CN103033480A - Testing method for color fastness to saliva of textile - Google Patents
Testing method for color fastness to saliva of textile Download PDFInfo
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- CN103033480A CN103033480A CN2012105799897A CN201210579989A CN103033480A CN 103033480 A CN103033480 A CN 103033480A CN 2012105799897 A CN2012105799897 A CN 2012105799897A CN 201210579989 A CN201210579989 A CN 201210579989A CN 103033480 A CN103033480 A CN 103033480A
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Abstract
The invention relates to the technical field of color fastness testing of textile, in particular to a testing method for color fastness to saliva of the textile. The testing method comprises the following steps of preparing artificial saliva, bonding a to-be-tested sample cut to a given size with multi-fiber accompanying fabric to form a composite sample, soaking in the artificial saliva, extruding the composite sample with a glass rod after soaking, pressing the composite sample with a counter weight, placing the composite sample in a drying oven simulating human body temperature, drying, placing the composite sample under standard atmospheric conditions with the temperature of 18-22 DEG C and the relative humidity of 61-69%, humidifying for at least four hours, and conducting an evaluation test on discoloring of the to-be-tested sample and staining of the accompanying fabric with a standard discoloring gray card and a standard staining gray card respectively. With the adoption of the testing method, the degree and the grade of the color fastness to saliva of the textile can be evaluated, deficiencies of the traditional staining test with filter paper are overcome, preparation of the artificial saliva is more reasonable, and the testing method is simple and easy to operate.
Description
[technical field]
The present invention relates to textile color stability detection technique field, specifically a kind of method of testing of the textile colour fastness of anti-the saliva.
[background technology]
Children use textile, because the singularity of its applicable object, so that the consumer has higher requirement to its security.Among numerous requirements, children's saliva is one of important indicator for the extraction of dyestuff in the textile, and the dyestuff on the relatively poor textile of colorfastness enters in children's body through the saliva extraction, bring for children's personal safety and have a strong impact on.Therefore, need a method of testing that the colour fastness of the anti-saliva of textile is graded.At present, Germany has for saliva the qualitative test method is arranged, and it uses filter paper to carry out the staining test, and whether observe at last filter paper has staining, be anti-saliva or not anti-saliva thereby decide conclusion, the shortcoming of this method of testing is to represent its colour fastness degree and rank; And in the testing standard of the domestic colour fastness of anti-the saliva, unreasonable for the prescription of artificial saliva, thus the test of saliva colour fastness in the textile affected; Therefore, if can provide the artificial saliva prescription more reasonable, and can represent other method of testing of colour fastness level of the anti-saliva of textile, consumer and manufacturer will have very important significance for the demand for control of this performance on the domestic and international market to satisfy.
[summary of the invention]
Purpose of the present invention is exactly to solve above-mentioned deficiency, and provide a kind of method of testing of the textile colour fastness of anti-the saliva, not only can evaluate colour fastness degree and the rank of the anti-saliva of textile, carry out the defective of staining test to overcome traditional employing filter paper, and the artificial saliva configuration is more reasonable, and method of testing is also more simple.
Purpose of the present invention can be achieved through the following technical solutions:
A kind of method of testing of the textile colour fastness of anti-the saliva may further comprise the steps:
1) configuration artificial saliva;
2) cutting sample to be tested is fitted sample to be tested and multifilament adjacent fabric, forms composite sample;
3) take by weighing the artificial saliva that disposes in an amount of step 1), add in the double dish, with step 2) in composite sample be soaked in the artificial saliva fully;
4) after immersion is finished, composite sample is taken out, and be placed on the PERSPIRATION COLOR FASTNESS instrument, by the weight of PERSPIRATION COLOR FASTNESS instrument composite sample is exerted pressure;
5) the PERSPIRATION COLOR FASTNESS instrument is put into to preset temperature be 37 ℃ ± 1 ℃ baking oven, kept 4 hours;
6) composite sample is taken off from the PERSPIRATION COLOR FASTNESS instrument, at the air drying that is no more than 60 ℃;
7) after the drying, composite sample is placed on 20 ℃ ± 2 ℃ of temperature, under the standard atmosphere condition of relative humidity 65 ± 4%, damping at least 4 hours;
8) adopt standard variable color ash card, standard staining ash card respectively test to be evaluated in the variable color of sample to be tested and the staining of adjacent fabric.
The configuration step of artificial saliva is in the described step 1); 0.75g potassium chloride, 0.33g sodium chloride and 0.53g sal tartari are added in the 1L beaker; add again three grades of water of about 900ml; then add 0.17g magnesium chloride hexahydrate, 0.15g calcium chloride dihydrate and 0.76g hydrogen phosphate dihydrate dipotassium; stir until fully dissolving; with the pH value of 1% hydrochloric acid adjustment mixed solution, the pH value of guaranteeing mixed solution is 6.8 ± 0.1, is settled to 1L with three grades of water at last.
Described step 2) in, sample to be tested is cut into 40mm * 100mm, sample to be tested and multifilament adjacent fabric is sew on along minor face close, and forms composite sample.
In the described step 3), the weight ratio of artificial saliva and composite sample is 100:1, adopts the extruding of resin plate or glass plate that composite sample is soaked in the artificial saliva fully, soaks action and keeps 30min ± 2min.
Between described step 3) and the step 4), the step that adopts glass bar that the composite sample that takes out is pushed is arranged, so that the composite sample liquid carrying rate is 100% ± 5%.
In the described step 4), composite sample is placed on resin plate or the glass plate, resin plate or glass plate are placed on the PERSPIRATION COLOR FASTNESS instrument, the pressurization weight of PERSPIRATION COLOR FASTNESS instrument applies the pressure of 12kPa to composite sample.
In the described step 5), the PERSPIRATION COLOR FASTNESS instrument is put into baking oven and was kept 4 hours;
Described PERSPIRATION COLOR FASTNESS instrument comprises stainless steel mounting, weight and resin plate or glass plate.
Compare with the method for testing technology of the traditional textile colour fastness of anti-the saliva, beneficial effect of the present invention: the textile colour fastness of anti-saliva method of testing provided by the present invention, not only can evaluate colour fastness degree and the rank of the anti-saliva of textile, carry out the defective of staining test to overcome traditional employing filter paper, and the artificial saliva configuration is more reasonable, has guaranteed that test result is more accurate; In addition, the method of testing of the textile colour fastness of anti-saliva the of the present invention, simple to operate, easy row, not only for guaranteeing that children provide strong instrument with textile for children's security, and for the children of domestic and international production firm and Supplier Selection safety also provide a quantitative criteria with textile, be worthy of popularization.
[description of drawings]
Fig. 1 is the structural representation of PERSPIRATION COLOR FASTNESS instrument among the present invention;
Among the figure: 1, weight 2, spring are pressed frame 3, trip bolt 4, glass plate or resin plate 5, stainless steel mounting.
[embodiment]
Further specify below below in conjunction with embodiment the present invention being done:
Embodiment 1
One, sample to be tested: the knitting pullover of mazarine children
Two, main experimental instrument or material:
(1) PERSPIRATION COLOR FASTNESS tester (such as accompanying drawing 1): resin plate or the glass plate 4 of being pressed the weight 1 of frame 2, trip bolt 3,50N (± 1%) and being of a size of 60mm * 115mm * 1.5mm by stainless steel mounting 5, spring form, and can apply to composite sample the pressure (12.5kPa) of uniform regulation;
(2) baking oven: temperature can be set in 37 ℃ ± 1 ℃;
(3) double dish: diameter 125mm;
(4) glass bar;
(5) pH meter: precision 0.05 or more than;
(6) multifilament adjacent fabric: meet GB/T11404;
(7) sewing thread: white and do not contain fluorescer;
(8) sewing needle.
Three, testing procedure:
1) configuration artificial saliva, 0.75g potassium chloride, 0.33g sodium chloride and 0.53g sal tartari are added in the 1L beaker, add again three grades of water of about 900ml, then add 0.17g magnesium chloride hexahydrate, 0.15g calcium chloride dihydrate and 0.76g hydrogen phosphate dihydrate dipotassium, stir until fully dissolving, adopt in case of necessity 1% hydrochloric acid to adjust the pH value of mixed solution, the pH value of guaranteeing mixed solution is 6.8 ± 0.1, is settled to 1L with three grades of water at last;
2) sample to be tested is cut into 40mm * 100mm size, and sample to be tested and multifilament adjacent fabric sew on along minor face close, form composite sample, guarantee that every kind of color all contacts with every converted top of multifilament adjacent fabric, can get several in case of necessity more;
3) take by weighing the weight of composite sample, calculate the artificial saliva milliliter number that needs according to the 100:1 bath raio, add in the double dish, then be soaked in composite sample in the double dish fully, adopt the extruding of resin plate or glass plate that it is soaked into fully, soak action and keep 30min ± 2min;
4) after immersion was finished, adopting the glass bar extruding to make its liquid carrying rate the composite sample taking-up was 100% ± 5%;
5) composite sample is placed on resin plate or the glass plate, a resin plate or glass plate are placed on the PERSPIRATION COLOR FASTNESS instrument, add 6 resin plates or glass plate, place at most 6 composite samples, the weight by the PERSPIRATION COLOR FASTNESS instrument applies the pressure of 12kPa on composite sample;
6) the PERSPIRATION COLOR FASTNESS instrument is put into to preset temperature be 37 ℃ ± 1 ℃ baking oven, kept 4 hours;
7) composite sample is taken off from the PERSPIRATION COLOR FASTNESS instrument, guarantee to only have in the situation that the minor face suture partly contacts, at the air drying that is no more than 60 ℃;
8) after the drying, composite sample is placed on 20 ℃ ± 2 ℃ of temperature, under the standard atmosphere condition of relative humidity 65 ± 4%, damping at least 4 hours;
9) adopt standard variable color ash card, standard staining ash card respectively test to be evaluated in the variable color of sample to be tested and the staining of adjacent fabric.
Four, the test result of suggestion is estimated foundation:
The sample to be tested variable color reach 4 grades on GB/T250 standard variable color ash card or more than, it is qualified to be judged to be; Below 4 grades, then be judged to be defective;
Adjacent fabric staining reach GB/T251 standard staining ash card 4-5 level or more than, it is qualified to be judged to be; Below the 4-5 level, then be judged to be defective.
Five, test result is as follows:
Sample to be tested variable color: 3-4 level;
Adjacent fabric staining: triacetate: 4
Cotton: 2-3
Nylon: 3
Terylene: 4-5
Acrylic fibers: 4
Wool: 3-4
Conclusion is: defective.
The artificial children's salivary that disposes among the present invention should be avoided solar radiation, and suggestion is kept in the brown bottle, and should check its pH value before using artificial children's salivary at every turn,, then abandons not 6.8 ± 0.1 such as the pH value; And the artificial saliva term of validity that configures was two weeks, expiredly then abandoned.
Damping environment of the present invention is: 20 ℃ ± 2 ℃ of temperature, relative humidity 65 ± 4%; Test environment is: 37 ℃ ± 1 ℃ of test oven environment temperature.
This method is estimated textile by test grades owing to soaked the variable color that brought and staining to the risk of other textiles by children's salivary, it is applicable to all textiles or textile product, is specially adapted to textile or textile product that children below 36 months use.
The present invention is not subjected to the restriction of above-mentioned embodiment, and other any do not deviate from change, the modification done under Spirit Essence of the present invention and the principle, substitutes, combination, simplify, and all should be the substitute mode of equivalence, is included within protection scope of the present invention.
Claims (8)
1. the method for testing of the textile colour fastness of anti-the saliva is characterized in that, may further comprise the steps:
1) configuration artificial saliva;
2) cutting sample to be tested is fitted sample to be tested and multifilament adjacent fabric, forms composite sample;
3) take by weighing the artificial saliva that disposes in an amount of step 1), add in the double dish, with step 2) in composite sample be soaked in the artificial saliva fully;
4) after immersion is finished, composite sample is taken out, and be placed on the PERSPIRATION COLOR FASTNESS instrument, by the weight of PERSPIRATION COLOR FASTNESS instrument composite sample is exerted pressure;
5) the PERSPIRATION COLOR FASTNESS instrument is put into to preset temperature be 37 ℃ ± 1 ℃ baking oven;
6) composite sample is taken off from the PERSPIRATION COLOR FASTNESS instrument, at the air drying that is no more than 60 ℃;
7) after the drying, composite sample is placed on 20 ℃ ± 2 ℃ of temperature, under the standard atmosphere condition of relative humidity 65 ± 4%, damping at least 4 hours;
8) adopt standard variable color ash card, standard staining ash card respectively test to be evaluated in the variable color of sample to be tested and the staining of adjacent fabric.
2. method of testing as claimed in claim 1; it is characterized in that: the configuration step of artificial saliva is in the described step 1); 0.75g potassium chloride, 0.33g sodium chloride and 0.53g sal tartari are added in the 1L beaker; add again three grades of water of about 900ml; then add 0.17g magnesium chloride hexahydrate, 0.15g calcium chloride dihydrate and 0.76g hydrogen phosphate dihydrate dipotassium; stir until fully dissolving; adjust the pH value of mixed solution with 1% hydrochloric acid; the pH value of guaranteeing mixed solution is 6.8 ± 0.1, is settled to 1L with three grades of water at last.
3. method of testing as claimed in claim 1, it is characterized in that: described step 2), sample to be tested is cut into 40mm * 100mm, sample to be tested and multifilament adjacent fabric is sew on along minor face close, and forms composite sample.
4. method of testing as claimed in claim 1, it is characterized in that: in the described step 3), the weight ratio of artificial saliva and composite sample is 100:1, adopts the extruding of resin plate or glass plate that composite sample is soaked in the artificial saliva fully, soaks action and keeps 30min ± 2min.
5. method of testing as claimed in claim 1 is characterized in that: between described step 3) and the step 4), the step that adopts glass bar that the composite sample that takes out is pushed is arranged, so that the composite sample liquid carrying rate is 100% ± 5%.
6. method of testing as claimed in claim 1, it is characterized in that: in the described step 4), composite sample is placed on resin plate or the glass plate, resin plate or glass plate are placed on the PERSPIRATION COLOR FASTNESS instrument, the pressurization weight of PERSPIRATION COLOR FASTNESS instrument applies the pressure of 12kPa to composite sample.
7. method of testing as claimed in claim 1 is characterized in that: in the described step 5), the PERSPIRATION COLOR FASTNESS instrument is put into baking oven and was kept 4 hours.
8. such as each described method of testing among the claim 1-7, it is characterized in that: described PERSPIRATION COLOR FASTNESS instrument comprises stainless steel mounting, weight and resin plate or glass plate.
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| CN201210579989.7A CN103033480B (en) | 2012-12-27 | 2012-12-27 | Testing method for color fastness to saliva of textile |
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| CN103033480B CN103033480B (en) | 2014-11-19 |
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| CN103868861A (en) * | 2014-03-25 | 2014-06-18 | 中国烟草总公司郑州烟草研究院 | Method for measuring color fastness to saliva of tipping paper for cigarette |
| CN104020104A (en) * | 2014-06-23 | 2014-09-03 | 中国烟草总公司郑州烟草研究院 | Automatic load bearing contact device for testing color fastness based on hot air circulation system temperature control |
| CN105043979A (en) * | 2015-06-09 | 2015-11-11 | 广东溢达纺织有限公司 | Method for testing industrial water washing color fastness of textile |
| CN105527143A (en) * | 2015-12-31 | 2016-04-27 | 宁波纺织仪器厂 | An infiltrating instrument for textile samples for testing color fastness to perspiration, water and sea water |
| CN106198380A (en) * | 2016-07-20 | 2016-12-07 | 清远市通用皮具配件有限公司 | The detection device of a kind of slide fastener color fastness and detection method thereof |
| CN107247027A (en) * | 2017-04-28 | 2017-10-13 | 芜湖富春染织股份有限公司 | Dyed yarn water colour fastness and sweat color fastness detection method |
| CN107561005A (en) * | 2017-09-28 | 2018-01-09 | 鹤山市鸿新经编厂有限公司 | A kind of tight device of textile pressing color fastness test clamp |
| CN109270254A (en) * | 2018-11-27 | 2019-01-25 | 中山中测纺织产业技术研究中心 | Method for detecting color fastness of textiles to perspiration and friction |
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| CN111398147A (en) * | 2020-04-15 | 2020-07-10 | 高铁检测仪器（东莞）有限公司 | Test method for color fastness of leather to saliva |
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| CN113092347A (en) * | 2021-03-01 | 2021-07-09 | 雅戈尔服装制造有限公司 | Method for testing color fastness of trademark for ready-made wash-and-wear shirt |
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