CN103088551A - Light bastose and flame-retardant polypropylene fiber composite board and method for manufacturing same - Google Patents
Light bastose and flame-retardant polypropylene fiber composite board and method for manufacturing same Download PDFInfo
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- CN103088551A CN103088551A CN2011103314308A CN201110331430A CN103088551A CN 103088551 A CN103088551 A CN 103088551A CN 2011103314308 A CN2011103314308 A CN 2011103314308A CN 201110331430 A CN201110331430 A CN 201110331430A CN 103088551 A CN103088551 A CN 103088551A
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Abstract
The invention discloses a light bastose and flame-retardant polypropylene fiber composite board which comprises 25-75wt% of bastose and 25-75wt% of flame-retardant polypropylene fibers. A method for manufacturing the light bastose and flame-retardant polypropylene fiber composite board includes performing flame-retardant treatment for the bastose; manufacturing the flame-retardant polypropylene fibers and the bastose which is subjected to the flame-retardant treatment into a composite felt; and performing baking and roll forming for the composite felt to obtain the light bastose and flame-retardant polypropylene fiber composite board. The light bastose and flame-retardant polypropylene fiber composite board used as an interior trim part of an automobile is environment-friendly and safe, and is excellent in flame-retardant performance owing to the flame-retardant polypropylene fibers and the flame-retardant treatment for the bastose, and potential safety hazards caused during production and service are prevented; mixed fibers are laid down in a crossed manner and the felt is formed by means of needling to form the board, raw materials are dispersed uniformly, degrees of adhesion of boundaries of the bastose and the polypropylene fibers are improved, and the board is excellent in comprehensive mechanical property; and the product is easy to form and simple in processing technology, the production efficiency can be improved, and the production cost can be reduced.
Description
Technical field
The present invention relates to technical field of polymer composite materials, relate in particular to a kind of flax fibre/flame-retardant polypropylene fibre light composite board and preparation method thereof.
Background technology
Ecological deterioration, resource shortage and energy crisis make the human knowledge to protection of the environment and efficent use of resources importance and the urgency to realizing society and sustained economic development, people more and more pay attention to adopting renewable biological source to make new material.In recent years, the natural plant fibre the abundantest with the occurring in nature resource substitutes the synthetic fortifying fibres such as present widely used glass fibre, and exploitation has the research of premium properties and low-cost composite, has caused people's great attention.
Natural fabric is inexpensive because of it, light weight, can natural degradation, the good characteristic such as specific strength and specific stiffness height, demonstrate good application prospect.In natural plant fibre, flax fibre not only has very high strength and modulus, has simultaneously that cellulose material is hard, a rub resistance, corrosion resistant characteristics, and the hemp resource of China is extremely abundant, is fiber crops one of the widest, that output the is maximum country that distributes in the world.The research of flax fibre reinforced composite at present extensively launches in American-European, Japan, and the part scientific achievement also is applied; The teachers such as domestic researcher or technical staff also have lot of documents and patent research and the application of flax fibre reinforced composite are reported, the Dai Gance of Chemical Engineering associating National Key Laboratory of East China University of Science and researcher are studied sisal fiber, tossa Reinforced Polypropylene material.publication number is that the Chinese patent of CN 101665015A can't be made fibrilia/polypropylene fiber composite board for the existing extruding-out process of solution and hot press forming technology exists raw material to be difficult to the problems such as evenly mixing, employing is compiled into sheet with linen fibre rope and polypropylene silk thread, through steel plate hot pressing, the method of cooling and shaping, prepare fibrilia/polypropylene fiber composite board, this method has improved the shared proportion of natural fiber material greatly, reduced production cost, but exist flax fibre and polypropylene fibre dipping inhomogeneous, the interfacial adhesion of product is inadequate, there is the defective of distribution of force inequality in the composite board of preparation.
In addition, lightweight, safe, comfortableization and environmental protection are the main trend of World Auto Industry development.Plastics and composite thereof are important materials used in auto manufacturing, and on average the quantity of plastics of each automobile has reached 105kg, account for the 8%-12% of automobile gross mass.The flax fibre composite is as the performance advantage of auto parts and components: alleviate vehicle weight, reduce manufacturing cost, improve the automobile crash worthiness, sound insulation, material itself are recyclable etc.In the situation that current oil is day by day in short supply, oil price rises steadily, its meaning is particularly evident.
The flax fibre composite is mainly used in car interior trim door-plate, driver with glove compartment, floor, boxcar, spare wheel cover, backrest in auto industry, can also be used for instrument board, armrest, roof interior trim, sunshading board, luggage compartment decorative panel etc.Chery Automobiles patent of invention CN 101549671A discloses a kind of fibrilia automobile inner decoration member and production method thereof, it is raw material that this method adopts tossa and polypropylene fiber, become net, acupuncture to become felt, Baking out, cold moudling to prepare automotive upholstery by combing mixing, fiber, this method technical process is simple, excellent product performance, and environment friendly and pollution-free, can be applicable to the parts such as roof decorations, door trim, luggage case sidewall plate, hat rack.The patent of invention CN 101045310A of domestic automobile interior material manufacturer also discloses a kind of automotive trim natural fiber composite plate and processing method thereof, this method adopts flax fibre, polyster fibre, compound glue surface layer, middle basic unit, the topcoat made of polypropylene fiber, then become compound numb felt by three layers of lapping, acupuncture that sheet material is required, more molded through warm-up mill.Wherein, flax fibre, polyster fibre, polypropylene fiber proportion between different layers can be regulated, and design flexibility is large, but the manufacture craft relative complex particularly prepares the process of compound numb felt, has greatly affected production efficiency.
The standby flax fibre reinforced composite of above patent system and as all Shortcomings parts that is applied on the preparation method of automotive upholstery is mainly manifested in: flax fibre causes easily loose, mechanical properties decrease of product with to strengthen the resin boundary surface cohesive force inadequate; The natural fabric that is easy to catch fire is not carried out flame treatment, have potential safety hazard in producing, using; The smooth appearance degree such as flax fibre are inadequate, easily cause product thickness and mass deviation, are unfavorable for satisfying auto industry to the requirement of product.
Summary of the invention
The present invention is exactly that this sheet material has good fire resistance for the flame retardant effect deficiency that solves above-mentioned prior art existence, production process relative complex, products material disperse unequal problem and a kind of flax fibre/flame-retardant polypropylene fibre light composite board is provided.
Another object of the present invention is to provide the preparation method of a kind of flax fibre/flame-retardant polypropylene fibre light composite board, and the method processing technology is simple, is easy to continuous production.
Purpose of the present invention is achieved through the following technical solutions:
A kind of flax fibre/flame-retardant polypropylene fibre light composite board, made by the component that comprises following weight percentage:
Flax fibre 25-75 wt%,
Flame-retardant polypropylene fibre 25-75 wt%.
Preferably, described flax fibre is processed through fire retardant, and the amount ratio of flax fibre and fire retardant is (1-3): 2; Described fire retardant is RF-203 III environment-friendly liquid fire retardant.RF-203 III environment-friendly liquid fire retardant is composite fire retardant, and the compound synergistic is composite forms by phosphorus, nitrogen etc., and wherein solid phase quality percentage composition is 25%, and being called for short solid content is 25%.
Preferably, described flax fibre is selected from one or more in jute, flax, sisal hemp or hemp.
Preferably, described tossa is chopped tossa, and white, length are 80-110mm.Rigidity and the intensity of tossa are better, and cheap.
Preferably, described linen fibre is chopped linen fibre, and is white or light yellow, and length is 80-110mm.Linen fibre moisture absorption thermal diffusivity is good, and has certain flame retardant effect.
Preferably, described sisal fiber is chopped sisal fiber, and white, length are 80-110mm.Sisal fiber is a kind of hard fibre, and is strong but pliable in texture, and wear-resisting wiping is difficult for brittle failure.
Preferably, described hemp is chopped hemp, and white, length are 80-110mm.Hemp has good hygroscopicity and heat resistance.
Preferably, described flame-retardant polypropylene fibre is white, and length is 60-90mm.
The preparation method of a kind of flax fibre/flame-retardant polypropylene fibre light composite board comprises the following steps:
(1) flax fibre is carried out flame treatment;
(2) the flax fibre 25-75 wt% after flame treatment and flame-retardant polypropylene fibre 25-75 wt% are prepared composite felt;
(3) composite felt is cured roll-forming, obtain flax fibre/flame-retardant polypropylene fibre light composite board.
Preferably, in described step (1), the flax fibre flame treatment comprises the following steps: flax fibre was soaked 15-30 minute in the fire retardant maceration extract of 20-40 ℃, roll clean; Repeatedly pad 2-4 time again, be dried to the flax fibre moisture content lower than 5% under 100-140 ℃.
Preferably, described fire retardant is RF-203 III environment-friendly liquid fire retardant, and solid content is 25%; The amount ratio of described flax fibre and fire retardant is (1-3): 2.
Preferably, in described step (2), preparation flax fibre/flame-retardant polypropylene fibre composite felt comprises the following steps: the flax fibre 25-75 wt% after flame treatment in step (1) and flame-retardant polypropylene fibre 25-75 wt% are evenly mixed, carrying out shredding processes, combing is shaped, the vertical and horizontal cross lapping, acupuncture becomes felt, obtains flax fibre/flame-retardant polypropylene fibre composite felt.Described acupuncture becomes felt to comprise acupuncture and lower acupuncture two parts.
Preferably, curing roll-forming in described step (3) comprises the following steps: the flax fibre that step (2) is prepared/flame-retardant polypropylene fibre composite felt adds the hot baked plasticizing at 195-235 ℃, then be the warm-up mill roll-in plasticizing forming of 115-135 ℃ through excess temperature, prepare flax fibre/flame-retardant polypropylene fibre light composite board.
Compared with prior art, the present invention has following beneficial effect:
Flax fibre of the present invention/flame-retardant polypropylene fibre light composite board is as automotive upholstery not only environmental protection but also safety, particularly the fire resistance of light composite board excellence is given in the introducing of the flame treatment of flax fibre and flame-retardant polypropylene fibre, has avoided the potential safety hazard in production and use procedure; Sheet material is to become felt to form by blended fiber cross lapping, acupuncture, and raw material is uniformly dispersed, and flax fibre and polypropylene fiber interfacial adhesion degree improve, and make this sheet material have good comprehensive mechanical property; Product is easy to moulding, and processing technology is simple, can enhance productivity, and reduces production costs.In sum, flax fibre provided by the invention/flame-retardant polypropylene fibre light composite board can be realized lightweight, safe, comfortableization and the environmental protection mission of auto parts and components.
The specific embodiment
Describe the present invention in detail below in conjunction with each embodiment.
Embodiment 1
Take raw material (kg) according to following weight:
Tossa (through flame treatment) 25 kg, the quality percentage composition is 25%,
Flame-retardant polypropylene fibre 75 kg, quality percentage composition are 75%,
What wherein the flax fibre flame treatment adopted is the RF-203 III environment-friendly liquid fire retardant (solid content is 25%) of 50kg.
Produce the method for this flax fibre/flame-retardant polypropylene fibre light composite board:
At 20 ℃, solid content is to soak 30 minutes in 25% 50kg fire retardant maceration extract, rolls clean with the chopped tossa (white, length are 80mm) of unpacking; Repeatedly pad again 2 times, be dried to the flax fibre moisture content lower than 5% under 100 ℃; Tossa after the 25kg flame treatment and 75kg flame-retardant polypropylene fibre (white, length are 60mm) are evenly mixed, carry out shredding and process, combing is shaped, the vertical and horizontal cross lapping becomes felt through upper and lower acupuncture, obtains flax fibre/flame-retardant polypropylene fibre composite felt; Being that the baking oven of 195 ℃ adds the hot baked plasticizing with this composite felt through excess temperature, is then the warm-up mill roll-forming of 115 ℃ by temperature, and cooling cutting prepares flax fibre/flame-retardant polypropylene fibre light composite board.The correlated performance of this material sees table 1 for details.
Embodiment 2
Take raw material (kg) according to following weight:
Tossa (through flame treatment) 35 kg, the quality percentage composition is 35%,
Flame-retardant polypropylene fibre 65 kg, quality percentage composition are 65%,
What wherein the flax fibre flame treatment adopted is the RF-203 III environment-friendly liquid fire retardant (solid content is 25%) of 50kg.
At 40 ℃, solid content is to soak 15 minutes in 25% 50kg fire retardant maceration extract, rolls clean with the chopped tossa (white, length are 110mm) of unpacking; Repeatedly pad again 4 times, be dried to the flax fibre moisture content lower than 5% under 140 ℃; Tossa after the 35kg flame treatment and 65kg flame-retardant polypropylene fibre (white, length are 90mm) are evenly mixed, carry out shredding and process, combing is shaped, the vertical and horizontal cross lapping becomes felt through upper and lower needing machine, obtains flax fibre/flame-retardant polypropylene fibre composite felt; Being that the baking oven of 235 ℃ adds the hot baked plasticizing with this composite felt through excess temperature, is then the warm-up mill roll-forming of 135 ℃ by temperature, and cooling cutting prepares flax fibre/flame-retardant polypropylene fibre light composite board.The correlated performance of this material sees table 1 for details.
Embodiment 3
Take raw material (kg) according to following weight:
Tossa (through flame treatment) 45 kg, the quality percentage composition is 45%,
Flame-retardant polypropylene fibre 55 kg, quality percentage composition are 55%,
What wherein the flax fibre flame treatment adopted is the RF-203 III environment-friendly liquid fire retardant (solid content is 25%) of 50kg.
At 30 ℃, solid content is to soak 25 minutes in 25% 50kg fire retardant maceration extract, rolls clean with the chopped tossa (white, length are 100mm) of unpacking; Repeatedly pad again 3 times, be dried to the flax fibre moisture content lower than 5% under 120 ℃; Tossa after the 45kg flame treatment and 55kg flame-retardant polypropylene fibre (white, length are 80mm) are evenly mixed, carry out shredding and process, combing is shaped, the vertical and horizontal cross lapping becomes felt through upper and lower needing machine, obtains flax fibre/flame-retardant polypropylene fibre composite felt; Being that the baking oven of 210 ℃ adds the hot baked plasticizing with this composite felt through excess temperature, is then the warm-up mill roll-forming of 120 ℃ by temperature, and cooling cutting prepares flax fibre/flame-retardant polypropylene fibre light composite board.The correlated performance of this material sees table 1 for details.
Embodiment 4
Take raw material (kg) according to following weight:
Linen fibre (through flame treatment) 50 kg, the quality percentage composition is 50%,
Flame-retardant polypropylene fibre 50 kg, quality percentage composition are 50%,
What wherein the flax fibre flame treatment adopted is the RF-203 III environment-friendly liquid fire retardant (solid content is 25%) of 50kg.
At 25 ℃, solid content is to soak 20 minutes in 25% 50kg fire retardant maceration extract, rolls clean with the chopped linen fibre (white, length are 80mm) of unpacking; Repeatedly pad again 3 times, be dried to the flax fibre moisture content lower than 5% under 110 ℃; Linen fibre after the 50kg flame treatment and 50kg flame-retardant polypropylene fibre (white, length are 70mm) are evenly mixed, carry out shredding and process, combing is shaped, the vertical and horizontal cross lapping becomes felt through upper and lower needing machine, obtains flax fibre/flame-retardant polypropylene fibre composite felt; Being that the baking oven of 200 ℃ adds the hot baked plasticizing with this composite felt through excess temperature, is then the warm-up mill roll-forming of 125 ℃ by temperature, and cooling cutting prepares flax fibre/flame-retardant polypropylene fibre light composite board.
Embodiment 5
Take raw material (kg) according to following weight:
Linen fibre (through flame treatment) 52 kg, the quality percentage composition is 52%,
Flame-retardant polypropylene fibre 48 kg, quality percentage composition are 48%,
What wherein the flax fibre flame treatment adopted is the RF-203 III environment-friendly liquid fire retardant (solid content is 25%) of 50kg.
At 26 ℃, solid content is to soak 21 minutes in 25% 50kg fire retardant maceration extract, rolls clean with the chopped linen fibre (light yellow, length is 110mm) of unpacking; Repeatedly pad again 3 times, be dried to the flax fibre moisture content lower than 5% under 112 ℃; Linen fibre after the 52kg flame treatment and 48kg flame-retardant polypropylene fibre (white, length are 75mm) are evenly mixed, carry out shredding and process, combing is shaped, the vertical and horizontal cross lapping becomes felt through upper and lower needing machine, obtains flax fibre/flame-retardant polypropylene fibre composite felt; Being that the baking oven of 205 ℃ adds the hot baked plasticizing with this composite felt through excess temperature, is then the warm-up mill roll-forming of 125 ℃ by temperature, and cooling cutting prepares flax fibre/flame-retardant polypropylene fibre light composite board.
Embodiment 6
Take raw material (kg) according to following weight:
Sisal fiber (through flame treatment) 55 kg, the quality percentage composition is 55%,
Flame-retardant polypropylene fibre 45 kg, quality percentage composition are 45%,
What wherein the flax fibre flame treatment adopted is the RF-203 III environment-friendly liquid fire retardant (solid content is 25%) of 50kg.
At 35 ℃, solid content is to soak 22 minutes in 25% 50kg fire retardant maceration extract, rolls clean with the chopped sisal fiber (white, length are 80mm) of unpacking; Repeatedly pad again 2 times, be dried to the flax fibre moisture content lower than 5% under 130 ℃; Sisal fiber after the 55kg flame treatment and 45kg flame-retardant polypropylene fibre are evenly mixed, carry out shredding and process, combing is shaped, and the vertical and horizontal cross lapping becomes felt through upper and lower needing machine, obtains flax fibre/flame-retardant polypropylene fibre composite felt; Being that the baking oven of 205 ℃ adds the hot baked plasticizing with this composite felt through excess temperature, is then the warm-up mill roll-forming of 130 ℃ by temperature, and cooling cutting prepares flax fibre/flame-retardant polypropylene fibre light composite board.
Embodiment 7
Take raw material (kg) according to following weight:
Sisal fiber (through flame treatment) 65 kg quality percentage compositions are 65%,
Flame-retardant polypropylene fibre 35 kg quality percentage compositions are 35%,
What wherein the flax fibre flame treatment adopted is the RF-203 III environment-friendly liquid fire retardant (solid content is 25%) of 50kg.
At 38 ℃, solid content is to soak 28 minutes in 25% 50kg fire retardant maceration extract, rolls clean with the chopped sisal fiber (white, length are 90mm) of unpacking; Repeatedly pad again 4 times, be dried to the flax fibre moisture content lower than 5% under 125 ℃; Sisal fiber after the 65kg flame treatment and 35kg flame-retardant polypropylene fibre are evenly mixed, carry out shredding and process, combing is shaped, and the vertical and horizontal cross lapping becomes felt through upper and lower needing machine, obtains flax fibre/flame-retardant polypropylene fibre composite felt; Being that the baking oven of 220 ℃ adds the hot baked plasticizing with this composite felt through excess temperature, is then the warm-up mill roll-forming of 118 ℃ by temperature, and cooling cutting prepares flax fibre/flame-retardant polypropylene fibre light composite board.
Embodiment 8
Take raw material (kg) according to following weight:
Hemp (through flame treatment) 75kg, the quality percentage composition is 75%,
Flame-retardant polypropylene fibre 25 kg, quality percentage composition are 25%,
What wherein the flax fibre flame treatment adopted is the RF-203 III environment-friendly liquid fire retardant (solid content is 25%) of 50kg.
At 22 ℃, solid content is to soak 18 minutes in 25% 50kg fire retardant maceration extract, rolls clean with the chopped hemp (white, length are 100mm) of unpacking; Repeatedly pad again 4 times, be dried to the flax fibre moisture content lower than 5% under 135 ℃; Hemp after the 75kg flame treatment and 25kg flame-retardant polypropylene fibre are evenly mixed, carry out shredding and process, combing is shaped, and the vertical and horizontal cross lapping becomes felt through upper and lower needing machine, obtains flax fibre/flame-retardant polypropylene fibre composite felt; Being that the baking oven of 215 ℃ adds the hot baked plasticizing with this composite felt through excess temperature, is then the warm-up mill roll-forming of 128 ℃ by temperature, and cooling cutting prepares flax fibre/flame-retardant polypropylene fibre light composite board.
The flax fibre that embodiment 1-3 is prepared/flame-retardant polypropylene fibre light composite board carries out performance test, and test result sees Table 1.
Table 1
Can find out from the data of table 1; flax fibre of the present invention/flame-retardant polypropylene fibre light composite board quality is light; the good mechanical properties such as TENSILE STRENGTH, bending strength, impact strength; horizontal firing tests also that testimonial material has good effect aspect fire resistance, has the outstanding advantages such as lightweight, environmental protection, safe as the automotive upholstery product.
Above disclosed be only several specific embodiments of the application, but the application is not limited thereto, the changes that any person skilled in the art can think of all should drop in the application's protection domain.
Claims (10)
1. flax fibre/flame-retardant polypropylene fibre light composite board, is characterized in that, made by the component that comprises following weight percentage:
Flax fibre 25-75 wt%,
Flame-retardant polypropylene fibre 25-75 wt%.
2. flax fibre as claimed in claim 1/flame-retardant polypropylene fibre light composite board, is characterized in that, described flax fibre is processed through fire retardant, and the amount ratio of flax fibre and fire retardant is (1-3): 2; Described fire retardant is RF-203 III environment-friendly liquid fire retardant, and solid content is 25%.
3. flax fibre as claimed in claim 1 or 2/flame-retardant polypropylene fibre light composite board, is characterized in that, described flax fibre is selected from one or more in jute, flax, sisal hemp or hemp.
4. flax fibre as claimed in claim 1 or 2/flame-retardant polypropylene fibre light composite board, is characterized in that, described flax fibre is staple fiber, and length is 80-110mm.
5. flax fibre as claimed in claim 1 or 2/flame-retardant polypropylene fibre light composite board, is characterized in that, the length of described flame-retardant polypropylene fibre is 60-90mm.
6. the preparation method of flax fibre as claimed in claim 1/flame-retardant polypropylene fibre light composite board, is characterized in that, comprises the following steps:
(1) flax fibre is carried out flame treatment;
(2) the flax fibre 25-75 wt% after flame treatment and flame-retardant polypropylene fibre 25-75 wt% are prepared composite felt;
(3) composite felt is cured roll-forming, obtain flax fibre/flame-retardant polypropylene fibre light composite board.
7. the preparation method of flax fibre as claimed in claim 6/flame-retardant polypropylene fibre light composite board, it is characterized in that, in described step (1), the flax fibre flame treatment comprises the following steps: flax fibre was soaked 15-30 minute in the fire retardant maceration extract of 20-40 ℃, roll clean; Repeatedly pad 2-4 time again, be dried to the flax fibre moisture content lower than 5% under 100-140 ℃.
8. the preparation method of flax fibre as claimed in claim 7/flame-retardant polypropylene fibre light composite board, is characterized in that, described fire retardant is RF-203 III environment-friendly liquid fire retardant, and solid content is 25%; The amount ratio of described flax fibre and fire retardant is (1-3): 2.
9. the preparation method of flax fibre as claimed in claim 6/flame-retardant polypropylene fibre light composite board, it is characterized in that, in described step (2), preparation flax fibre/flame-retardant polypropylene fibre composite felt comprises the following steps: the flax fibre 25-75 wt% after flame treatment in step (1) and flame-retardant polypropylene fibre 25-75 wt% are evenly mixed, carrying out shredding processes, combing is shaped, the vertical and horizontal cross lapping, acupuncture becomes felt, obtains flax fibre/flame-retardant polypropylene fibre composite felt.
10. the preparation method of flax fibre as claimed in claim 6/flame-retardant polypropylene fibre light composite board, it is characterized in that, curing roll-forming in described step (3) comprises the following steps: the flax fibre that step (2) is prepared/flame-retardant polypropylene fibre composite felt adds the hot baked plasticizing at 195-235 ℃, then be the warm-up mill roll-in plasticizing forming of 115-135 ℃ through excess temperature, prepare flax fibre/flame-retardant polypropylene fibre light composite board.
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