CN103141838A - Preparation method and application of female calcium supplementing product - Google Patents

Preparation method and application of female calcium supplementing product Download PDF

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Publication number
CN103141838A
CN103141838A CN201310074526XA CN201310074526A CN103141838A CN 103141838 A CN103141838 A CN 103141838A CN 201310074526X A CN201310074526X A CN 201310074526XA CN 201310074526 A CN201310074526 A CN 201310074526A CN 103141838 A CN103141838 A CN 103141838A
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powder
liquid
calcium
solid
deer
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殷涌光
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Jilin china and korea animal science and technology research institute
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Jilin china and korea animal science and technology research institute
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Abstract

The invention relates to a preparation method and application of a female calcium supplementing product. The new calcium supplementing product is prepared from deer fetus, deer placenta, rana japonica oil, royal jelly and calcium-containing material. The preparation method comprises the following steps of: cleaning the deer fetus or the deer placenta or a deer fetus product or the rana japonica oil by using water, drying in air, and crushing into powder I; or drying the royal jelly, and crushing into powder I; removing impurities from calcium carbonate or pilous antler or deer bone or deer cap or deer horn or other animal bones, and crushing into powder II; mixing the powder I and the powder II in a certain ratio, and adding proper auxiliary materials such as starch to form a raw material; filling the raw material into capsules or tabletting, sterilizing, and thus obtaining female calcium supplementing powder; or hydrolyzing the powder II through an organic acid, centrifuging, and taking supernate, namely liquid I; extracting supernate from the powder I by using absolute ethanol, distilling to remove the ethanol, and drying to obtain ethanol-soluble dry powder, namely powder III; mixing the liquid I and the powder III in a certain ratio, and adding a proper amount of stabilizer serving as an auxiliary material to form a raw material; and filling the raw material into a container, sterilizing, and thus obtaining a female calcium supplementing liquid preparation or product.

Description

A kind of women preparation method and application of the goods of replenishing the calcium
Technical field
The present invention relates to a kind of end user's placenta (or Chinese medicine dried human placenta), animal placenta, deer tire, oviductus ranae, royal jelly and calcareous material prepare method and the application that the women uses the goods of replenishing the calcium.
Background technology
At present, the goods of replenishing the calcium on market are a lot, all for the goods of replenishing the calcium by the calcareous material preparation, are suitable for replenishing the calcium of children.Women's special use is replenished the calcium goods seldom.Modern study proves, the women especially middle and aged women to replenish the calcium by simple replenishing the calcium be not reach the effect of replenishing the calcium, the Horizontal correlation of female hormone in this and women's body, the level of female hormone reduces the loss that causes calcium, osteoporosis can not reach the effect of replenishing the calcium by simple replenishing the calcium.Goods, the wood frog oil machine oviductus ranae goods such as deer tire and semifluid extract of deer foetus thereof have very large benefit to women's health.People's placenta (or Chinese medicine dried human placenta), the animal placenta contains micro-female hormone in deer tire, oviductus ranae, collagen and multiple nutrients material, women especially middle and aged women uses deer tire oviductus ranae to delay senility, beautifying face and moistering lotion.Calcareous material such as calcium carbonate, deer bone, Animal Bone, bird eggshell, pilose antler etc. all contain abundant calcium, can be used as the goods of replenishing the calcium, wherein in deer bone, Animal Bone, pilose antler, the calcium-phosphorus ratio of contained calcium-phosphorus ratio and human bone is close, is more suitable for replenishing the calcium, and promotes the growth of bone.Do not mend but replenish the calcium merely, eat merely deer tire, oviductus ranae and lack again calcium, therefore, for make the women especially middle and aged women solve and to replenish the calcium, delay the loss of calcium, prevent osteoporosis, delay senility, beautifying face and moistering lotion, improve the especially general level of the health of middle and aged women of women, the present invention uses deer tire, deer placenta, and oviductus ranae and calcareous material prepare the women with the goods of replenishing the calcium, and are of great benefit to for strengthening compatriots' physique.
Summary of the invention
The object of the invention is to propose a kind of end user's placenta (or Chinese medicine dried human placenta), animal placenta, deer tire, oviductus ranae, royal jelly and calcareous material obtain the women with preparation method and the application of the goods of replenishing the calcium, and develop a kind of new goods of replenishing the calcium.
Above-mentioned purpose of the present invention is achieved through the following technical solutions:
A kind of women preparation method of the goods of replenishing the calcium, end user's placenta (or Chinese medicine dried human placenta), the animal placenta, the deer tire, oviductus ranae, royal jelly and calcareous material preparation comprise the following steps:
A) people's placenta (or Chinese medicine dried human placenta), animal placenta, deer tire, royal jelly, deer tire goods or oviductus ranae washed be ground into powder after drying, be powder one; Or royal jelly is dry, be ground into powder, be powder one;
B) with calcium carbonate, bird eggshell, pilose antler, deer bone, Cornu Cervi cowl, one or more in deer horn, or other Animal Bone uses separately or mix and use, are ground into powder at impurity elimination, are powder two;
C) powder one and powder two are mixed into powder four in the ratio of 1:1~40, add starch or the dextrin auxiliary material of powder 4 0%~200%, then add the cholecalciferol of powder two 1g:0.5~2 international units, make the raw material of supplementary calcium food, health food; Incapsulate or compressing tablet, sterilization obtains the women with the pulvis of replenishing the calcium;
D) powder two is used the organic acid acidolysis, acid hydrolysis solution is centrifugal, get supernatant, be liquid one;
E) powder one use absolute ethyl alcohol is extracted, Separation of Solid and Liquid, solid is stand-by, gets supernatant, through distillation, removes ethanol, and drying obtains pure molten dry powder, is powder three; The solid water of getting above-mentioned Separation of Solid and Liquid extracts, and Separation of Solid and Liquid is got supernatant, is liquid two;
F) liquid one is mixed with liquid two, then mix in 1:0.005~1 ratio with powder three, add 0.01~0.5% xanthans or the food stabilizers such as dextrin or carragheen or sodium carboxymethylcellulose of liquid, make the raw material of supplementary calcium food, health food; The container of packing into, sterilization obtains women's Ca-containing liquid body preparation;
G) liquid one is concentrated, drying is mixed in 1:0.005~1 ratio with powder three, makes the raw material of water-soluble women supplementary calcium food, health food; Incapsulate, compressing tablet or make dripping pill, form water-soluble women with the goods of replenishing the calcium.
In step a:
Described people's placenta (dried human placenta), deer tire or animal placenta are cleaned 2~4 times with clear water clean, with 100~120 ℃ of thermophilic digestions 5~20 minutes, sterilising and enzyme inactivating dried, and then is ground into 60~200 purpose powder, formation powder one;
Described semifluid extract of deer foetus is ground into 60~200 purpose powder, forms powder one;
Described oviductus ranae is cleaned 2~4 times with clear water clean, reject impurity, with 100~120 ℃ of thermophilic digestions 5~20 minutes, sterilising and enzyme inactivating dried, and then is ground into 60~200 purpose powder, formation powder one;
Described royal jelly was steamed 5~20 minutes with 100~120 ℃ of high temperature, sterilising and enzyme inactivating, then drying is ground into 60~200 purpose powder, forms powder one.
In step b:
Described calcium carbonate is removed impurity, is ground into 60~200 purpose powder, forms powder two;
Described bird eggshell cleans, and thermophilic digestion is removed impurity, is ground into 60~200 purpose powder, forms powder two;
Described pilose antler unhairing cleans, and steams 5~20 minutes with 100~120 ℃ of high temperature, and sterilising and enzyme inactivating dries, then is ground into 60~200 purpose powder, forms powder two; Or described pilose antler unhairing, clean and dry, then be ground into 60~200 purpose powder, form powder two;
After described pilose antler is got through water extraction, remaining solid matter is the pilose antler slag, and the pilose antler slag is dry, forms powder two; Or the pilose antler slag is added the water of 5~20 times, and add 3%~5% protease of pilose antler slag amount to carry out enzymolysis, the centrifuging and taking solid matter, drying forms powder two;
Described Cornu Cervi cowl or deer horn clean 2~4 times with clear water and clean, and steam 5~20 minutes with 100~120 ℃ of high temperature, and sterilising and enzyme inactivating dries, and then is ground into 60~200 purpose powder, form powder two; Or Cornu Cervi cowl or deer horn are cleaned for 2~4 times with the clear water cleaning, dry, then be ground into 60~200 purpose powder, form powder two; Or the powder after Cornu Cervi cowl or deer horn are pulverized adds the water of 5~20 times, adds 3%~5% protease of Cornu Cervi cowl or deer horn quality to carry out enzymolysis, the centrifuging and taking solid matter, and drying forms powder two;
Described Animal Bone comprises deer bone, ox bone, sheep bone, dog bone, Rana sylvatica Le conte bone, Animal Bone is cleaned 2~4 times with clear water clean, and impurity elimination with 100~120 ℃ of thermophilic digestions 5~20 minutes, is ground into 60~200 purpose powder, is powder two.
In steps d:
Described powder two is added the water mixing of 5~20 times, add the organic acid acidolysis, when powder two is made by calcium carbonate, bird eggshell or Animal Bone, add powder 1: citric acid 0.25~0.45: malic acid 0.25~0.45 acidolysis, acid hydrolysis solution is centrifugal, get supernatant, be liquid one;
When described powder two is made by pilose antler, pilose antler slag, deer horn or Cornu Cervi cowl, add powder 1: citric acid 0.03~0.2: malic acid 0.03~0.2 acidolysis, acid hydrolysis solution is centrifugal, get supernatant, be liquid one.
In step e:
Described powder one is added the absolute ethyl alcohol alcohol extracting of 3~20 times, Separation of Solid and Liquid, solid is stand-by, gets supernatant, through distillation, removes ethanol, and drying obtains pure molten dry powder, is powder three; The solid of getting above-mentioned Separation of Solid and Liquid adds the water of 5~20 times of solid masses, carries out water extraction and gets, and Separation of Solid and Liquid is got supernatant, is liquid two.
The described women preparation method's of the goods of replenishing the calcium application, in step e:
Described powder two is added the water of 5~20 times, mixing adds the organic acid acidolysis, when powder two by calcium carbonate or or bird eggshell or Animal Bone when making, add powder 1: citric acid 0.25~0.45: malic acid 0.25~0.45, acidolysis, acid hydrolysis solution is centrifugal, get supernatant, be liquid one; When powder two is made by pilose antler or pilose antler slag or Cornu Cervi cowl, add powder 1: citric acid 0.03~0.1: malic acid 0.03~0.1:, acidolysis, acid hydrolysis solution is centrifugal, get supernatant, be liquid one;
Described powder one is added the absolute ethyl alcohol of 3~20 times, alcohol extracting, Separation of Solid and Liquid, solid is stand-by, gets supernatant, through distillation, removes ethanol, and drying obtains pure molten dry powder, is powder three; The solid of getting above-mentioned Separation of Solid and Liquid adds the water of 8~30 times of solid masses, carries out water extraction and gets, and Separation of Solid and Liquid is got supernatant, is liquid two;
Liquid one is mixed with liquid two, be mixed into liquid three in the liquid powder than for 1:0.005~1 ratio with powder three afterwards, then be that 0.01%~1% ratio joins in white wine in liquid three, make calsium-enriched wine.
Good effect of the present invention is: utilize fully people's placenta (dried human placenta) or animal placenta or deer tire or deer tire goods or oviductus ranae or oviductus ranae goods and calcareous material resource, develop a kind of new women with the goods of replenishing the calcium.Also can be used as the raw material material of other food, health food product, make other food, health food product, as various beverages, baked product, albumen calcium drink etc.
The specific embodiment
Below by specific embodiment, preparation method of the present invention is namely used and is described in further detail:
Embodiment 1.
The women preparation method of the pulvis of replenishing the calcium
1) preparation method of powder one
(1) end user's placenta (dried human placenta) or animal placenta prepare the method for powder one:
At first people's placenta (dried human placenta) or animal placenta are cleaned 2~4 times with clear water and clean, with 100~120 ℃ of thermophilic digestions 5~20 minutes, sterilising and enzyme inactivating dried, then is ground into 60~200 purpose powder, formation powder one;
(2) use the deer tire to prepare the method for powder one:
At first the deer tire is cleaned 2~4 times with clear water and clean, with 100~120 ℃ of thermophilic digestions 5~20 minutes, sterilising and enzyme inactivating dried, then is ground into 60~200 purpose powder, formation powder one;
(3) use semifluid extract of deer foetus to prepare the method for powder one;
Semifluid extract of deer foetus is ground into 60~200 purpose powder, forms powder one;
(4) use oviductus ranae to prepare the method for powder one;
At first oviductus ranae is cleaned 2~4 times with clear water and clean, reject impurity, with 100~120 ℃ of thermophilic digestions 5~20 minutes, sterilising and enzyme inactivating dried, then is ground into 60~200 purpose powder, formation powder one;
(5) use royal jelly to prepare the method for powder one;
With 100~120 ℃ of thermophilic digestions 5~20 minutes, sterilising and enzyme inactivating dried, then is ground into 60~200 purpose powder, forms powder one with royal jelly;
2) preparation method of powder two
(1) use calcium carbonate or bird eggshell to prepare the method for powder two
Calcium carbonate or bird eggshell are cleaned, and thermophilic digestion is removed impurity, is ground into 60~200 purpose powder, forms powder two;
(2) use pilose antler to prepare the method for powder two
With the pilose antler unhairing, clean and dry, then be ground into 60~200 purpose powder, form powder two;
(3) use the pilose antler slag to prepare the method for powder two
The pilose antler slag is remaining solid matter after pilose antler is got through water extraction.The pilose antler slag is dry, form powder two; Or the pilose antler slag is added the water of 5~20 times, and add 3%~5% protease of pilose antler slag amount to carry out enzymolysis, the centrifuging and taking solid matter, drying forms powder two;
(4) use Cornu Cervi cowl (or claiming the deer pallet) or deer horn to prepare the method for powder two
Cornu Cervi cowl or deer horn are cleaned for 2~4 times with the clear water cleaning, dried, then be ground into 60~200 purpose powder, form powder two; Or the powder after Cornu Cervi cowl or deer horn are pulverized adds the water of 5~20 times, adds 3%~5% protease of Cornu Cervi cowl or deer horn quality to carry out enzymolysis, the centrifuging and taking solid matter, and drying forms powder two;
(5) use Animal Bone to prepare the method for powder two
Animal Bone is deer bone, ox bone, sheep bone, dog bone, Rana sylvatica Le conte bone etc.
Animal Bone is cleaned 2~4 times with clear water clean, impurity elimination with 100~120 ℃ of thermophilic digestions 5~20 minutes, is ground into 60~200 purpose powder, is powder two;
3) the women preparation method of the pulvis of replenishing the calcium
Powder one and powder two are mixed into powder four in the ratio of 1:1~40, add starch or the dextrin of powder 4 0%~200%, then add the cholecalciferol of powder two 1g:0.5~2 international units, be prepared into the women with the pulvis raw material of replenishing the calcium; Incapsulate or compressing tablet, obtain the women with the pulvis of replenishing the calcium.
4) the women preparation method of calsium-enriched wine
(1) above-mentioned powder two is added the water of 5~20 times, mixing adds the organic acid acidolysis.When powder two by calcium carbonate or or bird eggshell or Animal Bone when making, add powder 1: citric acid 0.25~0.45: malic acid 0.25~0.45, acidolysis, acid hydrolysis solution is centrifugal, get supernatant, be liquid one; When powder two is made by pilose antler or pilose antler slag or Cornu Cervi cowl, add powder 1: citric acid 0.03~0.1: malic acid 0.03~0.1:, acidolysis, acid hydrolysis solution is centrifugal, get supernatant, be liquid one;
(2) above-mentioned powder one is added the absolute ethyl alcohol of 3~20 times, alcohol extracting, Separation of Solid and Liquid, solid is stand-by, gets supernatant, through distillation, removes ethanol, and drying obtains pure molten dry powder, is powder three; The solid of getting above-mentioned Separation of Solid and Liquid adds the water of 5~20 times of solid masses, carries out water extraction and gets, and Separation of Solid and Liquid is got supernatant, is liquid two;
(3) liquid one is mixed with liquid two, be mixed into liquid three in the liquid powder than for 1:0.005~1 ratio with powder three afterwards, then be that 0.01%~1% ratio joins in white wine in liquid three, make calsium-enriched wine.
Embodiment 2.
The women preparation method of Ca-containing liquid body preparation
1) above-mentioned powder two is added the water of 5~20 times, mixing adds the organic acid acidolysis.When powder two by calcium carbonate or or bird eggshell or Animal Bone when making, add powder 1: citric acid 0.25~0.45: malic acid 0.25~0.45, acidolysis, acid hydrolysis solution is centrifugal, get supernatant, be liquid one; When powder two is made by pilose antler or pilose antler slag or Cornu Cervi cowl, add powder 1: citric acid 0.03~0.2: malic acid 0.03~0.2, carry out acidolysis, acid hydrolysis solution is centrifugal, get supernatant, be liquid one;
2) above-mentioned powder one is added the absolute ethyl alcohol of 3~20 times, alcohol extracting, Separation of Solid and Liquid, solid is stand-by, gets supernatant, through distillation, removes ethanol, and drying obtains pure molten dry powder, is powder three; The solid of getting above-mentioned Separation of Solid and Liquid adds the water of 5~20 times of solid masses, carries out water extraction and gets, and Separation of Solid and Liquid is got supernatant, is liquid two;
3) liquid one is mixed with liquid two, mix than for 1:0.005~1 ratio in the liquid powder with powder three afterwards, 0.01%~0.5% xanthans or the food stabilizers such as dextrin or carragheen or sodium carboxymethylcellulose that add liquid are made the raw material of supplementary calcium food, health food; The container of packing into, sterilization obtains women's Ca-containing liquid body preparation;
Embodiment 3.
The women is with the preparation method of water-soluble calcium-supplementing preparation
Above-mentioned liquid one is mixed with liquid two, and concentrated, drying is mixed than for 1:0.005~1 ratio in the liquid powder with powder three, makes the raw material of water-soluble women supplementary calcium food, health food; Incapsulate or compressing tablet or make dripping pill, form water-soluble women with the goods of replenishing the calcium.

Claims (6)

1. a women with the preparation method of the goods of replenishing the calcium, is characterized in that, end user's placenta, and the animal placenta, deer tire, oviductus ranae, royal jelly prepare with calcareous material, comprise the following steps:
A) with people's placenta, the animal placenta, deer tire, deer tire goods or oviductus ranae are ground into powder after washing and drying, and are powder one; Or royal jelly is dry, be ground into powder, be powder one;
B) with calcium carbonate, bird eggshell, pilose antler, deer bone, Cornu Cervi cowl, one or more in deer horn, or other Animal Bone impurity elimination, be ground into powder, be powder two;
C) powder one and powder two are mixed into powder four in the ratio of 1:1~40, add starch or the dextrin auxiliary material of powder 4 0%~200%, add the cholecalciferol of powder two 1g:0.5~2 international units, make the raw material of supplementary calcium food, health food; Incapsulate or compressing tablet, sterilization obtains the women with the pulvis of replenishing the calcium;
D) powder two is used the organic acid acidolysis, acid hydrolysis solution is centrifugal, get supernatant, be liquid one;
E) powder one use absolute ethyl alcohol is extracted, Separation of Solid and Liquid, solid is stand-by, gets supernatant, through distillation, removes ethanol, and drying obtains pure molten dry powder, is powder three; The solid water of getting above-mentioned Separation of Solid and Liquid extracts, and Separation of Solid and Liquid is got supernatant, is liquid two;
F) liquid one is mixed with liquid two, then mix in 1:0.005~1 ratio with powder three, add 0.01%~0.5% xanthans or the food stabilizers such as dextrin or carragheen or sodium carboxymethylcellulose of liquid, make the raw material of supplementary calcium food, health food; The container of packing into, sterilization obtains women's Ca-containing liquid body preparation;
G) liquid one is concentrated, drying is mixed in 1:0.005~1 ratio with powder three, makes the raw material of water-soluble women supplementary calcium food, health food; Incapsulate, compressing tablet or make dripping pill, form water-soluble women with the goods of replenishing the calcium.
2. a kind of women according to claim 1 with the preparation method of the goods of replenishing the calcium, is characterized in that, in step a:
Described people's placenta or animal placenta or deer tire are cleaned 2~4 times with clear water clean, with 100~120 ℃ of thermophilic digestions 5~20 minutes, sterilising and enzyme inactivating dried, and then is ground into 60~200 purpose powder, formation powder one;
Described semifluid extract of deer foetus is ground into 60~200 purpose powder, forms powder one;
Described oviductus ranae is cleaned 2~4 times with clear water clean, reject impurity, with 100~120 ℃ of thermophilic digestions 5~20 minutes, sterilising and enzyme inactivating dried, and then is ground into 60~200 purpose powder, formation powder one;
With 100~120 ℃ of thermophilic digestions 5~20 minutes, sterilising and enzyme inactivating dried, and then is ground into 60~200 purpose powder, forms powder one with described royal jelly.
3. a kind of women according to claim 1 and 2 with the preparation method of the goods of replenishing the calcium, is characterized in that, in step b:
Described calcium carbonate or bird eggshell clean, and thermophilic digestion is removed impurity, is ground into 60~200 purpose powder, forms powder two;
Described pilose antler unhairing cleans and dries, then is ground into 60~200 purpose powder, forms powder two; Or the pilose antler unhairing is cleaned with 100~120 ℃ of thermophilic digestions 5~20 minutes, sterilising and enzyme inactivating dries, and then is ground into 60~200 purpose powder, formation powder two;
After described pilose antler is got through water extraction, remaining solid matter is the pilose antler slag, and the pilose antler slag is dry, forms powder two; Or the pilose antler slag is added the water of 5~20 times, and add 3%~5% protease of pilose antler slag amount to carry out enzymolysis, the centrifuging and taking solid matter, drying forms powder two;
Described Cornu Cervi cowl or deer horn clean 2~4 times with clear water and clean, and dry, and are ground into 60~200 purpose powder, form powder two; Or Cornu Cervi cowl or deer horn clean 2~4 times with clear water and clean, and with the sterilization in 5~20 minutes of 100~120 ℃ of thermophilic digestions, dries, and then is ground into 60~200 purpose powder, formation powder two; Or the powder through sterilization (or not sterilization), after pulverizing adds the water of 5~20 times with Cornu Cervi cowl or deer horn, adds 3%~5% protease of Cornu Cervi cowl quality to carry out enzymolysis, the centrifuging and taking solid matter, and drying forms powder two;
Described Animal Bone comprises deer bone, ox bone, sheep bone, dog bone, Rana sylvatica Le conte bone, Animal Bone is cleaned 2~4 times with clear water clean, and impurity elimination with 100~120 ℃ of thermophilic digestions 5~20 minutes, degreasing, is ground into 60~200 purpose powder, is powder two.
4. a kind of women according to claim 1 and 2 with the preparation method of the goods of replenishing the calcium, is characterized in that, in steps d:
Described powder two is added the water mixing of 5~20 times, add the organic acid acidolysis, when powder two is made by calcium carbonate, bird eggshell or Animal Bone, add powder 1: citric acid 0.25~0.45: malic acid 0.25~0.45 acidolysis, acid hydrolysis solution is centrifugal, get supernatant, be liquid one;
By pilose antler, pilose antler slag, when deer horn or Cornu Cervi cowl make, add powder 1: citric acid 0.03~0.2 when described powder two: malic acid 0.03~0.2 acidolysis, acid hydrolysis solution is centrifugal, get supernatant, be liquid one.
5. a kind of women according to claim 1 and 2 with the preparation method of the goods of replenishing the calcium, is characterized in that, in step e:
Described powder one is added the absolute ethyl alcohol alcohol extracting of 3~20 times, Separation of Solid and Liquid, solid is stand-by, gets supernatant, through distillation, removes ethanol, and drying obtains pure molten dry powder, is powder three; The solid of getting above-mentioned Separation of Solid and Liquid adds the water of 5~20 times of solid masses, carries out water extraction and gets, and Separation of Solid and Liquid is got supernatant, is liquid two.
6. women as described in claim 1 or 4 with the preparation method's of the goods of replenishing the calcium application, is characterized in that, in step e:
Described powder two is added the water of 5~20 times, mixing adds the organic acid acidolysis, when powder two by calcium carbonate or or bird eggshell or Animal Bone when making, add powder 1: citric acid 0.25~0.45: malic acid 0.25~0.45, acidolysis, acid hydrolysis solution is centrifugal, get supernatant, be liquid one; When powder two is made by pilose antler or pilose antler slag or Cornu Cervi cowl, add powder 1: citric acid 0.03~0.1: malic acid 0.03~0.1:, acidolysis, acid hydrolysis solution is centrifugal, get supernatant, be liquid one;
Described powder one is added the absolute ethyl alcohol of 3~20 times, alcohol extracting, Separation of Solid and Liquid, solid is stand-by, gets supernatant, through distillation, removes ethanol, and drying obtains pure molten dry powder, is powder three; The solid of getting above-mentioned Separation of Solid and Liquid adds the water of 8~30 times of solid masses, carries out water extraction and gets, and Separation of Solid and Liquid is got supernatant, is liquid two;
Liquid one is mixed with liquid two, be mixed into liquid three in the liquid powder than for 1:0.005~1 ratio with powder three afterwards, then be that 0.01%~1% ratio joins in white wine in liquid three, make calsium-enriched wine.
CN201310074526XA 2013-03-10 2013-03-10 Preparation method and application of female calcium supplementing product Pending CN103141838A (en)

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CN104434977A (en) * 2014-12-03 2015-03-25 吉林省东鳌鹿业集团有限公司 Preparation method of calcium supplement product
CN106071972A (en) * 2016-06-08 2016-11-09 吉林省东华生物科技有限公司 A kind of preparation method of supplementation product
CN112674289A (en) * 2021-01-09 2021-04-20 贵州轩煜辰科技有限公司 Food for preventing leg cramp

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JP2002020299A (en) * 2000-07-04 2002-01-23 Fine Chemical Laboratory Co Ltd Placenta-containing sublingual tablet
CN1369222A (en) * 2002-02-08 2002-09-18 上海方远科技发展有限公司 Health-care food containing sheep placenta extract and its preparing process
JP3919123B1 (en) * 2005-12-26 2007-05-23 株式会社ベスビオ Liquid skin external preparation containing stable glutathione and liquid skin external preparation for whitening and skin containing the same
CN101032523A (en) * 2006-03-10 2007-09-12 谢春生 Royal jelly acid calcium and preparation process thereof
CN101773249A (en) * 2010-03-01 2010-07-14 宋艳 Method for preparing active peptide calcium from loach and eel bone and sheep placenta
CN102805199A (en) * 2012-08-26 2012-12-05 吉林省中韩动物科学研究院 Method for preparing pilose antler protein calcium product

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104434977A (en) * 2014-12-03 2015-03-25 吉林省东鳌鹿业集团有限公司 Preparation method of calcium supplement product
CN106071972A (en) * 2016-06-08 2016-11-09 吉林省东华生物科技有限公司 A kind of preparation method of supplementation product
CN112674289A (en) * 2021-01-09 2021-04-20 贵州轩煜辰科技有限公司 Food for preventing leg cramp

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Application publication date: 20130612