CN103173295B - Smokeless environment-friendly birthday candle with color flame - Google Patents
Smokeless environment-friendly birthday candle with color flame Download PDFInfo
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Abstract
The invention discloses a smokeless environment-friendly birthday candle with a color flame and a preparation method of the smokeless environment-friendly birthday candle. The preparation method comprises the following steps of: with trimethyl citrate as a main combustible ingredient and octadecanamide, stearic acid and tristearin as a plasticizer, an emulsifying agent, a releasing agent and a dispersing agent, additionally adding erucamide, oleamide, propyl gallate, 2-hydroxy-4-n-octyloxybenzophenone, triclosan, 10,10'-oxybisphenoxarsine and an alcohol solubility pigment, melting all the materials at the temperature of 90-95 DEG C, and uniformly mixing the melted materials to obtain a candle material; dissolving a color flame color former in purified water to prepare a color forming liquid with the mass concentration of 3-6%, placing a cotton thread into the color forming liquid to soak for 2-24hours, then, taking the cotton thread out and drying the cotton thread to obtain a wick; and threading the wick on a candle machine, pouring the candle material on the machine, introducing cooling water, solidifying the candle material, then, forming and carrying out mould stripping. The preparation method is simple in production process, low in cost, labor-saving and suitable for large-scale mechanical production; and the produced candle with the flame is stable in flame, bright and pure in color of the flame, free of smoke and lachrymation in combustion and long in quality guarantee period.
Description
Technical field
The present invention relates to a kind of color flame candles and preparation method thereof, specifically coloured flame birthday candle of a kind of smokeless environment-friendly and preparation method thereof.
Background technology
Color flame candles technology is in the market substantially using trimethyl citrate as main fuel, using stearic amide, stearic acid or Tristearoylglycerol etc. as softening agent, emulsifying agent, releasing agent, dispersion agent and ignition dope, the activator using oil color as outward appearance, with lithium, potassium, sodium, copper, calcium, magnesium, boron, the metal-salts such as barium are as chromogenic reagent.Wick mainly adopts two, as patent documentation CN102559397A, in order to make candle send the bright-coloured flame color such as red, yellow, blue, green, purple, white, has adopted twin-core processing, and color development core of a burning core is kneaded into wick.
Though the document about color flame candles is many, but rare color flame candles product on the market, trace it to its cause, it is mainly the problem of depositing in the following areas: (1) poor stability: existing color flame candles is generally affected by climate change larger, storage time is short, the storage time of some half a year all cannot realize, especially southern humid area.Conventionally can due to occur efflorescence, mouldy, fade, the problem such as the moisture absorption, thereby seriously restricted the sale of product.(2) complex process: wick generally passes through multiple working procedure processing, as the CN100557004C of patent documentation, wick has passed through alkali, sour repeatedly soaking for a long time, and length consuming time, also needs to expend a large amount of labor forces.(3) mechanization degree is low: because the current cold contraction of color flame candles formula material is smaller, determine that it must complete making processes by splitting mould, this just needs a large amount of labor forces, under the environment that labor cost increases severely at present, is not suitable for batch production and is also unfavorable for promoting.(4) quality is unsecured: be mainly reflected in the following aspects: first, make in color flame candles technology current, Tristearoylglycerol and stearic acid separately use often, only use Tristearoylglycerol or stearic acid.While only using Tristearoylglycerol, because its oiliness is large, therefore often swim in above wax material in a large number, and be difficult for being dissolved in completely in wax material, cause wax material to mix inhomogeneous, the color flame candles that causes upper strata wax material to be prepared is defective, and sends yellow flame.In the time only using stearic acid, consumption is wayward, and in the time that consumption is very few, toughness is inadequate, easily crisp, in the time that consumption is too much, can form spray sour phenomenon, cause color flame candles occur yellow core and surface colour inhomogeneous.(5) appearance looks elegant degree is inadequate, not easy coloring and painted inhomogeneous.Many documents are recorded and are nearly all adopted oil color, as: document CN102268330A and CN101870928A etc.But through overtesting oil color and trimethyl citrate mutual solubility poor be difficult to painted or some pigment is painted hardly, or painted inequality, the formula poor heat resistance of color flame candles at present, oxidizable even coking, in long heating production process, easily variable color is rotten, and product strength is died down, and aberration is serious, outward appearance is barely satisfactory, thereby the product appearance quality of producing can not be guaranteed.(6) many documents are to mouldy, and the phenomenons such as rotten efflorescence do not have basic solution yet.In addition, naturally dry, air-dry or dry in the shade, need the oversize time of consumption, and gravitation will make the chromogenic reagent soaking pile up toward lower, the candle of working it out through the wick drying or natural air drying obtains again, some part color development is good especially and have what look of part all can not send out, and piles up color flame agent part moisture and form stone incrustation shape after dry and cannot operate.Therefore in batch production, cannot ensure the quality equilibrium of every candle.And can make wick weave construction be subject to havoc to the processing repeatedly of wick, and make it easily broken, oil absorption weakens greatly, affects combustion efficacy, therefore needs to add in addition a burning wick, has not only increased cost but also expended time in.
Summary of the invention
For the problems referred to above, the invention provides coloured flame birthday candle of a kind of smokeless environment-friendly and preparation method thereof, its reliable in quality, stability is high, technique is simple, with low cost, be suitable for mass mechanized production.
A kind of smokeless environment-friendly coloured flame birthday candle of the present invention is become by the preparation of raw material of following mass percent:
(1) all batchings are mixed in proportion, 90-95 DEG C of thawing, mixes, and makes wax material;
(2) required color flame chromogenic material is directly dissolved in to the color development liquid of making mass concentration 3-6% in pure water, adopt single Zhi Putong cotton thread to do wicking, cotton thread is placed in to color development liquid and soaks 2-24 hour, taking-up keeps flat, and puts air blast dryer into and at once dries moisture and obtain wick;
(3) wick has been measured to size on demand around pipe, be then directly through candle mechanically, the wax material having melted is cast directly over mechanically, logical upper water coolant, makes smokeless environment-friendly coloured flame birthday candle of the present invention after solidifying.
The invention has the beneficial effects as follows with respect to prior art:
(1) the present invention is combined with Tristearoylglycerol with stearic acid, the problem that perfection has existed while having solved independent use, the color flame candles making is all improved largely in hardness, intensity and flexibility, simultaneously wax material homogeneous media, very easily toning, and chromaticness is even.
(2) in wax material, added the erucicamide of 0.2-0.8% and the amine hydroxybenzene of 0.2-0.6%, candle has been had better high temperature resistantly anti-ly repeat to heat, anti-oxidant and hydrophobic function, extended the shelf life.
In addition, between material, interact, cause the contraction ratio of candle to increase, be convenient to the depanning of candle in machinery production, ensured integrity and the qualification rate of product.Make without specific installation, mechanically can process and produce suitable mass mechanized production at common candle.
(3) Tenox PG of 0.2-0.6%, the Octabenzone of 0.2-0.8% in wax material, have been added, ensure candle and melted down for a long time and repeatedly to heat and preserved pigment nondiscoloration and never degenerate and make appearance looks elegant, color homogeneous, not easy to change, not efflorescence, thereby greatly extended the quality guaranteed period, within 1 year, can there is not above physico-chemical property change even if deposit yet.
(4) in wax material add and 0.1-0.5% 10, the triclosan of the two phenoxazine arsenic of 10 '-oxo and 0.1-0.5%, thereby not only effectively raise mould fungus inhibition and other bacteriums the solution of growing essence the bad phenomenon such as the mouldy rotten and efflorescence causing, and triclosan can play and excites copper in combustion processes, to send more stable blue flame and do not go out peculiar smell in blue flame.
(5) replace oil color as outward appearance activator using alcohol dissolubility pigment, painted easy and uniform coloring in making processes, the color flame candles appearance looks elegant making.
(6)-as think that wick must will have burning core and color development core to exist simultaneously, when guarantee trouble-free burning, flame sends color, but the present invention only can address this problem with a wick, yellow, green is also without processing.Not because lacked a wick or do not processed wick and affect burning and color development effect.
(7) wick making processes is simple, do not need repeatedly to process, in cost-saving and labor force, can not cause damage to wick structure, therefore wick burning and the color development produced be respond well, and the flash baking after immersion has ensured being uniformly distributed of chromogenic reagent on wick, makes the quality balance of product consistent, even yellow, the green wick that waits also can complete without processing.
(8) flame stabilization of colour candle, bright-colored, pure, do not exist the phenomenons such as " Huang Xin " " dry branch " (through produce and research to find to produce the phenomenons such as Huang Xin be that the interpolations such as softening agent are improper and produce).
(9) environment protection smokeless, one's eyes drop millstones, therefore, in the time being inserted on cake, can not pollute cake, harmless.
(10) preparation technology simple, save labor force, efficiency is high, with low cost, taking our factory, 10 workmans, as example, produce candle per year and can exceed 1,500 ten thousand.
Embodiment
Below in conjunction with specific embodiment, the present invention will be further described.
Embodiment 1
Blushed flame candle
94.6 grams of trimethyl citrates, 2.8 grams of stearic amides, 0.6 gram of Tristearoylglycerol, 0.6 gram of stearic acid, 0.4 gram of erucicamide, 0.3 gram of amine hydroxybenzene, 0.2 gram of Tenox PG, 0.2 gram of Octabenzone, 10,0.15 gram of the two phenoxazine arsenic of 10 '-oxo, 0.14 gram of triclosan, 0.01 gram of alcohol dissolubility Pigment red.By 90 DEG C of thawings of above-mentioned materials, mix, make wax material.
Red chromogenic reagent adopts 5 grams of lithium chlorides, is fully dissolved in the pure water of 100 grams, and wick is soaked 4 hours, takes out and dries, and has measured as required size for subsequent use around pipe.The wick winding is directly through to candle mechanically, disposablely can wears 200, the wax material having melted is above cast directly over mechanically, logical upper water coolant, can moulding depanning after solidifying.
By this production method, a people just can produce 200 candles voluntarily at 5 minutes.And the wax material that produces the wax material that is not finished down and condense in mould outside also can again be refunded wax melting tank and continued to heat and reuse.The blushed flame candle flame of producing is stable, bright-colored, pure, smokeless, one's eyes drop millstones in burning.Confirm through practice, normal temperature was preserved after 1 year, and its outward appearance and burning chromophoric characteristic are without any change.
Embodiment 2
Yellow flame candle
88.98 grams of trimethyl citrates, 5.6 grams of stearic amides, 1.2 grams of Tristearoylglycerols, 1.0 grams of stearic acid, 0.8 gram of erucicamide, 0.5 gram of amine hydroxybenzene, 0.4 gram of Tenox PG, 0.7 gram of Octabenzone, 10,0.4 gram of the two phenoxazine arsenic of 10 '-oxo, 0.4 gram of triclosan, 0.02 gram of alcohol dissolubility Pigment Yellow 73.By 93 DEG C of thawings of above-mentioned materials, mix, make wax material.
Yellow wick is without special processing, because wick own just sends yellow flame color containing sodium.Measure as required wick size for subsequent use around pipe.The wick winding is directly through to candle mechanically, disposablely can wears 200, the wax material having melted is above cast directly over mechanically, logical upper water coolant, can moulding depanning after solidifying.
By this production method, a people just can produce 200 candles voluntarily at 5 minutes.And the wax material that produces the wax material that is not finished down and condense in mould outside also can again be refunded wax melting tank and continued to heat and reuse.The yellow flame candle flame of producing is stable, bright-colored, pure, smokeless, one's eyes drop millstones in burning.Confirm through practice, normal temperature was preserved after 1 year, and its outward appearance and burning chromophoric characteristic are without any change.
Embodiment 3
Purple flame candle
89.99 grams of trimethyl citrates, 4.9 grams of stearic amides, 1.0 grams of Tristearoylglycerols, 1.0 grams of stearic acid, 0.7 gram of erucicamide, 0.5 gram of amine hydroxybenzene, 0.5 gram of Tenox PG, 0.8 gram of Octabenzone, 10,0.3 gram of the two phenoxazine arsenic of 10 '-oxo, 0.3 gram of triclosan, 0.01 gram of alcohol dissolubility pigment violet.By 95 DEG C of thawings of above-mentioned materials, mix, make wax material.
Purple chromogenic reagent adopts the Repone K of 5 grams and the lithium nitrate of 1 gram, is fully dissolved in the pure water of 100 grams, soaks 24 hours, take out dry around managing for subsequent use.The wick winding is directly through to candle mechanically, disposablely can wears 200, the wax material having melted is above cast directly over mechanically, logical upper water coolant, can moulding depanning after solidifying.
By this production method, a people just can produce 200 candles voluntarily at 5 minutes.And the wax material that produces the wax material that is not finished down and condense in mould outside also can again be refunded wax melting tank and continued to heat and reuse.The purple flame candle flame stabilization, bright-colored, pure of producing, smokeless, one's eyes drop millstones in burning.Confirm through practice, normal temperature was preserved after 1 year, and its outward appearance and burning chromophoric characteristic are without any change.
Embodiment 4
Blue flame candle
94.98 grams of trimethyl citrates, 1.4 grams of stearic amides, 0.4 gram of Tristearoylglycerol, 0.4 gram of stearic acid, 0.3 gram of erucicamide, 0.3 gram of amine hydroxybenzene, 0.2 gram of zellon, 0.1 gram of clorafin, 0.4 gram of Tenox PG, 0.5 gram of Octabenzone, 10,0.5 gram of the two phenoxazine arsenic of 10 '-oxo, 0.5 gram of triclosan, 0.02 gram of alcohol dissolubility Pigment blue.By 94 DEG C of thawings of above-mentioned materials, mix, make wax material.
Blue chromogenic reagent adopts the venus crystals of 4 grams, and the cupric chloride of 2 grams is fully dissolved in the pure water of 100 grams, soaks within 2 hours, can take out dry around managing for subsequent use.The wick winding is directly through to candle mechanically, disposablely can wears 200, the wax material having melted is above cast directly over mechanically, logical upper water coolant, can moulding depanning after solidifying.
By this production method, a people just can produce 200 candles voluntarily at 5 minutes.And the wax material that produces the wax material that is not finished down and condense in mould outside also can again be refunded wax melting tank and continued to heat and reuse.The blue flame candle flame of producing is stable, bright-colored, pure, smokeless, one's eyes drop millstones in burning.Confirm through practice, normal temperature was preserved after 1 year, and its outward appearance and burning chromophoric characteristic are without any change.
Embodiment 5
Green flame candle
89.99 grams of trimethyl citrates, 3.6 grams of stearic amides, 0.9 gram of Tristearoylglycerol, 0.9 gram of stearic acid, 0.6 gram of erucicamide, 0.4 gram of amine hydroxybenzene, 0.6 gram of Tenox PG, 0.6 gram of Octabenzone, 10,0.4 gram of the two phenoxazine arsenic of 10 '-oxo, 1.5 grams of boric acid, 0.5 gram of triclosan, 0.01 gram of alcohol dissolubility Pigment green.By 92 DEG C of thawings of above-mentioned materials, mix, make wax material.
By this production method, a people just can produce 200 candles voluntarily at 5 minutes.Also can again refund wax melting tank and continue to heat and reuse and produce the wax material that is not finished down and condense in wax material above mould.The green flame candle flame of producing is stable, bright-colored, pure, smokeless, one's eyes drop millstones in burning.Confirm through practice, normal temperature was preserved after 1 year, and its outward appearance and burning chromophoric characteristic are without any change.
Yellow, the wick of green flame candle is all without processing, and what confirm and processed through practice all distinguishes without obvious aspect every quality.
Claims (7)
1. a smokeless environment-friendly coloured flame birthday candle, comprise candle body and wick, wherein candle body raw material comprises trimethyl citrate, stearic amide, Tristearoylglycerol, stearic acid, erucicamide, amine hydroxybenzene, it is characterized in that, described candle body is become by the preparation of raw material of following mass percent:
Described wick is one, preparation method is: color flame chromogenic material is dissolved in to the color development liquid of making mass concentration 3-6% in pure water, adopt single Zhi Putong cotton thread to do wicking, cotton thread is placed in to color development liquid and soaks 2-24 hour, taking-up keeps flat, and puts into air blast dryer and at once dries moisture and obtain wick.
2. the preparation method of-kind of smokeless environment-friendly coloured flame birthday candle, is characterized in that, comprises the following steps:
(1) batching described in claim 1 is mixed in proportion, 90-95 DEG C of thawing, mixes, and makes wax material;
(2) prepare wick claimed in claim 1;
(3) wick has been measured to size on demand around pipe, be then directly through candle mechanically, the wax material having melted is cast directly over mechanically, logical upper water coolant, makes smokeless environment-friendly coloured flame birthday candle of the present invention after solidifying.
3. a smokeless environment-friendly blushed flame birthday candle, is characterized in that, candle body is become by the preparation of raw material of following mass percent:
Above-mentioned raw materials is mixed to obtain to wax material in 90-95 DEG C of thawing;
5 grams of lithium chlorides are dissolved in 100 grams of pure water and make color development liquid, adopt single Zhi Putong cotton thread to do wicking, cotton thread is placed in to color development liquid and soaks 4 hours, taking-up keeps flat, and puts into air blast dryer and at once dries moisture and obtain wick;
Described wick is through to candle mechanically, and the wax material having melted casts directly over mechanically, and logical upper water coolant, solidifies aftershaping depanning and obtain blushed flame birthday candle.
4. a smokeless environment-friendly yellow flame birthday candle, is characterized in that, candle body is become by the preparation of raw material of following mass percent:
Above-mentioned raw materials is mixed to obtain to wax material in 90-95 DEG C of thawing;
Common wick is through to candle mechanically, and the wax material having melted casts directly over mechanically, and logical upper water coolant, solidifies aftershaping depanning and obtain yellow flame birthday candle.
5. a smokeless environment-friendly purple flame birthday candle, is characterized in that, candle body is become by the preparation of raw material of following mass percent:
Above-mentioned raw materials is mixed to obtain to wax material in 90-95 DEG C of thawing;
5 grams of Repone K and 1 gram of lithium nitrate are dissolved in 100 grams of pure water and make color development liquid, adopt single Zhi Putong cotton thread to do wicking, cotton thread is placed in to color development liquid and soaks 24 hours, taking-up keeps flat, and puts into air blast dryer and at once dries moisture and obtain wick;
Described wick is through to candle mechanically, and the wax material having melted casts directly over mechanically, and logical upper water coolant, solidifies aftershaping depanning and obtain purple flame birthday candle.
6. a smokeless environment-friendly blue flame birthday candle, is characterized in that, candle body is become by the preparation of raw material of following mass percent:
Above-mentioned raw materials is mixed to obtain to wax material in 90-95 DEG C of thawing;
The venus crystals of 6 grams or cupric chloride or its mixture are dissolved in 100 grams of pure water and make color development liquid, adopt single Zhi Putong cotton thread to do wicking, cotton thread is placed in to color development liquid and soaks 2 hours, taking-up keeps flat, and puts into air blast dryer and at once dries moisture and obtain wick;
Described wick is through to candle mechanically, and the wax material having melted casts directly over mechanically, and logical upper water coolant, solidifies aftershaping depanning and obtain blue flame birthday candle.
7.-kind of smokeless environment-friendly green flame birthday candle, is characterized in that, candle body is become by the preparation of raw material of following mass percent:
Above-mentioned raw materials is mixed to obtain to wax material in 90-95 DEG C of thawing;
Common wick is through to candle mechanically, and the wax material having melted casts directly over mechanically, and logical upper water coolant, solidifies aftershaping depanning and obtain green flame birthday candle.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310135152.8A CN103173295B (en) | 2013-04-18 | 2013-04-18 | Smokeless environment-friendly birthday candle with color flame |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310135152.8A CN103173295B (en) | 2013-04-18 | 2013-04-18 | Smokeless environment-friendly birthday candle with color flame |
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| CN103173295A CN103173295A (en) | 2013-06-26 |
| CN103173295B true CN103173295B (en) | 2014-06-25 |
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Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112143566B (en) * | 2020-10-12 | 2023-06-27 | 南京信息工程大学 | Biomass-based wick material and preparation method and application thereof |
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| CN1145945A (en) * | 1995-09-07 | 1997-03-26 | 王明凤 | Prodn process of color-flame candle |
| CN1343246A (en) * | 1999-03-11 | 2002-04-03 | 雷克特本克斯尔(英国)有限公司 | Candle composition |
| KR20040052552A (en) * | 2004-03-24 | 2004-06-23 | 씨.에프. 주식회사 | An candle containing a soy and wax and that composing method |
| EP1686159A1 (en) * | 2001-06-04 | 2006-08-02 | Arizona Chemical Company | Coated candles and coating compositions |
| CN101825230A (en) * | 2009-03-05 | 2010-09-08 | 范卸妹 | Novel artistic cup candle |
| CN102191136A (en) * | 2010-03-08 | 2011-09-21 | 建德市嘉轩工艺品有限公司 | Candle with color flame and manufacturing method thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20060272199A1 (en) * | 2005-06-02 | 2006-12-07 | Bmc Manufacturing, Llc | Aqueous gel candle for use with a warming device |
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2013
- 2013-04-18 CN CN201310135152.8A patent/CN103173295B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0265976A1 (en) * | 1986-09-25 | 1988-05-04 | Unilever N.V. | Fatty acid composition suitable for candle pressing |
| CN1145945A (en) * | 1995-09-07 | 1997-03-26 | 王明凤 | Prodn process of color-flame candle |
| CN1343246A (en) * | 1999-03-11 | 2002-04-03 | 雷克特本克斯尔(英国)有限公司 | Candle composition |
| EP1686159A1 (en) * | 2001-06-04 | 2006-08-02 | Arizona Chemical Company | Coated candles and coating compositions |
| KR20040052552A (en) * | 2004-03-24 | 2004-06-23 | 씨.에프. 주식회사 | An candle containing a soy and wax and that composing method |
| CN101825230A (en) * | 2009-03-05 | 2010-09-08 | 范卸妹 | Novel artistic cup candle |
| CN102191136A (en) * | 2010-03-08 | 2011-09-21 | 建德市嘉轩工艺品有限公司 | Candle with color flame and manufacturing method thereof |
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| CN103173295A (en) | 2013-06-26 |
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