CN103131316A - Clear wood paint and preparation method thereof - Google Patents
Clear wood paint and preparation method thereof Download PDFInfo
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- CN103131316A CN103131316A CN2013100833449A CN201310083344A CN103131316A CN 103131316 A CN103131316 A CN 103131316A CN 2013100833449 A CN2013100833449 A CN 2013100833449A CN 201310083344 A CN201310083344 A CN 201310083344A CN 103131316 A CN103131316 A CN 103131316A
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Abstract
The invention discloses a clear wood paint and a preparation method thereof, belonging to the technical field of application of paints. The invention solves the problem of poor transparency of the wood paint in the construction process, and the problem of white paint film after recoating. The clear wood paint is composed of a component A and a component B, wherein the component A is composed of an addition product of toluene diisocyanate (TDI) and trimethylolpropane or TDI tripolymer or mixture thereof, butyl acetate and ethyl acetate; the component B is composed of alkyd resin or modified alkyd resin or mixture thereof, butyl acetate, ethyl acetate, dimethylbenzene, defoaming agent, leveling agent, flatting agent, antimicrobial agent, dispersing agent, anti-settling agent and modified resin; and the weight ratio of the component A to the component B is 1:0.5 or 1:0.25. The invention also provides a preparation method of the wood paint. The wood paint disclosed by the invention has the advantage of clear and layered paint film, and can better display the beautiful texture of the wood.
Description
Technical field
The invention belongs to the application of paints technical field, be specifically related to a kind of clear wood lacquer and preparation method thereof thoroughly.
Background technology
In the product slate of China's woodwork coating, the solvent-borne type product is at present still in occupation of critical role.In the solvent-borne type woodwork coating, polyurethane coating accounts for more than 90%, wherein take two component polyurethane as main, but the transparency extreme difference of product in construction process, and the phenomenon that after recoat, paint film turns white is comparatively outstanding, can not satisfy people's demand.
Summary of the invention
The object of the present invention is to provide a kind of clear wood lacquer and preparation method thereof thoroughly, solve the transparency extreme difference of woodwork coating in construction process in prior art, and the problem that after recoat, paint film turns white.
To achieve these goals, technical scheme of the present invention is as follows:
A kind of clear wood lacquer thoroughly, it is comprised of component A and B component, and described component A is comprised of the raw material of following weight percent:
The affixture of tolylene diisocyanate TDI and TriMethylolPropane(TMP) or the tripolymer of TDI or their mixture 30%~70%
N-BUTYL ACETATE 15%~35%
Vinyl acetic monomer 15%~35%;
Described B component is comprised of the raw material of following weight percent:
Synolac or modified alkyd resin or their mixture 58%~79%
N-BUTYL ACETATE 0.5%~3%
Vinyl acetic monomer 0.5%~3%
Dimethylbenzene 0.5%~3%
Defoamer 0.16%~0.36%
Flow agent 0.2%~0.4%
Matting agent 0.01%~12.5%
Antiseptic-germicide 0.1%~5%
Dispersion agent 0.1%~0.3%
Anti-settling agent 0.04%~1%
Modified resin 8%~15%;
Wherein, the weight ratio of component A and B component is 1:0.5 or 1:0.25.
Further, described component A is comprised of the raw material of following weight percent: the affixture of 64% tolylene diisocyanate TDI and TriMethylolPropane(TMP) or the tripolymer of TDI or their mixture, 18% N-BUTYL ACETATE and 18% vinyl acetic monomer.
Again further, described B component is comprised of the raw material of following weight percent: 65.9% Synolac or modified alkyd resin or their mixture, 2.55% N-BUTYL ACETATE, 2.55% vinyl acetic monomer, 2.55% dimethylbenzene, 0.3% defoamer, 0.35% flow agent, 10.8% matting agent, 4% antiseptic-germicide, 0.2% dispersion agent, 0.8% anti-settling agent, 10% modified resin.
Based on above-mentioned a kind of clear preparation method of wood lacquer thoroughly, comprise the following steps:
The preparation of component A:
(1) be filled with nitrogen 5min in tank, keep pressure at 0.01~0.05Mpa, then drop into weight percent and be 15%~35% N-BUTYL ACETATE and 15%~35% vinyl acetic monomer, stirring at low speed 5min;
(2) under the stirring at low speed state, drop into again weight percent in the tank and be 30%~70% tolylene diisocyanate TDI and affixture or the tripolymer of TDI or their mixture of TriMethylolPropane(TMP), stir 15min, discharging namely gets component A;
The preparation of B component:
(1) dropping into weight percent in the cylinder is 58%~79% Synolac or modified alkyd resin or their mixture, 0.1%~0.3% dispersion agent, 0.16%~0.36% defoamer, 0.04%~1% anti-settling agent, X
1The N-BUTYL ACETATE of %, X
2The vinyl acetic monomer of %, X
3The dimethylbenzene of % stirs 5min;
(2) adding weight percent under whipped state is 0.01%~12.5% matting agent, then adds Y
1The N-BUTYL ACETATE of %, Y
2The vinyl acetic monomer of % and Y
3The dimethylbenzene of % cleans casing wall, disperses 10min, to fineness less than or equal to 30 μ m;
(3) add the flow agent of weight percent 0.2%~0.4%, 0.1%~5% antiseptic-germicide, 8%~15% modified resin under whipped state, be uniformly dispersed, namely get B component;
Take component A and B component that weight ratio is 1:0.5 or 1:0.25, mixing and stirring, then standing 12~17min, get product;
0.5≤X wherein
1+ Y
1≤ 3,0.5≤X
2+ Y
2≤ 3,0.5≤X
3+ Y
3≤ 3.
The present invention compared with prior art has the following advantages and beneficial effect:
(1) not only paint film is clear for wood lacquer of the present invention, and is rich in gradation sense, can better represent the beautiful texture of timber;
(2) it is tough that wood lacquer of the present invention also has paint film, and gloss is plentiful, strong adhesion, the advantages such as water proof and wearable, erosion resistance;
(3) raw material of the present invention is easy to get, and the preparation method is simple, is suitable for promoting.
Embodiment
The invention will be further described below in conjunction with embodiment, and embodiments of the present invention include but not limited to the following example.
Embodiment 1
a kind of clear wood lacquer thoroughly, component A and B component that it is 1:0.5 by weight ratio form, described component A is that the tripolymer of the affixture of 64% tolylene diisocyanate TDI and TriMethylolPropane(TMP) or TDI or their mixture, 18% N-BUTYL ACETATE and 18% vinyl acetic monomer form by weight percent, described B component is 65.9% Synolac or modified alkyd resin or their mixture by weight percent, 2.55% N-BUTYL ACETATE, 2.55% vinyl acetic monomer, 2.55% dimethylbenzene, 0.3% defoamer (BYK066, the Bi Ke chemistry), 0.35% flow agent (BYK310, the Bi Ke chemistry), 10.8% matting agent (ED30, Grace), 4% antiseptic-germicide, 0.2% dispersion agent (EFKA-4010, Ciba (China) company limited), 0.8% anti-settling agent (DISPARLON A-630-20X, Supreme Being Si Balong) and 10% modified resin (25%1/2S nitro-cotton liquid, the great achievement chemical industry) form.
Its preparation method is as follows:
The preparation of component A:
(1) be filled with nitrogen 5min in tank, keep pressure at 0.01~0.05Mpa, then drop into weight percent and be 18% N-BUTYL ACETATE and 18% vinyl acetic monomer, stirring at low speed 5min;
(2) under the stirring at low speed state, drop into again weight percent in the tank and be 64% tolylene diisocyanate TDI and affixture or the tripolymer of TDI or their mixture of TriMethylolPropane(TMP), stir 15min, discharging namely gets component A;
The preparation of B component:
(1) dropping into weight percent in the cylinder is 65.9% Synolac or modified alkyd resin or their mixture, 0.2% dispersion agent, 0.3% defoamer, 0.8% anti-settling agent, 1% N-BUTYL ACETATE, 1% vinyl acetic monomer, 1% dimethylbenzene, stirs 5min;
(2) adding weight percent under whipped state is 10.8% matting agent, then adds 1.55% N-BUTYL ACETATE, 1.55% vinyl acetic monomer and 1.55% dimethylbenzene to clean casing wall, disperses 10min, to fineness less than or equal to 30 μ m;
(3) add the flow agent of weight percent 0.35%, 4% antiseptic-germicide, 10% modified resin under whipped state, be uniformly dispersed, namely get B component;
Take component A and B component that weight ratio is 1:0.5, mixing and stirring, then standing 14min, get product.
Embodiment 2
a kind of clear wood lacquer thoroughly, component A and B component that it is 1:0.5 by weight ratio form, described component A is that the tripolymer of the affixture of 70% tolylene diisocyanate TDI and TriMethylolPropane(TMP) or TDI or their mixture, 15% N-BUTYL ACETATE and 15% vinyl acetic monomer form by weight percent, described B component is 79% Synolac or modified alkyd resin or their mixture by weight percent, 0.5% N-BUTYL ACETATE, 0.5% vinyl acetic monomer, 0.5% dimethylbenzene, 0.36% defoamer (BYK066, the Bi Ke chemistry), 0.4% flow agent (BYK310, the Bi Ke chemistry), 4.44% matting agent (ED30, Grace), 5% antiseptic-germicide, 0.3% dispersion agent (EFKA-4010, Ciba (China) company limited), 1% anti-settling agent (DISPARLON A-630-20X, Supreme Being Si Balong) and 8% modified resin (25%1/2S nitro-cotton liquid, the great achievement chemical industry) form.
Its preparation method is as follows:
The preparation of component A:
(1) be filled with nitrogen 5min in tank, keep pressure at 0.01~0.05Mpa, then drop into weight percent and be 15% N-BUTYL ACETATE and 15% vinyl acetic monomer, stirring at low speed 5min;
(2) under the stirring at low speed state, drop into again weight percent in the tank and be 70% tolylene diisocyanate TDI and affixture or the tripolymer of TDI or their mixture of TriMethylolPropane(TMP), stir 15min, discharging namely gets component A;
The preparation of B component:
(1) dropping into weight percent in the cylinder is 79% Synolac or modified alkyd resin or their mixture, 0.3% dispersion agent, 0.36% defoamer, 1% anti-settling agent, 0.2% N-BUTYL ACETATE, 0.2% vinyl acetic monomer, 0.2% dimethylbenzene, stirs 5min;
(2) adding weight percent under whipped state is 4.44% matting agent, then adds 0.3% N-BUTYL ACETATE, 0.3% vinyl acetic monomer and 0.3% dimethylbenzene to clean casing wall, disperses 10min, to fineness less than or equal to 30 μ m;
(3) add the flow agent of weight percent 0.4%, 5% antiseptic-germicide, 8% modified resin under whipped state, be uniformly dispersed, namely get B component;
Take component A and B component that weight ratio is 1:0.5, mixing and stirring, then standing 15min, get product.
Embodiment 3
a kind of clear wood lacquer thoroughly, component A and B component that it is 1:0.25 by weight ratio form, described component A is that the tripolymer of the affixture of 30% tolylene diisocyanate TDI and TriMethylolPropane(TMP) or TDI or their mixture, 35% N-BUTYL ACETATE and 35% vinyl acetic monomer form by weight percent, described B component is 58% Synolac or modified alkyd resin or their mixture by weight percent, 3% N-BUTYL ACETATE, 3% vinyl acetic monomer, 3% dimethylbenzene, 0.16% defoamer (BYK066, the Bi Ke chemistry), 0.2% flow agent (BYK310, the Bi Ke chemistry), 12.5% matting agent (ED30, Grace), 5% antiseptic-germicide, 0.1% dispersion agent (EFKA-4010, Ciba (China) company limited), 0.04% anti-settling agent (DISPARLON A-630-20X, Supreme Being Si Balong) and 15% modified resin (25%1/2S nitro-cotton liquid, the great achievement chemical industry) form.
Its preparation method is as follows:
The preparation of component A:
(1) be filled with nitrogen 5min in tank, keep pressure at 0.01~0.05Mpa, then drop into weight percent and be 35% N-BUTYL ACETATE and 35% vinyl acetic monomer, stirring at low speed 5min;
(2) under the stirring at low speed state, drop into again weight percent in the tank and be 30% tolylene diisocyanate TDI and affixture or the tripolymer of TDI or their mixture of TriMethylolPropane(TMP), stir 15min, discharging namely gets component A;
The preparation of B component:
(1) dropping into weight percent in the cylinder is 58% Synolac or modified alkyd resin or their mixture, 0.1% dispersion agent, 0.16% defoamer, 0.04% anti-settling agent, 1.2% N-BUTYL ACETATE, 1.2% vinyl acetic monomer, 1.2% dimethylbenzene, stirs 5min;
(2) adding weight percent under whipped state is 12.5% matting agent, then adds 1.8% N-BUTYL ACETATE, 1.8% vinyl acetic monomer and 1.8% dimethylbenzene to clean casing wall, disperses 10min, to fineness less than or equal to 30 μ m;
(3) add the flow agent of weight percent 0.2%, 5% antiseptic-germicide, 15% modified resin under whipped state, be uniformly dispersed, namely get B component;
Take component A and B component that weight ratio is 1:0.25, mixing and stirring, then standing 15min, get product.
Embodiment 4
a kind of clear wood lacquer thoroughly, component A and B component that it is 1:0.25 by weight ratio form, described component A is that the tripolymer of the affixture of 50% tolylene diisocyanate TDI and TriMethylolPropane(TMP) or TDI or their mixture, 25% N-BUTYL ACETATE and 25% vinyl acetic monomer form by weight percent, described B component is 75% Synolac or modified alkyd resin or their mixture by weight percent, 1% N-BUTYL ACETATE, 1% vinyl acetic monomer, 1% dimethylbenzene, 0.2% defoamer (BYK066, the Bi Ke chemistry), 0.3% flow agent (BYK310, the Bi Ke chemistry), 11.65% matting agent (ED30, Grace), 0.1% antiseptic-germicide, 0.15% dispersion agent (EFKA-4010, Ciba (China) company limited), 0.6% anti-settling agent (DISPARLON A-630-20X, Supreme Being Si Balong) and 9% modified resin (25%1/2S nitro-cotton liquid, the great achievement chemical industry) form.Its preparation method is identical with embodiment 1.
Embodiment 5
a kind of clear wood lacquer thoroughly, component A and B component that it is 1:0.25 by weight ratio form, described component A is that the tripolymer of the affixture of 60% tolylene diisocyanate TDI and TriMethylolPropane(TMP) or TDI or their mixture, 20% N-BUTYL ACETATE and 20% vinyl acetic monomer form by weight percent, described B component is 61% Synolac or modified alkyd resin or their mixture by weight percent, 2.5% N-BUTYL ACETATE, 2.5% vinyl acetic monomer, 2.5% dimethylbenzene, 0.32% defoamer (BYK066, the Bi Ke chemistry), 0.28% flow agent (BYK310, the Bi Ke chemistry), 12.5% matting agent (ED30, Grace), 3.5% antiseptic-germicide, 0.25% dispersion agent (EFKA-4010, Ciba (China) company limited), 0.7% anti-settling agent (DISPARLON A-630-20X, Supreme Being Si Balong) and 13.95% modified resin (25%1/2S nitro-cotton liquid, the great achievement chemical industry) form.Its preparation method is identical with embodiment 1.
Detection data of the present invention such as following table 1:
Table 1
The present invention is tough except paint film, and gloss is plentiful, strong adhesion, and outside water proof and wearable, erosion resistance, and paint film of the present invention is more clear, also is rich in gradation sense, can better represent the beautiful texture of timber.
According to above-described embodiment, just can realize well the present invention.What deserves to be explained is; under prerequisite based on above-mentioned design, for solving same technical problem, even some that make in the present invention are without substantial change or polishing; the essence of the technical scheme that adopts is still the same with the present invention, therefore it also should be in protection scope of the present invention.
Claims (4)
1. a clear wood lacquer thoroughly, is characterized in that, it is comprised of component A and B component, and described component A is comprised of the raw material of following weight percent:
The affixture of tolylene diisocyanate TDI and TriMethylolPropane(TMP) or the tripolymer of TDI or their mixture 30%~70%
N-BUTYL ACETATE 15%~35%
Vinyl acetic monomer 15%~35%;
Described B component is comprised of the raw material of following weight percent:
Synolac or modified alkyd resin or their mixture 58%~79%
N-BUTYL ACETATE 0.5%~3%
Vinyl acetic monomer 0.5%~3%
Dimethylbenzene 0.5%~3%
Defoamer 0.16%~0.36%
Flow agent 0.2%~0.4%
Matting agent 0.01%~12.5%
Antiseptic-germicide 0.1%~5%
Dispersion agent 0.1%~0.3%
Anti-settling agent 0.04%~1%
Modified resin 8%~15%;
Wherein, the weight ratio of component A and B component is 1:0.5 or 1:0.25.
2. a kind of clear wood lacquer thoroughly according to claim 1, it is characterized in that, described component A is comprised of the raw material of following weight percent: the affixture of 64% tolylene diisocyanate TDI and TriMethylolPropane(TMP) or the tripolymer of TDI or their mixture, 18% N-BUTYL ACETATE and 18% vinyl acetic monomer.
3. a kind of clear wood lacquer thoroughly according to claim 2, it is characterized in that, described B component is comprised of the raw material of following weight percent: 65.9% Synolac or modified alkyd resin or their mixture, 2.55% N-BUTYL ACETATE, 2.55% vinyl acetic monomer, 2.55% dimethylbenzene, 0.3% defoamer, 0.35% flow agent, 10.8% matting agent, 4% antiseptic-germicide, 0.2% dispersion agent, 0.8% anti-settling agent, 10% modified resin.
4. the described a kind of clear preparation method of wood lacquer thoroughly of claim 1~3 any one, is characterized in that, comprises the following steps:
The preparation of component A:
(1) be filled with nitrogen 5min in tank, keep pressure at 0.01~0.05Mpa, then drop into weight percent and be 15%~35% N-BUTYL ACETATE and 15%~35% vinyl acetic monomer, stirring at low speed 5min;
(2) under the stirring at low speed state, drop into again weight percent in the tank and be 30%~70% tolylene diisocyanate TDI and affixture or the tripolymer of TDI or their mixture of TriMethylolPropane(TMP), stir 15min, discharging namely gets component A;
The preparation of B component:
(1) dropping into weight percent in the cylinder is 58%~79% Synolac or modified alkyd resin or their mixture, 0.1%~0.3% dispersion agent, 0.16%~0.36% defoamer, 0.04%~1% anti-settling agent, X
1The N-BUTYL ACETATE of %, X
2The vinyl acetic monomer of %, X
3The dimethylbenzene of % stirs 5min;
(2) adding weight percent under whipped state is 0.01%~12.5% matting agent, then adds Y
1The N-BUTYL ACETATE of %, Y
2The vinyl acetic monomer of % and Y
3The dimethylbenzene of % cleans casing wall, disperses 10min, to fineness less than or equal to 30 μ m;
(3) add the flow agent of weight percent 0.2%~0.4%, 0.1%~5% antiseptic-germicide, 8%~15% modified resin under whipped state, be uniformly dispersed, namely get B component;
Take component A and B component that weight ratio is 1:0.5 or 1:0.25, mixing and stirring, then standing 12~17min, get product;
Wherein, 0.5≤X
1+ Y
1≤ 3,0.5≤X
2+ Y
2≤ 3,0.5≤X
3+ Y
3≤ 3.
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Cited By (5)
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CN104031539A (en) * | 2014-06-17 | 2014-09-10 | 展辰涂料集团股份有限公司 | Electrostatic spraying priming paint |
CN104449327A (en) * | 2013-09-17 | 2015-03-25 | 立邦涂料(中国)有限公司 | Anti-yellowing bi-component polyurethane woodware semigloss varnish |
CN107151528A (en) * | 2017-06-13 | 2017-09-12 | 安徽康瑞高科新材料技术工程有限公司 | A kind of two component polyurethane steric hammer varnish |
CN109627957A (en) * | 2018-10-31 | 2019-04-16 | 澳达树熊涂料(惠州)有限公司 | A kind of plentiful color inhibition showering glossy varnish coating of PU high and preparation method thereof |
CN112961593A (en) * | 2021-03-05 | 2021-06-15 | 广东美涂士建材股份有限公司 | Special primer for woodware |
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CN101781495A (en) * | 2010-01-26 | 2010-07-21 | 中华制漆(深圳)有限公司 | Environmental-friendly nitryl wood lacquer and preparation method thereof |
CN102533070A (en) * | 2011-12-31 | 2012-07-04 | 广州立邦涂料有限公司 | Luminant white paint and preparation method thereof |
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CN1603374A (en) * | 2003-09-29 | 2005-04-06 | 上海富臣化工有限公司 | Polyurethane (PU polyester) antibacterial wood varnish (dull, clear) |
CN101781495A (en) * | 2010-01-26 | 2010-07-21 | 中华制漆(深圳)有限公司 | Environmental-friendly nitryl wood lacquer and preparation method thereof |
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
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CN104449327A (en) * | 2013-09-17 | 2015-03-25 | 立邦涂料(中国)有限公司 | Anti-yellowing bi-component polyurethane woodware semigloss varnish |
CN104031539A (en) * | 2014-06-17 | 2014-09-10 | 展辰涂料集团股份有限公司 | Electrostatic spraying priming paint |
CN104031539B (en) * | 2014-06-17 | 2016-08-31 | 展辰新材料集团股份有限公司 | A kind of electrostatic spraying priming paint |
CN107151528A (en) * | 2017-06-13 | 2017-09-12 | 安徽康瑞高科新材料技术工程有限公司 | A kind of two component polyurethane steric hammer varnish |
CN109627957A (en) * | 2018-10-31 | 2019-04-16 | 澳达树熊涂料(惠州)有限公司 | A kind of plentiful color inhibition showering glossy varnish coating of PU high and preparation method thereof |
CN112961593A (en) * | 2021-03-05 | 2021-06-15 | 广东美涂士建材股份有限公司 | Special primer for woodware |
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