CN103073255B - A kind of sealing material making method for gas extraction hole - Google Patents

A kind of sealing material making method for gas extraction hole Download PDF

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Publication number
CN103073255B
CN103073255B CN201210567986.1A CN201210567986A CN103073255B CN 103073255 B CN103073255 B CN 103073255B CN 201210567986 A CN201210567986 A CN 201210567986A CN 103073255 B CN103073255 B CN 103073255B
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CN
China
Prior art keywords
sealing material
metakaolin
wilkinite
flyash
lime
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201210567986.1A
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Chinese (zh)
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CN103073255A (en
Inventor
符勇
熊祖强
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Henan University of Technology
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Henan University of Technology
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Priority to CN201210567986.1A priority Critical patent/CN103073255B/en
Publication of CN103073255A publication Critical patent/CN103073255A/en
Application granted granted Critical
Publication of CN103073255B publication Critical patent/CN103073255B/en
Expired - Fee Related legal-status Critical Current
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Abstract

The invention discloses a kind of sealing material of the gas extraction hole be made up of sulphur plaster of Paris, flyash, lime, wilkinite and metakaolin.Because desulphurization building gypsum is formed by desulphurization gypsum calcination, when adding water, meeting and flyash, lime and metakaolin generate a large amount of ettringite, and form reticulated structure, make slurry very rapid hardening, and produce intensity, and wilkinite falls into water body by volcanic ash is formed, and is a kind of natural nano-material, be filled in above-mentioned reticulated structure, serve good sealing process.

Description

A kind of sealing material making method for gas extraction hole
Technical field
What the present invention relates to is mining material use technical field, is specifically related to a kind of sealing material making method for gas extraction hole.
Background technology
Gas is the maximum technical barrier run in mining activity.Gas extraction hole is the effective ways solving gas problem, but the sealing of hole problem of gas extraction hole is a thorny problem always.If adopt silicate cement sealing of hole, shrink due to during silicate cement consolidation, make sealing of hole operation failure; If adopt aluminate cement sealing of hole, because inside during aluminate cement consolidation can produce some tiny cracks, closed material was lost efficacy; If adopt chemical pulp sealing of hole, cost is too high on the one hand, and chemical pulp is inflammable on the other hand, there is downhole safety hidden danger, neither a kind of desirable sealing material.
Summary of the invention
The object of the invention is to provide a kind of sealing material making method for gas extraction hole, and it can solve problem existing in background technology effectively.
This sealing material is made up of sulphur plaster of Paris, flyash, lime, wilkinite and metakaolin.
The composition range of this sealing material is:
The preferred component scope of this sealing material is:
The optimal components scope of this sealing material is:
The manufacture method of this sealing material is:
1, sulphur plaster of Paris, flyash, lime, wilkinite and metakaolin are processed into respectively fineness and are not less than 200 object powder;
2, sulphur plaster of Paris, flyash, lime, wilkinite and metakaolin after processing are proportionally mixed, to obtain final product.
Owing to have employed above technical scheme, the present invention has following beneficial effect: because desulphurization building gypsum is formed by desulphurization gypsum calcination, when adding water, meeting and flyash, lime and metakaolin generate a large amount of ettringite, and form reticulated structure, make slurry very rapid hardening, and produce intensity, and wilkinite falls into water body by volcanic ash is formed, be a kind of natural nano-material, be filled in above-mentioned reticulated structure, serve good sealing process.
Embodiment
The technique means realized to make the present invention, creation characteristic, reaching object and effect is easy to understand, below the technical scheme in the embodiment of the present invention being clearly and completely described.
This embodiment is achieved by the following technical solutions, and it is made up of sulphur plaster of Paris, flyash, lime, wilkinite and metakaolin, and its composition range is:
The manufacture method of sealing material is:
1, sulphur plaster of Paris, flyash, lime, wilkinite and metakaolin are processed into respectively fineness and are not less than 200 object powder;
2, sulphur plaster of Paris, flyash, lime, wilkinite and metakaolin after processing are proportionally mixed, to obtain final product.
During use, by water and sealing material in 0.5: 1 ratio stir and can use.
Owing to have employed above technical scheme, the present invention has following beneficial effect: because desulphurization building gypsum is formed by desulphurization gypsum calcination, when adding water, meeting and flyash, lime and metakaolin generate a large amount of ettringite, and form reticulated structure, make slurry very rapid hardening, and produce intensity, and wilkinite falls into water body by volcanic ash is formed, be a kind of natural nano-material, be filled in above-mentioned reticulated structure, serve good sealing process.
Last it is noted that above embodiment is only in order to illustrate technical scheme of the present invention, be not intended to limit; Although with reference to previous embodiment to invention has been detailed description, those of ordinary skill in the art should be appreciated that it still can be modified to the technical scheme described in foregoing embodiments, or carries out equivalent replacement to wherein portion of techniques feature; And these amendments or replacement, do not make the essence of appropriate technical solution depart from the spirit and scope of various embodiments of the present invention technical scheme.

Claims (1)

1. a sealing material for the gas extraction hole be made up of sulphur plaster of Paris, flyash, lime, wilkinite and metakaolin, is characterized in that the composition range of this sealing material is:
A kind of manufacture method of above-mentioned sealing material:
(1) sulphur plaster of Paris, flyash, lime, wilkinite and metakaolin are processed into respectively fineness and are not less than 200 object powder;
(2) sulphur plaster of Paris, flyash, lime, wilkinite and metakaolin after processing are proportionally mixed, to obtain final product.
CN201210567986.1A 2012-12-13 2012-12-13 A kind of sealing material making method for gas extraction hole Expired - Fee Related CN103073255B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201210567986.1A CN103073255B (en) 2012-12-13 2012-12-13 A kind of sealing material making method for gas extraction hole

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201210567986.1A CN103073255B (en) 2012-12-13 2012-12-13 A kind of sealing material making method for gas extraction hole

Publications (2)

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CN103073255A CN103073255A (en) 2013-05-01
CN103073255B true CN103073255B (en) 2015-08-12

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Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103849362B (en) * 2014-02-18 2016-06-15 六盘水师范学院 The formula of a kind of coal bed gas extraction discharge drilling sealing material and preparation method
US10173647B2 (en) 2016-03-24 2019-01-08 Ford Global Technologies, Llc Systems and methods for efficient automatic vehicle washing
CN108101483A (en) * 2017-12-26 2018-06-01 阳泉煤业(集团)有限责任公司 It is a kind of for early-strength cement base sealing material of gas pumping and preparation method thereof
CN111389866A (en) * 2020-04-06 2020-07-10 昆明理工大学 Method for neutralizing and mineralizing acid tailings

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1673168A (en) * 2004-03-25 2005-09-28 上海静安新建材科研所有限公司 Three-slag mixed material with waste gypsum modified flyash
JP2007077392A (en) * 2005-08-17 2007-03-29 Kyokado Eng Co Ltd Cavity filler
CN101182143A (en) * 2007-11-07 2008-05-21 北京航空航天大学 Preparation of composite high-expansion cementing material by using industrial slag and preparation technique thereof
CN101353261A (en) * 2008-09-01 2009-01-28 江苏省一夫新材料科技有限公司 Waterproof fireproofing inorganic plugging material

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1673168A (en) * 2004-03-25 2005-09-28 上海静安新建材科研所有限公司 Three-slag mixed material with waste gypsum modified flyash
JP2007077392A (en) * 2005-08-17 2007-03-29 Kyokado Eng Co Ltd Cavity filler
CN101182143A (en) * 2007-11-07 2008-05-21 北京航空航天大学 Preparation of composite high-expansion cementing material by using industrial slag and preparation technique thereof
CN101353261A (en) * 2008-09-01 2009-01-28 江苏省一夫新材料科技有限公司 Waterproof fireproofing inorganic plugging material

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