CN103131815B - 一种微波高温连续还原生产海绵铁或镍铁的工艺方法 - Google Patents
一种微波高温连续还原生产海绵铁或镍铁的工艺方法 Download PDFInfo
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- CN103131815B CN103131815B CN201310087810.0A CN201310087810A CN103131815B CN 103131815 B CN103131815 B CN 103131815B CN 201310087810 A CN201310087810 A CN 201310087810A CN 103131815 B CN103131815 B CN 103131815B
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- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 title claims abstract description 72
- 229910052742 iron Inorganic materials 0.000 title claims abstract description 34
- 230000009467 reduction Effects 0.000 title claims abstract description 25
- 238000000034 method Methods 0.000 title claims abstract description 19
- UGKDIUIOSMUOAW-UHFFFAOYSA-N iron nickel Chemical compound [Fe].[Ni] UGKDIUIOSMUOAW-UHFFFAOYSA-N 0.000 title abstract description 4
- 238000010438 heat treatment Methods 0.000 claims abstract description 36
- 239000000463 material Substances 0.000 claims abstract description 35
- 238000004519 manufacturing process Methods 0.000 claims abstract description 21
- 238000001816 cooling Methods 0.000 claims abstract description 9
- 239000003638 chemical reducing agent Substances 0.000 claims abstract description 8
- 239000000203 mixture Substances 0.000 claims abstract description 7
- 239000000843 powder Substances 0.000 claims abstract description 7
- 239000000654 additive Substances 0.000 claims abstract description 5
- 230000000996 additive effect Effects 0.000 claims abstract description 5
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 4
- 230000004044 response Effects 0.000 claims description 20
- 229910000863 Ferronickel Inorganic materials 0.000 claims description 16
- 230000005855 radiation Effects 0.000 claims description 12
- 238000007789 sealing Methods 0.000 claims description 12
- 238000009428 plumbing Methods 0.000 claims description 10
- 238000003672 processing method Methods 0.000 claims description 10
- 239000008188 pellet Substances 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 5
- 238000007885 magnetic separation Methods 0.000 claims description 5
- 238000012545 processing Methods 0.000 claims description 4
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 3
- 230000003064 anti-oxidating effect Effects 0.000 claims description 3
- 239000003245 coal Substances 0.000 claims description 3
- 239000006148 magnetic separator Substances 0.000 claims description 3
- 239000011148 porous material Substances 0.000 claims description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 2
- 239000002802 bituminous coal Substances 0.000 claims description 2
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical group [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 claims description 2
- 239000000292 calcium oxide Substances 0.000 claims description 2
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims description 2
- 239000003610 charcoal Substances 0.000 claims description 2
- 239000000571 coke Substances 0.000 claims description 2
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims description 2
- 239000000395 magnesium oxide Substances 0.000 claims description 2
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims description 2
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 claims description 2
- NDLPOXTZKUMGOV-UHFFFAOYSA-N oxo(oxoferriooxy)iron hydrate Chemical compound O.O=[Fe]O[Fe]=O NDLPOXTZKUMGOV-UHFFFAOYSA-N 0.000 claims description 2
- 230000001681 protective effect Effects 0.000 claims description 2
- 229910052814 silicon oxide Inorganic materials 0.000 claims description 2
- 238000005265 energy consumption Methods 0.000 abstract description 3
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- 238000005245 sintering Methods 0.000 abstract description 2
- 229910001030 Iron–nickel alloy Inorganic materials 0.000 abstract 2
- 238000003825 pressing Methods 0.000 abstract 2
- 229910000640 Fe alloy Inorganic materials 0.000 abstract 1
- 238000006722 reduction reaction Methods 0.000 description 19
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 8
- 230000000694 effects Effects 0.000 description 7
- 238000005516 engineering process Methods 0.000 description 5
- 238000011084 recovery Methods 0.000 description 5
- 229910052759 nickel Inorganic materials 0.000 description 4
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- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 2
- 230000005672 electromagnetic field Effects 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 238000012423 maintenance Methods 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- 235000007926 Craterellus fallax Nutrition 0.000 description 1
- 240000007175 Datura inoxia Species 0.000 description 1
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 1
- 241001417490 Sillaginidae Species 0.000 description 1
- 238000003723 Smelting Methods 0.000 description 1
- 241001062472 Stokellia anisodon Species 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
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- 150000001875 compounds Chemical class 0.000 description 1
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- 238000013461 design Methods 0.000 description 1
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- 239000000945 filler Substances 0.000 description 1
- 229910052595 hematite Inorganic materials 0.000 description 1
- 239000011019 hematite Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- LIKBJVNGSGBSGK-UHFFFAOYSA-N iron(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Fe+3].[Fe+3] LIKBJVNGSGBSGK-UHFFFAOYSA-N 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- 239000011572 manganese Substances 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000012256 powdered iron Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 230000003245 working effect Effects 0.000 description 1
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Abstract
Description
加热方式 | 还原物质重量(Kg) | 还原温度(°C) | 还原时间(Min) | 还原率(%) | 回收率(%) | 每金属吨耗费成本(万元) |
回转窑 | 1000 | 1050 | 70-120 | 60-85 | 75 | 6-8 |
本发明工艺 | 1000 | 850 | 5-60 | 95 | ≥90 | 2-3 |
Claims (4)
Priority Applications (1)
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CN201310087810.0A CN103131815B (zh) | 2013-03-19 | 2013-03-19 | 一种微波高温连续还原生产海绵铁或镍铁的工艺方法 |
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CN201310087810.0A CN103131815B (zh) | 2013-03-19 | 2013-03-19 | 一种微波高温连续还原生产海绵铁或镍铁的工艺方法 |
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CN103131815A CN103131815A (zh) | 2013-06-05 |
CN103131815B true CN103131815B (zh) | 2014-10-01 |
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CN201310087810.0A Expired - Fee Related CN103131815B (zh) | 2013-03-19 | 2013-03-19 | 一种微波高温连续还原生产海绵铁或镍铁的工艺方法 |
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Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105509464B (zh) * | 2016-01-07 | 2017-12-15 | 新冶高科技集团有限公司 | 一种红土镍矿微波低温冶炼装置 |
CN106244755B (zh) * | 2016-08-19 | 2018-06-08 | 环境保护部华南环境科学研究所 | 一种海绵铁生产装置 |
CN108048612B (zh) * | 2017-11-28 | 2019-08-20 | 辽宁科技大学 | 一种利用可再生能源在微波下还原铁鳞制备高纯海绵铁方法 |
CN108913897A (zh) * | 2018-08-06 | 2018-11-30 | 王德清 | 一种节能铬铁生产方法 |
CN108842056B (zh) * | 2018-09-07 | 2020-11-03 | 安徽工业大学 | 一种鲕状赤铁矿快速加热还原制备还原铁粉的方法 |
CN110499463A (zh) * | 2019-08-28 | 2019-11-26 | 深圳市晶莱新材料科技有限公司 | 一种微波还原铁矿石制备316l不锈钢3d打印金属粉末的方法 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1403595A (zh) * | 2002-04-22 | 2003-03-19 | 任瑞刚 | 煤-铁矿微波还原-电炉直接炼钢方法及设备 |
CN1724695A (zh) * | 2005-05-10 | 2006-01-25 | 太原理工大学 | 用微波竖炉制取低碳海绵铁的方法 |
CN101457269A (zh) * | 2008-12-30 | 2009-06-17 | 重庆高岭投资(集团)有限公司 | 微波碳热还原钢铁冶金含铁粉尘直接生产海绵铁工艺 |
CN202590777U (zh) * | 2012-06-19 | 2012-12-12 | 李学文 | 一种用于微波高温连续反应的舟车装置 |
CN202590778U (zh) * | 2012-06-19 | 2012-12-12 | 李学文 | 一种用于微波高温连续氧化、还原的装置 |
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2013
- 2013-03-19 CN CN201310087810.0A patent/CN103131815B/zh not_active Expired - Fee Related
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1403595A (zh) * | 2002-04-22 | 2003-03-19 | 任瑞刚 | 煤-铁矿微波还原-电炉直接炼钢方法及设备 |
CN1724695A (zh) * | 2005-05-10 | 2006-01-25 | 太原理工大学 | 用微波竖炉制取低碳海绵铁的方法 |
CN101457269A (zh) * | 2008-12-30 | 2009-06-17 | 重庆高岭投资(集团)有限公司 | 微波碳热还原钢铁冶金含铁粉尘直接生产海绵铁工艺 |
CN202590777U (zh) * | 2012-06-19 | 2012-12-12 | 李学文 | 一种用于微波高温连续反应的舟车装置 |
CN202590778U (zh) * | 2012-06-19 | 2012-12-12 | 李学文 | 一种用于微波高温连续氧化、还原的装置 |
Non-Patent Citations (2)
Title |
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张世敏等.微波加热钛精矿含碳球团制取初级富钛料的研究.《稀有金属》.2006,第30卷(第1期),第78-81页. |
微波加热钛精矿含碳球团制取初级富钛料的研究;张世敏等;《稀有金属》;20060228;第30卷(第1期);第78-81页 * |
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