CN103102146A - XuanMing porcelain and producing method - Google Patents
XuanMing porcelain and producing method Download PDFInfo
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- CN103102146A CN103102146A CN2013100504649A CN201310050464A CN103102146A CN 103102146 A CN103102146 A CN 103102146A CN 2013100504649 A CN2013100504649 A CN 2013100504649A CN 201310050464 A CN201310050464 A CN 201310050464A CN 103102146 A CN103102146 A CN 103102146A
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Abstract
The invention discloses a XuanMing porcelain and a producing method, which is characterized in that a plurality of elements such as black stone and red glue soil are added in a XuanMing porcelain producing raw material composition, and a blank material comprises the components of black stone, red glue soil, clay and kaolin. The production process flow comprises the following steps: fragmenting, performing ball milling, sieving, squeezing to mud, performing coarse refining, aging, refining, shaping a base substrate, drying, fettling, decorating, placing and sintering, and drawing to obtain the product. the black stone with a ferrotitanium coloring element is used in a ceramic blank material composition and presents brownish black and has metal luster, and the XuanMing porcelain is sintered through high temperature of 1150-1200 DEG C, the thermal stability is good, the strength is high, the surface is smooth, lead-free cadmium is molten, and the XuanMing porcelain is suitable for high temperature boiling and rapid heating of a microwave oven, the integral effect of the pattern can be considered, and is combined with a traditional pottery making technology and a modern art technology, and the grade and the artistic value of the XuanMing porcelain can be enhanced. A traditional black pottery making technology can be inherited and developed, and the brilliant Chinese culture can be developed.
Description
Technical field
The invention belongs to the domestic ceramics technical field, relate to a kind of ceramic and production method thereof, particularly relate to a kind of profound tender tea leaves magnetic and production method thereof.
Background technology
Black pottery is the ancient culture and arts crystallization of China, rises in the Longshan culture of B.C. 2500 period of late Neolithic.This pure characteristics of making the black pottery goods by hand be deceive, thin, light, can present the color and lusters such as purple, indigo, silver under different light rays, the good reputation of " black as paint, light such as jade " is arranged.Radiating prismatic radiance on world's history of arts and craft.China's black pottery art, wide in variety colorful, make exquisite originally, they are used for decorating the palace, intersperse the hall, become and brag about rich, as to show status and grade sign, and rare making inquiries among the people.after the founding of the state, black pottery art has obtained attention, cause attracting attention of various circles of society, for many years, black pottery be produced on we among the people follow always imitated, it is made the place and mostly is the original home workshop, small scale, equipment is old, yield poorly and be difficult to form series, along with socioeconomic development, improving constantly of living standards of the people, consumption idea is constantly updated, new variation appears in the requirement to ceramic, progress due to technology, make ceramic many new variety occur, different human consumers' needs have been satisfied, particularly present the black pottery product of different-style and class, black pottery as western in the Buddhist nun, sunshine black pottery, Dezhou black pottery, Longshan black pottery, redemption is on the brink of the traditional culture legacy of lost art and obtains to succeed and develop, for making China Dark pottery technique innovation and development in succession, thereby enrich the demand of modern cultural life with exquisite artwork, at present except northern minority enterprise, the black pottery product that most of black pottery manufacturer produces is art ceramics, the product assortment are few, further enrich particularly black pottery kind of pottery, improve quality, satisfy social different levels human consumer's needs, to promoting that industry development has positive effect.
Summary of the invention
The object of the present invention is to provide a kind of in the ceramic batch prescription, utilize local profound stone high ore deposit, the raw material of blank prescription is hybridly prepared into the base substrate base-material, adds the suitable quantity of water ball milling, sieve, press filt, thick experienced, old, concise, be shaped, be dried to base substrate, again through decorate, burn till, classification, polishing grinding obtain " black as China ink; light such as jade ", color is rich and varied, color and luster is simple and tasteful, intensity is high, Heat stability is good, the profound tender tea leaves magnetic finished product of sanitation and hygiene.
Technical solution of the present invention is such, and a kind of profound tender tea leaves magnetic is characterized in that its blank base-material chemistry weight percent is: Al
2O
313.5～20%, SiO
260～71%, FeO
35～9.5%, Cano O.5～5.5%, Mgo 0.1～2%, Kano 3～9%, its blank base-material ingredients by weight per-cent is: profound stone 40～52%, red glue soil 20～25%, clay 6～10%, kaolin 18～25%.
Profound stone Chemical Composition is: Al
2O
37.83%, SiO
264.46%, FeO
38.67%, Cao 3.31%, Mgo 0.84%, Kano 8.29%, its blank base-material ingredients by weight per-cent is: profound stone 48%, red glue soil 22%, clay 8%, kaolin 22%.
its processing step is: step 1: the base material, by described blank base-material, the chemistry weight percent takes, its blank base-material ingredients by weight part per-cent: profound stone 48%, red glue soil 22%, clay 8%, kaolin 22%, and add pug moisture content to be converted into wet feed, step 2: put into ball mill mixing and water adding ball milling 8 ~ 12 hours after first the blank of step 1 being mixed into the base base-material, go out to grind → sieve → press filt → thick white silk → old → concise → roll extrusion → drying → repaired biscuit → make base substrate, step 3: body drying temperature 70 C, 1190～1200 ℃ of firing temperatures, firing time was fired into finished product in 12 hours.
The technological process of production by step 1 is: fragmentation → batching → ball milling → sieve → press filt → pugging → moulding → drying → repaired biscuit → decorate → burn till → classification → polishing grinding → finished product.
Production unit: roller press, wheel roller, ball mill, chain drier, mistake sieve apparatus, slip drying press, vacuum deairing machine, trimming machine, compression molding machine, combustion gas shuttle kiln, tunnel furnace, its main test set: atomic absorption spectrophotometer, muffle furnace, Electric heat oven, analytical balance, oil free compressor, digital display temperature instrumentation.
Quality product reaches " GB/T3532-2009 domestic porcelain " standard-required.Specific targets are as follows:
1. water-intake rate 0.3%;
2. heat-shock resistance (n=5 Ac=0 Re=2 is not once split in 250 ℃ to 20 ℃ heat exchanges of national standard heat-shock resistance) does not split;
3. lead (mg/L) (technical indicator≤0.2) assay is 0.1; 0.1; 0.2; 0.2; 0.1; 0.1 meet;
4. cadmium (mg/L) (technical indicator≤0.30) assay is 0.01; 0.02; 0.01; 0.01; 0.01; 0.02 meet;
5. microwave oven adaptability once circulates and does not split and produce without electric arc;
6. refrigerator does not once split and produces without electric arc to microwave oven adaptability;
7. refrigerator once circulates to baking box adaptability and does not split.
The present invention's beneficial effect compared with prior art is: utilize local profound stone to be rich in ferrotitanium color development element in the ceramic batch prescription, be stable dark brown tone and general metalluster with it, through 1150～1200 ℃ of once-firings of high temperature, thermally-stabilised good, intensity is high, smooth surface, lead and cadmium free melt out, adapt to high temperature steaming, and microwave oven be rapidly heated, and consider the whole structure of design pattern, it melts ancient pottery and Modern Arts, technique in one, improves class and the artistic value of profound tender tea leaves magnetic product.Inherit and develop this ancient black pottery manufacture craft, carrying forward magnificent Chinese national culture.Profound tender tea leaves magnetic
CanDo the boiling crockery, color is rich and varied, the appearance light, feel is level and smooth, and color and luster is simple and tasteful, and intensity is high, Heat stability is good, the Lead and cadmium amount is few, safety and sanitation, water-intake rate 0.3%, 250 ℃ to 20 ℃ heat exchanges of heat-shock resistance are not once split, and microwave oven adaptability is not split and produces without electric arc for once circulating, and refrigerator does not split and produces without electric arc for once circulating to microwave oven adaptability, refrigerator does not split for once circulating to baking box adaptability, is fit to scale operation.
Embodiment
Below by the present invention is described in further detail as example take profound tender tea leaves magnetic bowl.
Embodiment 1,Have drawn from pure, fine and smooth red glue soil and local peculiar profound stone, the Chemical Composition of profound tender tea leaves magnetic blank: Al
2O
313-18%, SiO
265-71%, Fe
2O
35-7.5%, CaO 0.5-2.5%, MgO 0.1-2%, KNaO 3-5%.
The Chemical Composition of profound stone raw material: Al
2O
37.83%, SiO
264.46%, Fe
2O
38.67%, CaO 3.31%, MgO 0.84%, KNaO 8.29%.
Its blank base-material ingredients by weight per-cent consists of: profound stone 40-52%, red glue soil 20-25%, clay 6-10%, kaolin 18-25%.
The material of black pottery mainly contains: the elements such as silicon oxide, aluminum oxide, ferric oxide, titanium oxide, calcium oxide, magnesium oxide, potassium oxide, sodium oxide, manganese oxide.Large percentage be silicon oxide and aluminum oxide, account for respectively 66.32% and 14.90%.The technological process of production of profound tender tea leaves magnetic: fragmentation → batching → ball milling → sieve → press filt → pugging → moulding → drying → repaired biscuit → decorate → burn till → classification → polishing grinding → pack → dispatch from the factory.
The technological process of production of the present invention and main production, test set,
1, main production equipments: roller press, wheel roller, ball mill, chain drier, mistake sieve apparatus, slip drying press, vacuum deairing machine, trimming machine, compression molding machine, combustion gas shuttle kiln, tunnel furnace.
2, main test set: atomic absorption spectrophotometer, muffle furnace, Electric heat oven, analytical balance, oil free compressor, digital display temperature instrumentation.
Embodiment 2,Comprise the following steps: described profound tender tea leaves magnetic, its blank base-material ingredients by weight per-cent consists of: profound stone 48%, red glue soil 22%, clay 8%, kaolin 22%.
1. base: first prepare blank, take the base-material raw material in aforementioned blank base-material ingredients by weight ratio and be mixed into the blank base-material; With raw material put into that ball mill mixing and water adding ball milling 8-10 hours goes out grind to required fineness 200 orders, sieves, press filt, slightly experienced, old, concise, roll extrusion, drying, repaired biscuit, make the china bowl base substrate.The body drying temperature is 70 ℃, and be 4.5 hours time of drying.
Base substrate is decorated, and in the kiln of then packing into, firing temperature is controlled at 1190-1200 ℃, and firing time was fired finished product in 12 hours, and kiln discharge sorting packing obtains profound tender tea leaves magnetic bowl.
The end properties of being made by above-described embodiment: water-intake rate 0.2%, be stable dark brown tone, 250 ℃ of-20 ℃ of heat exchanges of heat-shock resistance are not once split, microwave oven adaptability and do not split and produce without electric arc from microwave oven to refrigerator adaptability for circulation once, refrigerator does not split for once circulating to baking box adaptability.
Embodiment 3,Described profound tender tea leaves magnetic, its blank base-material chemistry weight percent consists of: Al
2O
313.5-20%, SiO
265-71%, FeO
35-7.5%, CaO 0.5-1.5%, MgO 0.1-2%, KNaO 3-5%.
Described profound tender tea leaves magnetic, its blank base-material ingredients by weight per-cent consists of: profound stone 40-52%, red glue soil 20-25%, clay 6-10%, kaolin 18-25%.
Described production method
Profound tender tea leaves magnetic, comprise the following steps: fragmentation → batching → ball milling → sieve → press filt → pugging → moulding → drying → repaired biscuit → decorate → burn till → classification → polishing grinding → pack → dispatch from the factory.
Described
Profound tender tea leaves magneticProduction method, the manufacture craft of described base substrate is: blank is hybridly prepared into the base substrate base-material, adds the suitable quantity of water ball milling, sieve, press filt, thick experienced, old, concise, be shaped, be dried to base substrate.
Described
Profound tender tea leaves magneticProduction method, described body drying temperature is 65-80 ℃, be 3-5 hours time of drying.
Described
Profound tender tea leaves magneticProduction method, described dress firing technique is: will in the kiln of packing into, control temperature and be 1150-1200 ℃ through decorating base substrate, firing time is 4-12 hours.
The present invention reaches the key technical indexes:
Product shows through national Guangxi domestic ceramic product quality supervision and test Spot detection: quality product reaches " GB/T3532-2009 domestic porcelain " standard-required.Specific targets are as follows:
1. water-intake rate 0.3%;
2. heat-shock resistance (n=5 Ac=0 Re=2 is not once split in 250 ℃ to 20 ℃ heat exchanges of national standard heat-shock resistance) does not split;
3. lead (mg/L) (technical indicator≤0.2) assay is 0.1; 0.1; 0.2; 0.2; 0.1; 0.1 meet;
4. cadmium (mg/L) (technical indicator≤0.30) assay is 0.01; 0.02; 0.01; 0.01; 0.01; 0.02 meet;
5. microwave oven adaptability once circulates and does not split and produce without electric arc;
6. refrigerator does not once split and produces without electric arc to microwave oven adaptability;
7. refrigerator once circulates to baking box adaptability and does not split.
The color and luster of profound tender tea leaves magnetic product is simple and tasteful, Heat stability is good, and cold and hot acute degeneration is good, is difficult for explosion, and the lead and cadmium free stripping becomes the domestic ceramics tableware of new generation of green environmental protection.Magnetite or kind stone are used in daily tea set, tableware, and the profound stone that product uses is rich in iron, can play the effect of health care.
Product of the present invention is suitable for high-temperature sterilization, machine washing and microwave oven, light-wave cooker is rapidly heated.
Above-described embodiment explanation is to be described in further detail for the present invention, can not assert that concrete enforcement of the present invention is confined to aforesaid embodiment, does not allly break away from equivalence of the present invention and implements and change, all should be considered as belonging to protection scope of the present invention.
Claims (6)
1. a profound tender tea leaves magnetic, is characterized in that its blank base-material chemistry weight percent is: Al
2O
313.5～20%, SiO
260～71%, FeO
35～9.5%, CaO O.5～5.5%, MgO 0.1～2%, KNaO 3～9%, its blank base-material ingredients by weight per-cent is: profound stone 40～52%, red glue soil 20～25%, clay 6～10%, kaolin 18～25%.
2. according to a kind of profound tender tea leaves magnetic claimed in claim 1, it is characterized in that profound petrochemical industry per-cent is: Al
2O
37.83%, SiO
264.46%, FeO
38.67%, CaO 3.31%, MgO 0.84%, KNaNo 8.29%, its blank base-material ingredients by weight per-cent is: profound stone 48%, red glue soil 22%, clay 8%, kaolin 22%.
3. according to a kind of profound tender tea leaves magnetic production method claimed in claim 1, it is characterized in that its processing step is: step 1: base, first join blank, take by described blank base-material chemistry weight percent, its blank base-material ingredients by weight part per-cent: profound stone 48%, red glue soil 22%, clay 8%, kaolin 22%, step 2: the blank of step 1 is mixed into puts into ball mill mixing and ball milling 8 ~ 10 hours after the base base-material by with water for ball milling → sieve → press filt → slightly practice old mill → roll extrusion → drying → repaired biscuit → make base substrate, step 3: body drying temperature 70 C, 1190～1200 ℃ of firing temperatures, firing time was fired into finished product in 12 hours.
4. according to a kind of profound tender tea leaves magnetic production method claimed in claim 3, it is characterized in that by the technological process of production of step 1 being: fragmentation → batching → ball milling → sieve → press filt → pugging → moulding → drying → repaired biscuit → decorate → burn till → classification → polishing grinding → finished product.
5. according to claim 1 or 3 or 4 described a kind of profound tender tea leaves magnetic production methods, it is characterized in that its production unit: roller press, wheel roller, ball mill, chain drier, mistake sieve apparatus, slip drying press, vacuum deairing machine, trimming machine, compression molding machine, combustion gas shuttle kiln, tunnel furnace, its main test set: atomic absorption spectrophotometer, muffle furnace, Electric heat oven, analytical balance, oil free compressor, digital display temperature instrumentation.
6. according to a kind of profound tender tea leaves magnetic claimed in claim 1, it is characterized in that quality product reaches " GB/T3532-2009 domestic porcelain " standard-required, specific targets are as follows:
1. water-intake rate 0.3%,
2. heat-shock resistance (n=5 Ac=0 Re=2 is not once split in 250 ℃ to 20 ℃ heat exchanges of national standard heat-shock resistance) does not split,
3. lead (mg/L) (technical indicator≤0.2) assay is 0.1,0.1,0.2,0.2, and 0.1,0.1 meets,
4. cadmium (mg/L) (technical indicator≤0.30) assay is 0.01,0.02,0.01,0.01, and 0.01,0.02 meets,
5. microwave oven adaptability once circulates and does not split and produce without electric arc,
6. refrigerator does not once split and produces without electric arc to microwave oven adaptability,
7. refrigerator once circulates to baking box adaptability and does not split.
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|---|---|---|---|
| CN201310050464.9A CN103102146B (en) | 2013-02-14 | 2013-02-14 | A kind of profound tender tea leaves magnetic and production method thereof |
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| CN103102146B CN103102146B (en) | 2016-03-30 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104355599A (en) * | 2014-10-22 | 2015-02-18 | 梅州市裕丰陶瓷有限公司 | Formula of preform body of lime sand ware and preparation method of same |
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| CN102040374A (en) * | 2009-10-19 | 2011-05-04 | 泉州坤达礼品有限公司 | Lithium-magnesium ceramic fired at low temperature and manufacturing method thereof |
| CN102153336A (en) * | 2010-12-04 | 2011-08-17 | 黄俊杰 | Heat-resistant porcelain clay for manufacturing porcelain product and heat-resistant porcelain made from same |
| CN102249654A (en) * | 2011-04-29 | 2011-11-23 | 广西南山瓷器有限公司 | Ancient blue and white porcelain and production method thereof |
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2013
- 2013-02-14 CN CN201310050464.9A patent/CN103102146B/en active Active
Patent Citations (4)
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|---|---|---|---|---|
| CN101386522A (en) * | 2008-10-28 | 2009-03-18 | 林道藩 | Bone porcelain and production process thereof |
| CN102040374A (en) * | 2009-10-19 | 2011-05-04 | 泉州坤达礼品有限公司 | Lithium-magnesium ceramic fired at low temperature and manufacturing method thereof |
| CN102153336A (en) * | 2010-12-04 | 2011-08-17 | 黄俊杰 | Heat-resistant porcelain clay for manufacturing porcelain product and heat-resistant porcelain made from same |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104355599A (en) * | 2014-10-22 | 2015-02-18 | 梅州市裕丰陶瓷有限公司 | Formula of preform body of lime sand ware and preparation method of same |
| CN104355599B (en) * | 2014-10-22 | 2016-03-09 | 梅州市裕丰陶瓷有限公司 | Blank of a kind of sand-lime pottery and preparation method thereof |
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|---|---|
| CN103102146B (en) | 2016-03-30 |
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