CN103103595A - Ultrasonic brightness cleaning agent for special die-casting aluminum workpiece for high-speed rail before anodizing and preparation method - Google Patents

Ultrasonic brightness cleaning agent for special die-casting aluminum workpiece for high-speed rail before anodizing and preparation method Download PDF

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Publication number
CN103103595A
CN103103595A CN2012104527310A CN201210452731A CN103103595A CN 103103595 A CN103103595 A CN 103103595A CN 2012104527310 A CN2012104527310 A CN 2012104527310A CN 201210452731 A CN201210452731 A CN 201210452731A CN 103103595 A CN103103595 A CN 103103595A
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raw material
deionized water
preparation
minutes
cleaning agent
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CN2012104527310A
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CN103103595B (en
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潘德顺
黄文飞
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Dalian Sandaaoke Chemistry Co Ltd
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Dalian Sandaaoke Chemistry Co Ltd
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Abstract

The invention discloses an ultrasonic brightness cleaning agent for a special die-casting aluminum workpiece for a high-speed rail before anodizing. The cleaning agent is composed of the following components by mass percent: 1-3% of potassium pyrophosphate, 1-3% of borax, 0.5-2.5% of sodium tripolyphosphate, 0.5-2.5% of sodium methasilicate pentahydrate, 1-5% of triethanolamine, 0.1-1.0% of active agent (QYL-20), 1-2% of AEO-9, 1-2% of Turkey red oil, 0.1-1.0% of nekal, 0.1-1.0% of JFC, 0.1-0.6% of defoaming agent and the balance of deionized water. The preparation method comprises the following steps of: firstly adding the deionized water in a stainless steel reaction kettle, starting an agitator with rotation speed of 60r/m, slowly adding the solid raw materials in the reaction kettle, agitating for at least 15 minutes after adding each raw material, then orderly and slowly adding the liquid raw materials in the reaction kettle, agitating for at least 10 minutes after adding each raw material, and continuously agitating until the solution becomes a light brown transparent liquid.

Description

Ultrasonic wave light clean-out system and preparation method before the anodic oxidation of the special-purpose die casting aluminium workpiece of high ferro vehicle
Technical field
The present invention relates to a kind of aluminium matter workpiece ultrasonic cleaning agent, especially a kind of dirt that can thoroughly remove on workpiece, guarantee cleanliness factor and the luminance brightness of workpiece surface, ultrasonic wave light clean-out system and preparation method before the anodic oxidation of the special-purpose die casting aluminium workpiece of long-lived high ferro vehicle.
Background technology
Metal cleans, adopt exactly corresponding processing unit and processing condition, with specific solution, the dirt removal on the metal products workpiece surface is fallen, make product reach the technical requirements of design, clean as ultrasonic cleaning, steam purge, high pressure cleaning, ozone-ultraviolet ray, ion beam cleaning and plasma clean etc. are as just carrying out ultrasonic cleaning to it before the anodic oxidation of the special-purpose die casting aluminium workpiece of high ferro vehicle.There are two technical problems in the special-purpose die casting aluminium workpiece of existing high ferro vehicle anodic oxidation fore shell ultrasonic cleaning agent always: the one, and after cleaning, the workpiece surface luminance brightness is not up to standard; The 2nd, the cleaning liquid life-span is short, and change once every day, cleans cost high.
Summary of the invention
The present invention is in order to solve the existing above-mentioned technical problem of prior art, a kind of dirt that can thoroughly remove on workpiece is provided, guarantees cleanliness factor and luminance brightness and the front ultrasonic wave light clean-out system of the special-purpose die casting aluminium workpiece of long-lived high ferro vehicle anodic oxidation and the preparation method of workpiece surface.
Technical solution of the present invention is: ultrasonic wave light clean-out system before the anodic oxidation of the special-purpose die casting aluminium workpiece of a kind of high ferro vehicle is made of the component of following mass percent: potassium pyrophosphate 1 ~ 3%, borax 1 ~ 3%, tripoly phosphate sodium STPP 0.5 ~ 2.5%, metasilicate pentahydrate sodium 0.5 ~ 2.5%, trolamine 1 ~ 5%, promoting agent (QYL-20) 0.1 ~ 1.0%, AEO-9 1 ~ 2%, alizarin assistant 1 ~ 2%, pull open powder 0.1 ~ 1.0%, JFC 0.1 ~ 1.0%, defoamer 0.1 ~ 0.6% and deionized water surplus.
The preparation method of ultrasonic wave light clean-out system before the anodic oxidation of the special-purpose die casting aluminium workpiece of a kind of above-mentioned high ferro vehicle, it is characterized in that carrying out as follows: the deionized water that first will calculate weighing joins in stainless steel cauldron, start agitator, rotating speed is 60 rev/mins, with calculate weighing solid part raw material potassium pyrophosphate, borax, tripoly phosphate sodium STPP, trisodium phosphate, metasilicate pentahydrate sodium, pull open powder and slowly join successively in reactor, often add a kind of raw material and all stirred at least 15 minutes; Liquid part raw material trolamine, promoting agent (QYL-20), AEO-9, alizarin assistant, JFC, the defoamer that will calculate weighing join in reactor successively slowly again, often add a kind of raw material and all stirred at least 10 minutes, be continuously stirring to solution and be the light brown transparent liquid.
The present invention is the acidic cleaner that is applicable to ultrasonic cleaning, can effectively remove the dirt of the special-purpose die casting aluminium workpiece surface of high ferro vehicle, has guaranteed cleanliness factor and the luminance brightness of workpiece surface, reaches the front specification of quality of anodic oxidation.And the usage period long (three days), reduced the production cost of the special-purpose die casting aluminium workpiece of high ferro vehicle, and in rear six months of cleaning the No oxidation discoloration phenomenon.
Embodiment
Embodiment 1:
Each component and mass percent are as follows: the component by following mass percent consists of: potassium pyrophosphate 1%, borax 3%, tripoly phosphate sodium STPP 0.5%, metasilicate pentahydrate sodium 2.5%, trolamine 1%, promoting agent (QYL-20) 1.0%, AEO-9 1%, alizarin assistant 2%, pull open powder 0.1%, JFC1.0%, defoamer (MS-575) 0.1% and deionized water surplus.
The preparation method carries out as follows: the deionized water that first will calculate weighing joins in stainless steel cauldron, start agitator, rotating speed is 60 rev/mins, with calculate weighing solid part raw material potassium pyrophosphate, borax, tripoly phosphate sodium STPP, trisodium phosphate, metasilicate pentahydrate sodium, pull open powder and slowly join successively in reactor, often add a kind of raw material and all stirred at least 15 minutes; Liquid part raw material trolamine, promoting agent (QYL-20), AEO-9, alizarin assistant, JFC, the defoamer that will calculate weighing join in reactor successively slowly again, often add a kind of raw material and all stirred at least 10 minutes, be continuously stirring to solution and be the light brown transparent liquid.
The raw materials used commercially available prod of adopting, wherein promoting agent (QYL-20) is the product that Yang Long Science and Technology Ltd. public offering opens in the Shenzhen, product type is QYL-20.
Embodiment 2:
Each component and mass percent are as follows: potassium pyrophosphate 3%, borax 1%, tripoly phosphate sodium STPP 2.5%, metasilicate pentahydrate sodium 0.5%, trolamine 5%, promoting agent (QYL-20) 0.1%, AEO-9 2%, alizarin assistant 1%, pull open powder 1.0%, JFC 0.1%, defoamer (MS-575) 0.6% and deionized water surplus.
Raw material sources and preparation method are with embodiment 1.
Embodiment 3:
Potassium pyrophosphate 2%, borax 2%, tripoly phosphate sodium STPP 1.0%, metasilicate pentahydrate sodium 1.0%, trolamine 3%, promoting agent (QYL-20) 0.5%, AEO-9 1.5%, alizarin assistant 1.5%, pull open powder 0.5%, JFC 0.5%, defoamer (MS-575) 0.3% and deionized water surplus.
Raw material sources and preparation method are with embodiment 1.
During use, adopting deionized water is 8 ~ 10% preparation ultrasonic cleaning agents with the embodiment of the present invention 1,2 or 3 by mass concentration, ultrasonic cleaning schrittmacher Precision Aluminum matter workpiece, 50 ~ 60 ℃, 4 ~ 8min reaches bright cleaning degree, satisfies anodised requirement, No oxidation discoloration within six months was changed once in three days.

Claims (2)

1. ultrasonic wave light clean-out system before the anodic oxidation of the special-purpose die casting aluminium workpiece of a high ferro vehicle is characterized in that being made of the component of following mass percent: potassium pyrophosphate 1 ~ 3%, borax 1 ~ 3%, tripoly phosphate sodium STPP 0.5 ~ 2.5%, metasilicate pentahydrate sodium 0.5 ~ 2.5%, trolamine 1 ~ 5%, promoting agent (QYL-20) 0.1 ~ 1.0%, AEO-9 1 ~ 2%, alizarin assistant 1 ~ 2%, pull open powder 0.1 ~ 1.0%, JFC 0.1 ~ 1.0%, defoamer 0.1 ~ 0.6% and deionized water surplus.
2. the preparation method of ultrasonic wave light clean-out system before the special-purpose die casting aluminium workpiece of high ferro vehicle as claimed in claim 1 anodic oxidation, it is characterized in that carrying out as follows: the deionized water that first will calculate weighing joins in stainless steel cauldron, start agitator, rotating speed is 60 rev/mins, with calculate weighing solid part raw material potassium pyrophosphate, borax, tripoly phosphate sodium STPP, trisodium phosphate, metasilicate pentahydrate sodium, pull open powder and slowly join successively in reactor, often add a kind of raw material and all stirred at least 15 minutes; Liquid part raw material trolamine, promoting agent (QYL-20), AEO-9, alizarin assistant, JFC, the defoamer that will calculate weighing join in reactor successively slowly again, often add a kind of raw material and all stirred at least 10 minutes, be continuously stirring to solution and be the light brown transparent liquid.
CN201210452731.0A 2012-11-13 2012-11-13 Ultrasonic wave bright clean-out system and preparation method before the anodic oxidation of high ferro vehicle special die casting aluminium workpiece Active CN103103595B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108754507A (en) * 2018-05-26 2018-11-06 厦门力九化工有限公司 A kind of ultrasonic cleaning agent and preparation method and application method

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CN102418108A (en) * 2011-12-30 2012-04-18 大连三达奥克化学股份有限公司 Spraying normal temperature degreasing agent for galvanized steel sheet and production method thereof
CN102533421A (en) * 2011-12-30 2012-07-04 大连三达奥克化学股份有限公司 Machining cutting fluid for die casting aluminum alloy to cast motor shell and preparation method
CN102534634A (en) * 2011-12-30 2012-07-04 大连三达奥克化学股份有限公司 Ultrasonic degreasing agent for cast magnesium alloy workpiece and production method thereof
CN102719840A (en) * 2012-06-21 2012-10-10 大连三达奥克化学股份有限公司 Cleaning agent for stainless steel-aluminum alloy plate combined electric kettle and preparation method

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Publication number Priority date Publication date Assignee Title
GB1479959A (en) * 1973-09-26 1977-07-13 Hoeganaes Ab Magnetite article and method of its production
CN101660152A (en) * 2009-09-27 2010-03-03 大连三达奥克化学股份有限公司 Normal-temperature cleaning anti-rust agent of cylinder body of host machine of iron-casting diesel engine and preparation method thereof
CN101956200A (en) * 2010-11-03 2011-01-26 大连三达奥克化学股份有限公司 Non-phosphorus environment-friendly powdery degreasing agent and manufacturing method thereof
CN101956199A (en) * 2010-11-03 2011-01-26 大连三达奥克化学股份有限公司 Non-phosphorus environment-friendly water-based degreasing agent and manufacturing method thereof
CN102418108A (en) * 2011-12-30 2012-04-18 大连三达奥克化学股份有限公司 Spraying normal temperature degreasing agent for galvanized steel sheet and production method thereof
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108754507A (en) * 2018-05-26 2018-11-06 厦门力九化工有限公司 A kind of ultrasonic cleaning agent and preparation method and application method
CN108754507B (en) * 2018-05-26 2020-11-10 厦门力九化工有限公司 Ultrasonic cleaning agent, preparation method and use method

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