CN103073975B - A kind of Alkyd resin vehicle primer and preparation method thereof - Google Patents
A kind of Alkyd resin vehicle primer and preparation method thereof Download PDFInfo
- Publication number
- CN103073975B CN103073975B CN201210389835.1A CN201210389835A CN103073975B CN 103073975 B CN103073975 B CN 103073975B CN 201210389835 A CN201210389835 A CN 201210389835A CN 103073975 B CN103073975 B CN 103073975B
- Authority
- CN
- China
- Prior art keywords
- sepiolite
- alkyd resin
- powder
- zinc
- resin vehicle
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Abstract
The invention provides a kind of Alkyd resin vehicle primer, it is made up of following parts by weight of component: Synolac 70-80, melamine resin 3-4, two benzoylphenyl phosphine oxide 1-2, dipropylene glycol monomethyl ether 8-10, sodium laurylsulfate 2-3, myo-Inositol hexaphosphate 4-6, vinylbenzene 10-15, sodium polyacrylate 0.3-0.5, stannous pyrophosphate 0.1-0.3, rust-preventive agent 0.2-0.3, N-BUTYL ACETATE 1-2, polyvinyl alcohol 1-2, pure aluminium silicate 5-8, Tritolyl Phosphate 3-5, zinc powder 8-10, zinc molybdate 8-10, modified meerschaum 3-5, barium metaborate 8-10, silicon sol 3-5, zinc naphthenate 2-5, polysiloxane defoamers 0.1-0.3.Alkyd resin vehicle primer of the present invention, have good anti-hitting property of stone, good corrosion resistance, water-tolerant, flame retardant properties are good, to the strong adhesion of base material.<!--1-->
Description
Technical field:
The present invention relates to a kind of paint, be specifically related to a kind of Alkyd resin vehicle primer its preparation method.
Background technology:
Along with the development of society, paint in the widespread use of various fields, while playing beauty function, also there is provide protection, there is corrosion-resistant, ageing-resistant effect.Such as in the application of metallic surface, effect that is attractive in appearance, protection possesses simultaneously.Require that it has anti-hitting property of stone for vehicle paint base, wear resisting property is good.
Goal of the invention:
The invention provides a kind of Alkyd resin vehicle primer its preparation method, this paint application, at car surface, has good anti-hitting property of stone, also has heat-resisting, flame retardant properties simultaneously.
The technical solution used in the present invention is as follows for achieving the above object:
A kind of Alkyd resin vehicle primer, it is characterized in that, it is made up of the component of following weight part:
Synolac 70-80, melamine resin 3-4, two benzoylphenyl phosphine oxide 1-2, dipropylene glycol monomethyl ether 8-10, sodium laurylsulfate 2-3, myo-Inositol hexaphosphate 4-6, vinylbenzene 10-15, sodium polyacrylate 0.3-0.5, stannous pyrophosphate 0.1-0.3, rust-preventive agent 0.2-0.3, N-BUTYL ACETATE 1-2, polyvinyl alcohol 1-2, pure aluminium silicate 5-8, Tritolyl Phosphate 3-5, zinc powder 8-10, zinc molybdate 8-10, modified meerschaum 3-5, barium metaborate 8-10, silicon sol 3-5, zinc naphthenate 2-5, polysiloxane defoamers 0.1-0.3
The preparation method of described modified meerschaum is: a, first activated by sepiolite: activation condition 85 DEG C, 45h, then crosses 150 mesh sieves; B, with hydrochloric Acid Modification: with 0.5mol/LHCl, modification is carried out to sepiolite, solid-to-liquid ratio (g/ml) 1:3, be oscillation treatment 8h in the constant temperature oscillator of 55 DEG C in temperature, then centrifugation, add deionized water wash to pH value about 6, centrifugation is placed in the loft drier of 55 DEG C and dries;
Modification is carried out in c, the coupling of dried sepiolite recycle silicon alkane, and concrete operations are as follows:
Take the silane coupling agent KH792 of dry sepiolite quality 2%, 2-3% vinyl three ('beta '-methoxy oxyethyl group) silane, 20-25% ferrophosphorus powder, high speed dispersion 4300-4500 rev/min, 20-30 minute;
Sepiolite good for coupling agent treatment is taken out, first cleans with a small amount of ethanolic soln and then repeatedly rinse with deionized water, filter in neutral, the sepiolite cleaned up is dried, grinds to form superfine nano powder, modified Nano sepiolite can be obtained;
Described rust-preventive agent is prepared from by the component of following weight part: citric acid 49-51, aluminium powder 0.8-0.9, gelatin 0.3-0.5, Tritolyl Phosphate 0.2-0.4, talcum powder 1-2, total amount 100 is added to water, after formula material is added mixing and stirring in proportion successively, mix through ground elimination.
(1) first Synolac, melamine resin, two benzoylphenyl phosphine oxide, dipropylene glycol monomethyl ether, sodium laurylsulfate, myo-Inositol hexaphosphate and vinylbenzene are mixed by formula rate, high-speed stirring, rear formation emulsion;
(2) all the other components in formula are joined in the emulsion of step (1) gained and are fully ground to particle diameter 25-40um, then after 30 minutes, with 280 order filter-cloth filterings, get product in high-speed stirring.
Using method:
1, before using, substrate surface must be cleaned drying, remove dust and greasy dirt;
2, stir;
3, directly brush, spraying, roller application be all passable;
Every 1kg coating area 12-14 square metres.
Beneficial effect:
A kind of Alkyd resin vehicle primer of the present invention, have good anti-hitting property of stone, good corrosion resistance, water-tolerant, flame retardant properties are good, to the strong adhesion of base material, environmental protection simultaneously, free from environmental pollution, be environmental protection paint.
Be widely used in various steamer, vehicle, payload of freight container automobile, tractor, the surface of all iron structures is antirust and protect decorative operation.
Claims (2)
1. an Alkyd resin vehicle primer, it is characterized in that, it is made up of the component of following weight part: Synolac 70-80, melamine resin 3-4, two benzoylphenyl phosphine oxide 1-2, dipropylene glycol monomethyl ether 8-10, sodium laurylsulfate 2-3, myo-Inositol hexaphosphate 4-6, vinylbenzene 10-15, sodium polyacrylate 0.3-0.5, stannous pyrophosphate 0.1-0.3, rust-preventive agent 0.2-0.3, N-BUTYL ACETATE 1-2, polyvinyl alcohol 1-2, pure aluminium silicate 5-8, Tritolyl Phosphate 3-5, zinc powder 8-10, zinc molybdate 8-10, modified meerschaum 3-5, barium metaborate 8-10, silicon sol 3-5, zinc naphthenate 2-5, polysiloxane defoamers 0.1-0.3, the preparation method of described modified meerschaum is: a, first sepiolite is activated: activation condition 85 DEG C, 45h, then 150 mesh sieves are crossed, b, with hydrochloric Acid Modification: with 0.5mol/LHCl, modification is carried out to sepiolite, solid-to-liquid ratio (g/ml) 1:3 is oscillation treatment 8h, then centrifugation in the constant temperature oscillator of 55 DEG C in temperature, add deionized water wash to pH value 6, centrifugation is placed in the loft drier of 55 DEG C and dries, modification is carried out in c, the coupling of dried sepiolite recycle silicon alkane, concrete operations are as follows: the silane coupling agent KH792 taking dry sepiolite quality 2%, 2-3% vinyl three ('beta '-methoxy oxyethyl group) silane, 20-25% ferrophosphorus powder, high speed dispersion 4300-4500 rev/min, 20-30 minute, sepiolite good for coupling agent treatment is taken out, first cleans with ethanolic soln and then repeatedly rinse with deionized water, filter in neutral, the sepiolite cleaned up is dried, grinds to form superfine nano powder, modified Nano sepiolite can be obtained, described rust-preventive agent is prepared from by the component of following weight part: citric acid 49-51, aluminium powder 0.8-0.9, gelatin 0.3-0.5, Tritolyl Phosphate 0.2-0.4, talcum powder 1-2, total amount 100 is added to water, after formula material is added mixing and stirring in proportion successively, mix through ground elimination.
2. the production method of a kind of Alkyd resin vehicle primer according to claim 1, it is characterized in that, (1) first Synolac, melamine resin, two benzoylphenyl phosphine oxide, dipropylene glycol monomethyl ether, sodium laurylsulfate, myo-Inositol hexaphosphate and vinylbenzene are mixed by formula rate, high-speed stirring; (2) all the other components in formula are joined in the emulsion of step (1) gained and are fully ground to particle diameter 25-40 μm, then after 30 minutes, with 280 order filter-cloth filterings, get product in high-speed stirring.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210389835.1A CN103073975B (en) | 2012-10-15 | 2012-10-15 | A kind of Alkyd resin vehicle primer and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210389835.1A CN103073975B (en) | 2012-10-15 | 2012-10-15 | A kind of Alkyd resin vehicle primer and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103073975A CN103073975A (en) | 2013-05-01 |
| CN103073975B true CN103073975B (en) | 2016-03-02 |
Family
ID=48150678
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210389835.1A Expired - Fee Related CN103073975B (en) | 2012-10-15 | 2012-10-15 | A kind of Alkyd resin vehicle primer and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103073975B (en) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103396726B (en) * | 2013-06-25 | 2016-02-17 | 寿县风顺船舶修造有限责任公司 | A kind of marine metal rust-inhibiting paint and preparation method thereof |
| CN103421402A (en) * | 2013-08-26 | 2013-12-04 | 江苏中威重工机械有限公司 | High-temperature-resistant anticorrosion anti-rust paint |
| CN103483997B (en) * | 2013-09-30 | 2015-09-09 | 中国兵器工业集团第五三研究所 | One can weld antifouling paste |
| CN103695921B (en) * | 2013-12-02 | 2016-05-18 | 马聪 | A kind of derusting rust-proofing liquid containing alkyd resins and preparation method thereof |
| CN104356901A (en) * | 2014-10-23 | 2015-02-18 | 安徽省金盾涂料有限责任公司 | Easily-cured flame-retardant corrosion-resistant coating |
| CN105153897A (en) * | 2015-09-14 | 2015-12-16 | 安徽华润涂料有限公司 | Domestic outer security door prime paint and preparation method thereof |
| CN106047105A (en) * | 2016-07-18 | 2016-10-26 | 天长市巨龙车船涂料有限公司 | Alkyd resin paint special for stainless steel |
| CN106379107B (en) * | 2016-09-27 | 2018-08-07 | 瞿勤荣 | Electric bicycle hub cap |
| CN109021643A (en) * | 2018-07-16 | 2018-12-18 | 安徽正阳机械科技有限公司 | A kind of heat-resisting paint outside energy-saving environment protection air heater |
| CN109539191A (en) * | 2018-11-19 | 2019-03-29 | 安徽蓝锐电子科技有限公司 | A kind of LED lamp that heat dissipation performance is outstanding |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1743390A (en) * | 2004-09-03 | 2006-03-08 | 罗门哈斯公司 | Multilayer coatings having color matched adhesion promoters |
| CN1942544A (en) * | 2005-03-10 | 2007-04-04 | 德古萨公司 | Aqueous coating substance compositions having an improved resistance to stoning |
| CN101117547A (en) * | 2006-08-02 | 2008-02-06 | 福特汽车公司 | Coating compositions and methods of applying the same |
| CN102031058A (en) * | 2010-12-01 | 2011-04-27 | 陕西宝塔山油漆股份有限公司 | Composite interpenetrating polymer network coating and preparation method thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5736149A (en) * | 1980-08-14 | 1982-02-26 | Dainippon Ink & Chem Inc | Coating resin composition |
-
2012
- 2012-10-15 CN CN201210389835.1A patent/CN103073975B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1743390A (en) * | 2004-09-03 | 2006-03-08 | 罗门哈斯公司 | Multilayer coatings having color matched adhesion promoters |
| CN1942544A (en) * | 2005-03-10 | 2007-04-04 | 德古萨公司 | Aqueous coating substance compositions having an improved resistance to stoning |
| CN101117547A (en) * | 2006-08-02 | 2008-02-06 | 福特汽车公司 | Coating compositions and methods of applying the same |
| CN102031058A (en) * | 2010-12-01 | 2011-04-27 | 陕西宝塔山油漆股份有限公司 | Composite interpenetrating polymer network coating and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103073975A (en) | 2013-05-01 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103073975B (en) | A kind of Alkyd resin vehicle primer and preparation method thereof | |
| CN102993793B (en) | A kind of Anti-crack automobile primer and preparation method thereof | |
| CN103073969B (en) | A kind of Epoxy resin antirust paint and preparation method thereof | |
| CN102888137B (en) | A kind of Ultraviolet-resistinmetal metal anti-rust paint and preparation method thereof | |
| CN102993841B (en) | A kind of waterborne flame retardant anticorrosive paint | |
| JP4800578B2 (en) | Pigment preparation | |
| CN102993899B (en) | A kind of salt spray resistance metal anti-corrosion paint and preparation method thereof | |
| CN102391743A (en) | Aqueous primer used for bicycles | |
| CN102627872A (en) | Method for modifying attapulgite clay | |
| CN104817929B (en) | A kind of track traffic water-base epoxy dual-component coating and preparation method thereof | |
| CN102993794B (en) | A kind of wheel refractory anti-rust paint peculiar to vessel and preparation method thereof | |
| CN102888179B (en) | Alkaline-resisting metallic anti-rust paint of a kind of oil resistant and preparation method thereof | |
| CN104449391A (en) | Iron red anticorrosive paint and preparation method thereof | |
| CN102993791B (en) | A kind of metallic paint and preparation method thereof | |
| CN104817856A (en) | Water-based aluminum powder pigment, and preparation method and application thereof | |
| CN102888156B (en) | A kind of Uvioresistant fluorocarbon metal anti-rust paint and preparation method thereof | |
| CN106590432B (en) | Cold spray zinc surface sealer of one kind and preparation method thereof | |
| CN103073978B (en) | A kind of Polyurethane automotive primer and preparation method thereof | |
| CN103087627B (en) | A kind of metal aluminum alloy silane surface treatment agent and preparation method thereof | |
| CN101705039A (en) | High-temperature-resistant flame-retardant anti-rust paint and preparation method thereof | |
| CN102888167B (en) | A kind of aging-resistant metal anti-rust paint and preparation method thereof | |
| CN104449390A (en) | Quick-drying, alcohol-soluble and antirust paint and preparation method thereof | |
| CN102888169B (en) | A kind of alkaline-resisting oil-resistant metal antirust paint and preparation method thereof | |
| CN102888172B (en) | A kind of water-fast aging-resistant metal anti-rust paint and preparation method thereof | |
| CN105949902A (en) | Anticorrosion water-borne coating for surfaces of mechanical environmental protection equipment and preparation method of anticorrosion water-borne coating |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160302 Termination date: 20161015 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |