when spring in full valve is the active force of compression 2MPa atmospheric pressure.
CN201710585879.4A 2017-07-18 2017-07-18 A kind of sampling sampling and testing device for shale gas exploitation Pending CN107314919A (en)

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CN201710585879.4A CN107314919A (en) 2017-07-18 2017-07-18 A kind of sampling sampling and testing device for shale gas exploitation

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Application Number Priority Date Filing Date Title
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111272503A (en) * 2020-04-07 2020-06-12 北部湾大学 Karst area shale gas is opened sampling article testing arrangement
CN112478437A (en) * 2020-12-11 2021-03-12 迈瑞尔实验设备(上海)有限公司 Sampling box

Citations (12)

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Publication number Priority date Publication date Assignee Title
CN201575947U (en) * 2009-09-01 2010-09-08 陕西电力科学研究院 Environment-friendly anti-pollution SF6 collection and detection device
CN103207101A (en) * 2013-04-09 2013-07-17 中国石油化工股份有限公司 Outdoor shale gas collecting tank and method
CN103245588A (en) * 2013-05-17 2013-08-14 国家地质实验测试中心 Gas content measurement and gas collection device
CN103487593A (en) * 2013-09-18 2014-01-01 中国科学院微电子研究所 Gas analysis device and method
CN203443817U (en) * 2013-09-05 2014-02-19 上海锐宇流体系统有限公司 Liquefied natural gas sampling system with buffer tank
CN204649366U (en) * 2015-05-25 2015-09-16 先尼科化工(上海)有限公司 A kind of leak test detection platform
CN105067392A (en) * 2015-07-16 2015-11-18 苏州华达仪器设备有限公司 Regular, quantitative and automatic gas sampling device
CN205228896U (en) * 2015-12-12 2016-05-11 广东电网有限责任公司江门供电局 Gaseous test sampling device of multi -functional SF6
CN205301018U (en) * 2016-01-11 2016-06-08 北京安赛克科技有限公司 Flue gas composition detection device
CN205538320U (en) * 2016-01-20 2016-08-31 抚顺市博瑞特科技有限公司 Sampling steel bottle keeps warm
CN106353238A (en) * 2016-10-31 2017-01-25 贵州大学 Auxiliary device for permeability test of shale sample
CN206990284U (en) * 2017-07-18 2018-02-09 贵州大学 A kind of sampling sampling and testing device for shale gas exploitation

Patent Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201575947U (en) * 2009-09-01 2010-09-08 陕西电力科学研究院 Environment-friendly anti-pollution SF6 collection and detection device
CN103207101A (en) * 2013-04-09 2013-07-17 中国石油化工股份有限公司 Outdoor shale gas collecting tank and method
CN103245588A (en) * 2013-05-17 2013-08-14 国家地质实验测试中心 Gas content measurement and gas collection device
CN203443817U (en) * 2013-09-05 2014-02-19 上海锐宇流体系统有限公司 Liquefied natural gas sampling system with buffer tank
CN103487593A (en) * 2013-09-18 2014-01-01 中国科学院微电子研究所 Gas analysis device and method
CN204649366U (en) * 2015-05-25 2015-09-16 先尼科化工(上海)有限公司 A kind of leak test detection platform
CN105067392A (en) * 2015-07-16 2015-11-18 苏州华达仪器设备有限公司 Regular, quantitative and automatic gas sampling device
CN205228896U (en) * 2015-12-12 2016-05-11 广东电网有限责任公司江门供电局 Gaseous test sampling device of multi -functional SF6
CN205301018U (en) * 2016-01-11 2016-06-08 北京安赛克科技有限公司 Flue gas composition detection device
CN205538320U (en) * 2016-01-20 2016-08-31 抚顺市博瑞特科技有限公司 Sampling steel bottle keeps warm
CN106353238A (en) * 2016-10-31 2017-01-25 贵州大学 Auxiliary device for permeability test of shale sample
CN206990284U (en) * 2017-07-18 2018-02-09 贵州大学 A kind of sampling sampling and testing device for shale gas exploitation

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111272503A (en) * 2020-04-07 2020-06-12 北部湾大学 Karst area shale gas is opened sampling article testing arrangement
CN112478437A (en) * 2020-12-11 2021-03-12 迈瑞尔实验设备(上海)有限公司 Sampling box

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Application publication date: 20171103