CN103073255A - Production method of hole sealing material for gas drainage hole - Google Patents

Production method of hole sealing material for gas drainage hole Download PDF

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Publication number
CN103073255A
CN103073255A CN2012105679861A CN201210567986A CN103073255A CN 103073255 A CN103073255 A CN 103073255A CN 2012105679861 A CN2012105679861 A CN 2012105679861A CN 201210567986 A CN201210567986 A CN 201210567986A CN 103073255 A CN103073255 A CN 103073255A
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China
Prior art keywords
sealing material
plaster
metakaolin
hole
lime
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Application number
CN2012105679861A
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Chinese (zh)
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CN103073255B (en
Inventor
符勇
熊祖强
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Henan University of Technology
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Henan University of Technology
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Priority to CN201210567986.1A priority Critical patent/CN103073255B/en
Publication of CN103073255A publication Critical patent/CN103073255A/en
Application granted granted Critical
Publication of CN103073255B publication Critical patent/CN103073255B/en
Expired - Fee Related legal-status Critical Current
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Abstract

The invention discloses hole sealing material for a gas drainage hole, which comprises sulfur building plaster, coal ash, lime, bentonite and metakaolin. As desulfurization building plaster is formed by calcining desulphurization plaster, the desulfurization building plaster generates a large amount of ettringite with the coal ash, the line and the metakaolin when water is added, and net structures are formed, so that slurry is quickly hardened, and the strength is generated; and the bentonite which is formed by dropping volcanic ash in water is a natural nanometer material, and is filled in the net structures, so as to achieve excellent sealing effect.

Description

A kind of sealing material making method for gas extraction hole
Technical field
What the present invention relates to is mining material use technical field, is specifically related to a kind of sealing material making method for gas extraction hole.
Background technology
Gas is the maximum technical barrier that runs in the mining activity.Gas extraction hole is the effective ways that solve the gas problem, but the sealing of hole problem of gas extraction hole is a thorny problem always.If adopt the silicate cement sealing of hole, because silicate cement shrinks when fixed, make sealing of hole operation failure; If adopt the aluminate cement sealing of hole, can produce some tiny cracks because aluminate cement is inner when fixed, closed material was lost efficacy; If adopt the chemical pulp sealing of hole, cost is too high on the one hand, and chemical pulp is inflammable on the other hand, has downhole safety hidden danger, neither a kind of desirable sealing material.
Summary of the invention
The object of the invention provides a kind of sealing material making method for gas extraction hole, and it can solve existing problem in the background technology effectively.
This sealing material is comprised of sulphur plaster of Paris, flyash, lime, wilkinite and metakaolin.
The composition range of this sealing material is:
Figure BSA00000829806700011
The preferred component scope of this sealing material is:
The optimal components scope of this sealing material is:
Figure BSA00000829806700022
The manufacture method of this sealing material is:
1, sulphur plaster of Paris, flyash, lime, wilkinite and metakaolin are processed into respectively fineness and are not less than 200 purpose powder;
2, sulphur plaster of Paris, flyash, lime, wilkinite and the metakaolin after will processing proportionally mixes, and get final product.
Owing to having adopted above technical scheme, the present invention has following beneficial effect: because desulphurization building gypsum is formed by desulphurization gypsum calcination, meeting and flyash, lime and metakaolin generate a large amount of ettringite when adding water, and the formation reticulated structure, make very rapid hardening of slurry, and produce intensity, and falling into water body by volcanic ash, wilkinite forms, be a kind of natural nano-material, filling has been played good sealing process in above-mentioned reticulated structure.
Embodiment
For technique means, creation characteristic that the present invention is realized, reach purpose and effect is easy to understand, the below is clearly and completely described the technical scheme in the embodiment of the invention.
This embodiment is to be achieved by the following technical solutions, and it is comprised of sulphur plaster of Paris, flyash, lime, wilkinite and metakaolin, and its composition range is:
Figure BSA00000829806700031
The manufacture method of sealing material is:
1, sulphur plaster of Paris, flyash, lime, wilkinite and metakaolin are processed into respectively fineness and are not less than 200 purpose powder;
2, sulphur plaster of Paris, flyash, lime, wilkinite and the metakaolin after will processing proportionally mixes, and get final product.
During use, water and sealing material can be used in 0.5: 1 ratio stirring.
Owing to having adopted above technical scheme, the present invention has following beneficial effect: because desulphurization building gypsum is formed by desulphurization gypsum calcination, meeting and flyash, lime and metakaolin generate a large amount of ettringite when adding water, and the formation reticulated structure, make very rapid hardening of slurry, and produce intensity, and falling into water body by volcanic ash, wilkinite forms, be a kind of natural nano-material, filling has been played good sealing process in above-mentioned reticulated structure.
It should be noted that at last: above embodiment only in order to technical scheme of the present invention to be described, is not intended to limit; Although with reference to previous embodiment the present invention is had been described in detail, those of ordinary skill in the art should be appreciated that it still can make amendment to the technical scheme that aforementioned each embodiment puts down in writing, and perhaps part technical characterictic wherein is equal to replacement; And these modifications or replacement do not make the essence of appropriate technical solution break away from the spirit and scope of various embodiments of the present invention technical scheme.

Claims (2)

1. the sealing material of a gas extraction hole that is comprised of sulphur plaster of Paris, flyash, lime, wilkinite and metakaolin is characterized in that the composition range of this sealing material is:
Figure FSA00000829806600011
2. the manufacture method of a sealing material:
(1) sulphur plaster of Paris, flyash, lime, wilkinite and metakaolin are processed into respectively fineness and are not less than 200 purpose powder;
(2) sulphur plaster of Paris, flyash, lime, wilkinite and the metakaolin after will processing proportionally mixes, and get final product.
CN201210567986.1A 2012-12-13 2012-12-13 A kind of sealing material making method for gas extraction hole Expired - Fee Related CN103073255B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201210567986.1A CN103073255B (en) 2012-12-13 2012-12-13 A kind of sealing material making method for gas extraction hole

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201210567986.1A CN103073255B (en) 2012-12-13 2012-12-13 A kind of sealing material making method for gas extraction hole

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CN103073255A true CN103073255A (en) 2013-05-01
CN103073255B CN103073255B (en) 2015-08-12

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103849362A (en) * 2014-02-18 2014-06-11 六盘水师范学院 Formula of coal-bed gas extraction drilling-sealing material and preparation method thereof
CN108101483A (en) * 2017-12-26 2018-06-01 阳泉煤业(集团)有限责任公司 It is a kind of for early-strength cement base sealing material of gas pumping and preparation method thereof
US10173647B2 (en) 2016-03-24 2019-01-08 Ford Global Technologies, Llc Systems and methods for efficient automatic vehicle washing
CN111389866A (en) * 2020-04-06 2020-07-10 昆明理工大学 Method for neutralizing and mineralizing acid tailings

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1673168A (en) * 2004-03-25 2005-09-28 上海静安新建材科研所有限公司 Three-slag mixed material with waste gypsum modified flyash
JP2007077392A (en) * 2005-08-17 2007-03-29 Kyokado Eng Co Ltd Cavity filler
CN101182143A (en) * 2007-11-07 2008-05-21 北京航空航天大学 Preparation of composite high-expansion cementing material by using industrial slag and preparation technique thereof
CN101353261A (en) * 2008-09-01 2009-01-28 江苏省一夫新材料科技有限公司 Waterproof fireproofing inorganic plugging material

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1673168A (en) * 2004-03-25 2005-09-28 上海静安新建材科研所有限公司 Three-slag mixed material with waste gypsum modified flyash
JP2007077392A (en) * 2005-08-17 2007-03-29 Kyokado Eng Co Ltd Cavity filler
CN101182143A (en) * 2007-11-07 2008-05-21 北京航空航天大学 Preparation of composite high-expansion cementing material by using industrial slag and preparation technique thereof
CN101353261A (en) * 2008-09-01 2009-01-28 江苏省一夫新材料科技有限公司 Waterproof fireproofing inorganic plugging material

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103849362A (en) * 2014-02-18 2014-06-11 六盘水师范学院 Formula of coal-bed gas extraction drilling-sealing material and preparation method thereof
CN103849362B (en) * 2014-02-18 2016-06-15 六盘水师范学院 The formula of a kind of coal bed gas extraction discharge drilling sealing material and preparation method
US10173647B2 (en) 2016-03-24 2019-01-08 Ford Global Technologies, Llc Systems and methods for efficient automatic vehicle washing
CN108101483A (en) * 2017-12-26 2018-06-01 阳泉煤业(集团)有限责任公司 It is a kind of for early-strength cement base sealing material of gas pumping and preparation method thereof
CN111389866A (en) * 2020-04-06 2020-07-10 昆明理工大学 Method for neutralizing and mineralizing acid tailings

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