CN103054188B - Nozzle tipping paper for antibiosis cigarette, preparation method thereof, and nozzle for antibiosis cigarette - Google Patents
Nozzle tipping paper for antibiosis cigarette, preparation method thereof, and nozzle for antibiosis cigarette Download PDFInfo
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- CN103054188B CN103054188B CN201210457031.0A CN201210457031A CN103054188B CN 103054188 B CN103054188 B CN 103054188B CN 201210457031 A CN201210457031 A CN 201210457031A CN 103054188 B CN103054188 B CN 103054188B
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- 238000002360 preparation method Methods 0.000 title claims abstract description 13
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- 239000002904 solvent Substances 0.000 claims abstract description 30
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- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims description 12
- 239000003292 glue Substances 0.000 claims description 8
- 238000005507 spraying Methods 0.000 claims description 7
- IHZXTIBMKNSJCJ-UHFFFAOYSA-N 3-{[(4-{[4-(dimethylamino)phenyl](4-{ethyl[(3-sulfophenyl)methyl]amino}phenyl)methylidene}cyclohexa-2,5-dien-1-ylidene)(ethyl)azaniumyl]methyl}benzene-1-sulfonate Chemical compound C=1C=C(C(=C2C=CC(C=C2)=[N+](C)C)C=2C=CC(=CC=2)N(CC)CC=2C=C(C=CC=2)S([O-])(=O)=O)C=CC=1N(CC)CC1=CC=CC(S(O)(=O)=O)=C1 IHZXTIBMKNSJCJ-UHFFFAOYSA-N 0.000 claims description 4
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Abstract
The invention discloses nozzle tipping paper for an antibiosis cigarette, a preparation method thereof and a nozzle for the antibiosis cigarette. The nozzle tipping paper for the antibiosis cigarette is prepared by evenly distributing mixed medicine extracting solution on the surface of the tipping original paper and drying the mixed medicine extracting solution. The mixed medicine extracting solution is prepared by 10-27 parts of mother chrysanthemum, 3-7 parts of jasmine, 8-14 parts of fresh lemon, 2-17 parts of violet, 0.5-2 parts of radix angelicae pubescentis and 1.5-4 parts of folium eucalypti by weight, ethanol water solution serves as the extracting solvent after mixing, and the mixed medicine extracting solution with the relative density of 1.02-1.20 is prepared through reflux extraction. By means of the nozzle tipping paper for the antibiosis cigarette, the preparation method thereof and the nozzle for the antibiosis cigarette, the problem that after a cigarette box is opened, the nozzle of the cigarette can be contaminated by microorganisms easily is fundamentally solved. The antibiosis effect is further strengthened by using flax cellosilk beams, cellulose acetate beams, the nozzle tipping paper for the antibiosis cigarette and nozzle forming paper, and the cigarette can be further provided with the aroma of natural plants.
Description
Technical field
The present invention relates to a kind of cigarette mouth rod tipping paper and cigarette mouth rod, more specifically refer to a kind of antibacterial cigarette mouth rod tipping paper and preparation method thereof and antibacterial cigarette mouth rod.
Background technology
In recent years, along with the continuous concern of various circles of society to Smoking is harmful to your health problem, the understanding of the security of consumer to cigarette is also significantly increased.At present, most new cigarette filter tip purposes of design are to enter tar, nicotine and CO content in smoker oral cavity for reducing.But consumer is after opening a box cigarette, by approach such as finger contact, circulations of air, on cigarette filter tip, can adsorb in some air or the harmful microorganism of body surface, then enter in consumer's mouth by sucking, easily human body be produced to secondary injury.And the cigarette mouth rod at present with antibiotic effect have not been reported.
Summary of the invention
The object of the invention is to fill up the blank of prior art, a kind of antibacterial cigarette mouth rod tipping paper with antibiotic effect and preparation method thereof and antibacterial cigarette mouth rod are provided.
For achieving the above object, the designed antibacterial cigarette of the present invention is by described tipping body paper dry making after its surface uniform distribution medicine mixed extract with mouth rod tipping paper, described medicine mixed extract is take mother chrysanthemum 10～27 weight portions, jasmine 3～7 weight portions, new lemon 8～14 weight portions, violet 2～17 weight portions, levisticum 0.5～2 weight portion, folium eucalypti 1.5～4 weight portions as raw material, after mixing, with 0%～35% ethanol water as extract solvent, the medicine mixed extract that the relative density that refluxing extraction makes is 1.02～1.20.
Preferably, described medicine mixed extract is take mother chrysanthemum 18～25 weight portions, jasmine 3～6 weight portions, new lemon 8～12 weight portions, violet 7～15 weight portions, levisticum 1～2 weight portion, folium eucalypti 1.5～3 weight portions as raw material, after mixing, with 15%～30% ethanol water as extract solvent, the medicine mixed extract that the relative density that refluxing extraction makes is 1.05～1.15.
More preferably, described medicine mixed extract is take mother chrysanthemum 20 weight portions, jasmine 5 weight portions, new lemon 9 weight portions, violet 10 weight portions, levisticum 1.5 weight portions, folium eucalypti 2 weight portions as raw material, after mixing, with 30% ethanol water as extract solvent, the medicine mixed extract that the relative density that refluxing extraction makes is 1.05～1.15.
The preparation method of mouth rod tipping paper for above-mentioned antibacterial cigarette provided by the invention, comprises the following steps:
1) by raw material mother chrysanthemum 10～27 weight portions, jasmine 3～7 weight portions, new lemon 8～14 weight portions, violet 2～17 weight portions, levisticum 0.5～2 weight portion, folium eucalypti 1.5～4 weight portions, after mixing, with 0%～35% ethanol water as extract solvent refluxing extract twice, each 2～4 hours, each solvent adding amount that extracts is advisable with submergence raw material, merge extracted twice liquid, filter and obtain medicine mixed extract;
2) to tipping body paper surfaces externally and internally spraying medicine mixed extract, then tipping body paper is placed in 25～40 ℃ of environment dry, so that active ingredient is adsorbed on tipping body paper in medicine mixed extract, after being dried, obtain described antibacterial cigarette mouth rod tipping paper.
Preferred version is, described step 1) is by raw material mother chrysanthemum 18～25 weight portions, jasmine 3～6 weight portions, new lemon 8～12 weight portions, violet 10～15 weight portions, levisticum 1～1.5 weight portion, folium eucalypti 1.5～3 weight portions, after mixing, with 15%～30% ethanol water as extract solvent refluxing extract twice, each 2～4 hours, each solvent adding amount that extracts is advisable with submergence raw material, merges extracted twice liquid, filters and obtains medicine mixed extract.
More preferably scheme is, described step 1) is by raw material mother chrysanthemum 20 weight portions, jasmine 5 weight portions, new lemon 9 weight portions, violet 10 weight portions, levisticum 1.5 weight portions, folium eucalypti 2 weight portions, after mixing, with 30% ethanol water as extract solvent refluxing extract twice, each 3.5 hours, each solvent adding amount that extracts is advisable with submergence raw material, merges extracted twice liquid, filters and obtains medicine mixed extract.
The present invention also provides a kind of antibacterial cigarette mouth rod, comprise mouth rod body and wrap up the cigarette plug paper of described mouth rod body, described cigarette plug paper outside is enclosed with antibacterial cigarette mouth rod tipping paper claimed in claim 1, described mouth rod body according to the interlaced arrangement of the ratio of mass ratio 0.1～6:1, then adds liquid glue aftershaping to obtain by flax fiber tow and acetate silk.
Wherein, the mass ratio of described flax fiber tow and acetate silk is preferably 0.5～4.5:1, more preferably 3:1.
Antibacterial cigarette by the preferred embodiment of mouth rod is: comprise mouth rod body and wrap up the cigarette plug paper of described mouth rod body, described cigarette plug paper outside is enclosed with antibacterial cigarette mouth rod tipping paper, described mouth rod body according to the interlaced arrangement of the ratio of mass ratio 3:1, then adds liquid glue aftershaping to obtain by flax fiber tow and acetate silk.Described antibacterial cigarette is by described tipping body paper dry making after its surface uniform distribution medicine mixed extract with mouth rod tipping paper, described medicine mixed extract is take mother chrysanthemum 20 weight portions, jasmine 5 weight portions, new lemon 9 weight portions, violet 10 weight portions, levisticum 1.5 weight portions, folium eucalypti 2 weight portions as raw material, after mixing, with 30% ethanol water as extract solvent, the medicine mixed extract that the relative density that refluxing extraction makes is 1.05～1.15.
The effect of the each component of the present invention is as follows:
Flax fiber: pliability, good hygroscopicity, antibiotic property is strong, the bacteriostasis rate of the international standard bacterium such as Pseudomonas aeruginosa, white bead-containing bacteria is reached more than 65%, to the bacteriostasis rate of Escherichia coli, gold-coloured staphylococci up to more than 90%.
Mother chrysanthemum: anti-inflammation, has inhibitory action to staphylococcus aureus, shigella flexneri, typhoid bacillus etc.
Jasmine: clearing heat and detoxicating.
New lemon: be rich in vitamin C, there is the effect of bactericidal antiphlogistic.
Violet: clearing heat and detoxicating, remove oral peculiar smell.
Levisticum: experiment in vitro shows that 11 kinds of bacterial strains are had to antimicrobial spectrum widely.
Folium eucalypti: gram-positive bacterium is had to inhibitory action.
Beneficial effect of the present invention: by a kind of antibacterial cigarette mouth rod tipping paper of the natural botanical extraction liquid that contains antibiotic effect is provided, fundamentally solved after cigarette case unlatching, cigarette filter tip is easily subject to the problem of microbial contamination.The mouth rod body that utilizes flax fiber tow and acetate silk rational proportion to make, antibacterial cigarette is wrapped on mouth rod body with mouth rod tipping paper together with cigarette plug paper, the antibacterial cigarette mouth rod making, not only there is mouthfeel and the effect of traditional cigarette, meet smoker's Physiological Psychology requirement, further strengthen its antibiotic effect, can also give the odor characteristic of cigarette natural plants simultaneously.Antibacterial cigarette is simple by the preparation method of mouth rod tipping paper, has good practicality.
Accompanying drawing explanation
Fig. 1 is the bacterial clump growth conditions figure of antibacterial cigarette mouth rod in contrast test 1.
Fig. 2 is the bacterial clump growth conditions figure of common cigarette mouth rod in contrast test 1.
Fig. 3 places the bacterial clump growth conditions figure after 24h in antibacterial cigarette mouth rod air in contrast test 2.
Fig. 4 places the bacterial clump growth conditions figure after 96h in antibacterial cigarette mouth rod air in contrast test 2.
The specific embodiment
Below in conjunction with the drawings and specific embodiments, the present invention is described in further detail.
Embodiment 1
After mixing, 10 parts of raw material mother chrysanthemums, 5 parts of jasmines, 14 parts of new lemons, 2 parts of violets, 0.5 part of levisticum, folium eucalypti 3 parts (being above weight portion) extract twice as extracting solvent refluxing with 35% ethanol water, each 2 hours, each solvent adding amount that extracts is advisable with submergence raw material, merge extracted twice liquid, filter and obtain medicine mixed extract.
Flax fiber tow and acetate silk, according to the interlaced arrangement of the ratio of mass ratio 0.1:1, and are carried out to moulding with conventional liquid glue, and wrap up by forming paper tow outside.
To tipping body paper surfaces externally and internally spraying medicine mixed extract, then tipping body paper is placed in 35 ℃ of environment and is dried, obtain antibacterial cigarette mouth rod tipping paper 1.
Again antibacterial cigarette is wrapped in to forming paper outside with mouth rod tipping paper 2 and makes antibacterial cigarette mouth rod 1.
Embodiment 2
After mixing, 27 parts of raw material mother chrysanthemums, 7 parts of jasmines, 8 parts of new lemons, 2 parts of violets, 2 parts of levisticums, folium eucalypti 1.5 parts (being above weight portion) extract twice as extracting solvent refluxing with the aqueous solution, each 3 hours, each solvent adding amount that extracts is advisable with submergence raw material, merge extracted twice liquid, filter and obtain medicine mixed extract.
Flax fiber tow and acetate silk, according to the interlaced arrangement of the ratio of mass ratio 6:1, and are carried out to moulding with conventional liquid glue, and wrap up by forming paper tow outside.
To tipping body paper surfaces externally and internally spraying medicine mixed extract, then tipping body paper is placed in 25 ℃ of environment and is dried, obtain antibacterial cigarette mouth rod tipping paper 2.
Again antibacterial cigarette is wrapped in to forming paper outside with mouth rod tipping paper 2 and makes antibacterial cigarette mouth rod 2.
Embodiment 3
After mixing, 18 parts of raw material mother chrysanthemums, 3 parts of jasmines, 8 parts of new lemons, 10 parts of violets, 1 part of levisticum, folium eucalypti 1.5 parts (being above weight portion) extract twice as extracting solvent refluxing with 15% ethanol water, each 4 hours, each solvent adding amount that extracts is advisable with submergence raw material, merge extracted twice liquid, filter and obtain medicine mixed extract.
Flax fiber tow and acetate silk, according to the interlaced arrangement of the ratio of mass ratio 0.5:1, and are carried out to moulding with conventional liquid glue, and wrap up by forming paper tow outside.
To tipping body paper surfaces externally and internally spraying medicine mixed extract, then tipping body paper is placed in 30 ℃ of environment and is dried, obtain antibacterial cigarette mouth rod tipping paper 3.
Again antibacterial cigarette is wrapped in to forming paper outside with mouth rod tipping paper 3 and makes antibacterial cigarette mouth rod 3.
Embodiment 4
After mixing, 25 parts of raw material mother chrysanthemums, 6 parts of jasmines, 12 parts of new lemons, 15 parts of violets, 1.5 parts of levisticums, folium eucalypti 3 parts (being above weight portion) extract twice as extracting solvent refluxing with 25% ethanol water, each 2.5 hours, each solvent adding amount that extracts is advisable with submergence raw material, merge extracted twice liquid, filter and obtain medicine mixed extract.
Flax fiber tow and acetate silk, according to the interlaced arrangement of the ratio of mass ratio 4.5:1, and are carried out to moulding with conventional liquid glue, and wrap up by forming paper tow outside.
To tipping body paper surfaces externally and internally spraying medicine mixed extract, then tipping body paper is placed in 40 ℃ of environment and is dried, obtain antibacterial cigarette mouth rod tipping paper 4.
Again antibacterial cigarette is wrapped in to forming paper outside with mouth rod tipping paper 4 and makes antibacterial cigarette mouth rod 4.
Embodiment 5
After mixing, 20 parts of raw material mother chrysanthemums, 5 parts of jasmines, 9 parts of new lemons, 10 parts of violets, 1.5 parts of levisticums, folium eucalypti 2 parts (being above weight portion) extract twice as extracting solvent refluxing with 30% ethanol water, each 3.5 hours, each solvent adding amount that extracts is advisable with submergence raw material, merge extracted twice liquid, filter and obtain medicine mixed extract.
Flax fiber tow and acetate silk, according to the interlaced arrangement of the ratio of mass ratio 3:1, and are carried out to moulding with conventional liquid glue, and wrap up by forming paper tow outside.
To tipping body paper surfaces externally and internally spraying medicine mixed extract, then tipping body paper is placed in 30 ℃ of environment and is dried, obtain antibacterial cigarette mouth rod tipping paper 5.
Again antibacterial cigarette is wrapped in to forming paper outside with mouth rod tipping paper 5 and makes antibacterial cigarette mouth rod 5.
The test of smokeing panel test:
The antibacterial cigarette mouth rod of preparing in above-described embodiment is made to cigarette, and choose 30 experimenters and smoke panel test, smoking result shows, mouth rod taste Hui Tian for antibacterial cigarette, fragrance is pure and fresh, wherein antibacterial cigarette is more satisfactory by the cigarette mouthfeel of mouth rod 3,4 preparations, and antibacterial cigarette is the most desirable by the cigarette mouthfeel of mouth rod 5 preparations, illustrates that the medicine mixed extract in antibacterial mouth rod can also give the odor characteristic of cigarette natural plants.
Contrast test: this test adopts the mode of across comparison to prove:
1, antibacterial cigarette is placed on to 24h under identical atmospheric environment with mouth rod 5 and common cigarette mouth rod, then with the sterilized water of same amount, two kinds of cigarette mouth rods are cleaned, take out respectively 1mL cleaning fluid and carry out inoculated and cultured, under 37 ℃ of conditions, cultivate after 72h, in two kinds of cleaning fluid culture dishes, colony growth situation as shown in Figure 1, 2.
From Fig. 1 and Fig. 2, bacterial clump growing state can be found out, antibacterial cigarette will obviously be weaker than common mouth rod with the colony counts in the culture dish of mouth rod 5 and growing state.Can infer thus, utilize antibacterial cigarette mouth rod prepared by this method to there is better effects at antibiosis.
2, get 4 two of antibacterial cigarette mouth rods, and be placed in identical atmospheric environment.Wherein after a placement 24h, with sterilized water, it is cleaned, taking-up is taken out respectively 1mL cleaning fluid and is carried out inoculated and cultured, under 37 ℃ of conditions, cultivates after 72h, observes colony growth situation in culture dish; After another placement 96h, with the sterilized water of same amount, it is cleaned, taking-up is taken out respectively 1mL cleaning fluid and is carried out inoculated and cultured, under 37 ℃ of conditions, cultivates after 72h, observes colony growth situation in culture dish.
From Fig. 3 and Fig. 4, bacterial clump growing state can be found out, is placing after 24h and 96h, and colony counts and growing state in antibacterial mouth rod culture dish are basic identical.Can infer thus, use the standby cigarette of this legal system mouth rod to there is good stability and persistence at antibiosis.
Above two tests show, at the cigarette mouth rod that uses flax fiber and natural mixed plant extract to make, at the certain tool of antibiosis, have certain effect.
Claims (9)
1. a mouth rod tipping paper for antibacterial cigarette, comprise tipping body paper, it is characterized in that: described antibacterial cigarette mouth rod tipping paper is by described tipping body paper dry making after its surface uniform distribution medicine mixed extract, described medicine mixed extract is with mother chrysanthemum 10～27 weight portions, jasmine 3～7 weight portions, new lemon 8～14 weight portions, violet 2～17 weight portions, levisticum 0.5～2 weight portion, folium eucalypti 1.5～4 weight portions are raw material, after mixing, with 0%～35% ethanol water as extract solvent, the relative density that refluxing extraction makes is 1.02～1.20 medicine mixed extract.
2. mouth rod tipping paper for antibacterial cigarette according to claim 1, it is characterized in that: described medicine mixed extract is take mother chrysanthemum 18～25 weight portions, jasmine 3～6 weight portions, new lemon 8～12 weight portions, violet 7～15 weight portions, levisticum 1～2 weight portion, folium eucalypti 1.5～3 weight portions as raw material, after mixing, with 15%～30% ethanol water as extract solvent, the medicine mixed extract that the relative density that refluxing extraction makes is 1.05～1.15.
3. mouth rod tipping paper for antibacterial cigarette according to claim 1, it is characterized in that: described medicine mixed extract is take mother chrysanthemum 20 weight portions, jasmine 5 weight portions, new lemon 9 weight portions, violet 10 weight portions, levisticum 1.5 weight portions, folium eucalypti 2 weight portions as raw material, after mixing, with 30% ethanol water as extract solvent, the medicine mixed extract that the relative density that refluxing extraction makes is 1.05～1.15.
4. a preparation method for antibacterial cigarette use mouth rod tipping paper described in claim 1, comprises the following steps:
1) by raw material mother chrysanthemum 10～27 weight portions, jasmine 3～7 weight portions, new lemon 8～14 weight portions, violet 2～17 weight portions, levisticum 0.5～2 weight portion, folium eucalypti 1.5～4 weight portions, after mixing, with 0%～35% ethanol water as extract solvent refluxing extract twice, each 2～4 hours, each solvent adding amount that extracts is advisable with submergence raw material, merge extracted twice liquid, filter and obtain medicine mixed extract;
2) to tipping body paper surfaces externally and internally spraying medicine mixed extract, then tipping body paper is placed in 25～40 ℃ of environment dry, so that active ingredient is adsorbed on tipping body paper in medicine mixed extract, after being dried, obtain described antibacterial cigarette mouth rod tipping paper.
5. the preparation method of mouth rod tipping paper for antibacterial cigarette according to claim 4, it is characterized in that: described step 1) is by raw material mother chrysanthemum 18～25 weight portions, jasmine 3～6 weight portions, new lemon 8～12 weight portions, violet 10～15 weight portions, levisticum 1～1.5 weight portion, folium eucalypti 1.5～3 weight portions, after mixing, with 15%～30% ethanol water as extract solvent refluxing extract twice, each 2～4 hours, each solvent adding amount that extracts is advisable with submergence raw material, merge extracted twice liquid, filter and obtain medicine mixed extract.
6. the preparation method of mouth rod tipping paper for antibacterial cigarette according to claim 4, it is characterized in that: described step 1) is by raw material mother chrysanthemum 20 weight portions, jasmine 5 weight portions, new lemon 9 weight portions, violet 10 weight portions, levisticum 1.5 weight portions, folium eucalypti 2 weight portions, after mixing, with 30% ethanol water as extract solvent refluxing extract twice, each 3.5 hours, each solvent adding amount that extracts is advisable with submergence raw material, merges extracted twice liquid, filters and obtains medicine mixed extract.
7. an antibacterial cigarette mouth rod, comprise mouth rod body and wrap up the cigarette plug paper of described mouth rod body, it is characterized in that: described cigarette plug paper outside is enclosed with antibacterial cigarette mouth rod tipping paper claimed in claim 1, described mouth rod body according to the interlaced arrangement of the ratio of mass ratio 0.1～6:1, then adds liquid glue aftershaping to obtain by flax fiber tow and acetate silk.
8. antibacterial cigarette mouth rod according to claim 7, is characterized in that: the mass ratio of described flax fiber tow and acetate silk is 0.5 ~ 4.5:1.
9. antibacterial cigarette mouth rod according to claim 7, is characterized in that: the mass ratio of described flax fiber tow and acetate silk is 3:1.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210457031.0A CN103054188B (en) | 2012-11-14 | 2012-11-14 | Nozzle tipping paper for antibiosis cigarette, preparation method thereof, and nozzle for antibiosis cigarette |
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| CN201210457031.0A CN103054188B (en) | 2012-11-14 | 2012-11-14 | Nozzle tipping paper for antibiosis cigarette, preparation method thereof, and nozzle for antibiosis cigarette |
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| CN103054188B true CN103054188B (en) | 2014-04-16 |
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| CN104947505A (en) * | 2015-04-30 | 2015-09-30 | 湖北中烟工业有限责任公司 | Cigarette paper bacteriostat and application thereof |
| CN104839886B (en) * | 2015-04-30 | 2018-11-13 | 湖北中烟工业有限责任公司 | A kind of antibacterial cigarette filter and preparation method thereof |
| CN104789035B (en) * | 2015-05-06 | 2017-08-01 | 湖北中烟工业有限责任公司 | A kind of cigarette tipping paper and preparation method thereof |
| CN105167194B (en) * | 2015-06-17 | 2019-01-22 | 湖北中烟工业有限责任公司 | Cigarette mouth stick and preparation method thereof of the essence containing plant flavone |
| CN106509989A (en) * | 2016-12-05 | 2017-03-22 | 湖北中烟工业有限责任公司 | Mouth stick for antibacterial cigarette and its preparation method and tipping paper for antibacterial cigarette |
| CN108077997A (en) * | 2017-12-12 | 2018-05-29 | 江西中烟工业有限责任公司 | A kind of preparation method and applications of cigarette filter combination |
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| JP3384734B2 (en) * | 1997-12-09 | 2003-03-10 | 株式会社大阪前田製菓 | Substitute for cigarette paper and method for producing the same |
| WO2012061249A2 (en) * | 2010-11-02 | 2012-05-10 | Greenbutts Llc | Cigarette filter with modified wrapper |
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| CN1417413A (en) * | 2002-11-05 | 2003-05-14 | 天津大学 | Making process of Chinese cypress paper with wide-spectrum antiseptic function for cygarette |
| CN101191311A (en) * | 2006-11-20 | 2008-06-04 | 青岛喜盈门集团有限公司 | Antibiotic package paper |
| CN101666062A (en) * | 2008-09-04 | 2010-03-10 | 红塔烟草(集团)有限责任公司 | Tipping paper added with Chinese herbal medicinal additive and preparation method thereof |
| CN102240070A (en) * | 2011-06-30 | 2011-11-16 | 红云红河烟草(集团)有限责任公司 | Filter stick shaping paper capable of improving cigarette smoking quality and preparation method thereof |
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