CN103027076B - 10% boric acid cockroach gel and preparation method thereof - Google Patents
10% boric acid cockroach gel and preparation method thereof Download PDFInfo
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- CN103027076B CN103027076B CN201210525557.8A CN201210525557A CN103027076B CN 103027076 B CN103027076 B CN 103027076B CN 201210525557 A CN201210525557 A CN 201210525557A CN 103027076 B CN103027076 B CN 103027076B
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- boric acid
- propolis
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- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 title claims abstract description 70
- 239000004327 boric acid Substances 0.000 title claims abstract description 70
- 238000002360 preparation method Methods 0.000 title claims abstract description 35
- 241001674044 Blattodea Species 0.000 title abstract description 20
- 238000001879 gelation Methods 0.000 title 1
- 235000013312 flour Nutrition 0.000 claims abstract description 69
- 241000241413 Propolis Species 0.000 claims abstract description 45
- 229940069949 propolis Drugs 0.000 claims abstract description 45
- 238000003756 stirring Methods 0.000 claims abstract description 43
- 235000014121 butter Nutrition 0.000 claims abstract description 41
- 240000008042 Zea mays Species 0.000 claims abstract description 40
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 claims abstract description 40
- 235000002017 Zea mays subsp mays Nutrition 0.000 claims abstract description 40
- 235000005822 corn Nutrition 0.000 claims abstract description 40
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 25
- 238000000465 moulding Methods 0.000 claims abstract description 5
- 239000002674 ointment Substances 0.000 claims description 8
- 239000003292 glue Substances 0.000 claims description 7
- 238000001035 drying Methods 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 5
- 239000000853 adhesive Substances 0.000 claims description 4
- 230000001070 adhesive effect Effects 0.000 claims description 4
- 239000004615 ingredient Substances 0.000 claims description 3
- 238000005303 weighing Methods 0.000 claims description 2
- 235000013305 food Nutrition 0.000 abstract description 9
- 210000002784 stomach Anatomy 0.000 abstract description 3
- 230000001580 bacterial effect Effects 0.000 abstract description 2
- 235000013339 cereals Nutrition 0.000 abstract description 2
- 239000000645 desinfectant Substances 0.000 abstract description 2
- 238000000855 fermentation Methods 0.000 abstract description 2
- 230000004151 fermentation Effects 0.000 abstract description 2
- 150000004676 glycans Chemical class 0.000 abstract description 2
- 239000003966 growth inhibitor Substances 0.000 abstract description 2
- 229920001282 polysaccharide Polymers 0.000 abstract description 2
- 239000005017 polysaccharide Substances 0.000 abstract description 2
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- 230000002335 preservative effect Effects 0.000 abstract description 2
- 239000000126 substance Substances 0.000 abstract description 2
- 241000209140 Triticum Species 0.000 abstract 2
- 235000021307 Triticum Nutrition 0.000 abstract 2
- 239000004480 active ingredient Substances 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 235000011837 pasties Nutrition 0.000 abstract 1
- 231100000572 poisoning Toxicity 0.000 abstract 1
- 230000000607 poisoning effect Effects 0.000 abstract 1
- 238000007493 shaping process Methods 0.000 abstract 1
- 241000231739 Rutilus rutilus Species 0.000 description 6
- 201000010099 disease Diseases 0.000 description 6
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 6
- 230000002147 killing effect Effects 0.000 description 6
- 231100000225 lethality Toxicity 0.000 description 4
- 239000003814 drug Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 230000002265 prevention Effects 0.000 description 3
- 231100000419 toxicity Toxicity 0.000 description 3
- 230000001988 toxicity Effects 0.000 description 3
- 241000238631 Hexapoda Species 0.000 description 2
- 230000000857 drug effect Effects 0.000 description 2
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- 241000894007 species Species 0.000 description 2
- IQVNEKKDSLOHHK-FNCQTZNRSA-N (E,E)-hydramethylnon Chemical compound N1CC(C)(C)CNC1=NN=C(/C=C/C=1C=CC(=CC=1)C(F)(F)F)\C=C\C1=CC=C(C(F)(F)F)C=C1 IQVNEKKDSLOHHK-FNCQTZNRSA-N 0.000 description 1
- 235000007516 Chrysanthemum Nutrition 0.000 description 1
- 244000189548 Chrysanthemum x morifolium Species 0.000 description 1
- 241000254173 Coleoptera Species 0.000 description 1
- 229920002261 Corn starch Polymers 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 244000241257 Cucumis melo Species 0.000 description 1
- 235000015510 Cucumis melo subsp melo Nutrition 0.000 description 1
- DNXHEGUUPJUMQT-CBZIJGRNSA-N Estrone Chemical compound OC1=CC=C2[C@H]3CC[C@](C)(C(CC4)=O)[C@@H]4[C@@H]3CCC2=C1 DNXHEGUUPJUMQT-CBZIJGRNSA-N 0.000 description 1
- 239000005949 Malathion Substances 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 241000269799 Perca fluviatilis Species 0.000 description 1
- 241000700605 Viruses Species 0.000 description 1
- FJJCIZWZNKZHII-UHFFFAOYSA-N [4,6-bis(cyanoamino)-1,3,5-triazin-2-yl]cyanamide Chemical compound N#CNC1=NC(NC#N)=NC(NC#N)=N1 FJJCIZWZNKZHII-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 235000010338 boric acid Nutrition 0.000 description 1
- 235000008429 bread Nutrition 0.000 description 1
- 235000012970 cakes Nutrition 0.000 description 1
- 210000003555 cloaca Anatomy 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 239000008120 corn starch Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- JXSJBGJIGXNWCI-UHFFFAOYSA-N diethyl 2-[(dimethoxyphosphorothioyl)thio]succinate Chemical compound CCOC(=O)CC(SP(=S)(OC)OC)C(=O)OCC JXSJBGJIGXNWCI-UHFFFAOYSA-N 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 210000003608 fece Anatomy 0.000 description 1
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- 239000008187 granular material Substances 0.000 description 1
- 235000003642 hunger Nutrition 0.000 description 1
- 239000010985 leather Substances 0.000 description 1
- 229960000453 malathion Drugs 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
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- 235000009566 rice Nutrition 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 235000015096 spirit Nutrition 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- CCEKAJIANROZEO-UHFFFAOYSA-N sulfluramid Chemical compound CCNS(=O)(=O)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F CCEKAJIANROZEO-UHFFFAOYSA-N 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention relates to a 10% boric acid cockroach gel and a preparation method thereof. The 10% boric acid cockroach gel takes boric acid as an active ingredient, wheat flour and/or corn flour as a skeleton and propolis and butter as baits; the formula comprises 9.5-11.5% of boric acid, 4-6% of propolis, 0.5-1.5% of butter, 57-68% of wheat flour and/or corn flour, 18-24% of brown sugar and a right amount of water. The preparation method comprises the following steps: proportioning, mixing, stirring, shaping, standing and molding. The product provided by the invention has stable physical and chemical performance, is highly attractive to cockroaches and is a viscous pasty stomach poisoning preparation. The butter and the propolis are highly attractive, and polysaccharide formed by the fermentation of the corn flour can also have high attraction power; the viscous paste (in a semisolid state) conforms to feeding habits of cockroaches; all the components except the boric acid are edible grains and foods; and the boric acid is a bacterial growth inhibitor and often serves as weakly-acidic disinfectant and preservative. Thus, the product is very safe for non-target organisms.
Description
Technical field
The invention belongs to the daily hygiene articles for use, particularly relate to a kind of boric acid cockroach-killing gel bait, relate to the preparation method of this boric acid cockroach-killing gel bait simultaneously.
Background technology
Cockroach is a kind of place perch of liking selecting warm, moist, food in abundance and many gaps, and happiness secretly keeps in dark place, hide by day and come out at night, and the insect of infringement huge numbers of families health, boring.Cockroach is omnivorous insect, and food species is very extensive.Varieties of food items, comprise bread, rice, cake, meat and vegetables delicatessen, melon and fruit and beverage etc., especially fragrant, sweet, the oily flour-made food of happiness food.Except liking varieties of food items, cockroach also often stings his article of Shiqi, and such as locating at house, warehouse, storeroom etc., they can gnaw cotton wool goods, leather and fur products, paper, books, soap etc.In places such as outdoor rubbish heap, cloaca and lavatories, they take again corrupt organic matter as food, even the dead animal that bites.Just because of cockroach, creep everywhere, nothing institute does not eat, and they are infected with and have swallowed a lot of pathogene, add the bad habit that they draw while eating, and become the mechanical transmitter of some pathogene.
The medicine of killing cockroach has a lot, as (1) class of tagging: 1. chrysanthemum ester class spray, 2. Kothrin pulvis, 0.09% synergy hundred worm spirits, 5% malathion, 1% unden pulvis etc., roach smog 3. goes out; (2) stomach toxicity is killed class: roach granule, 2. gel bait 1. go out.Some medicine is used for a long time, and cockroach has produced extremely strong pesticide resistance to it, and roach weak effect or substantially invalid goes out.Also have to adopt the biological roach mode of going out, 1. the main inadaptability difference characteristics of utilizing different biological (species) reach the roach purpose of going out, and cause the cockroach death of killing each other and go on a hunger strike, as product " flat No. 1 of dung beetle "; 2. utilize cockroach virus to manufacture cockroach pestilence and carry out killing cockroach, as product " pathogenicity island ".But the use of these products often has certain limitation.
In the medicine of numerous killing cockroachs, gel bait is leading, and killing effect is good, easy to use.And drug effect be take sulfluramid, hydramethylnon and boric acid as best, particularly boric acid, minimum to people's toxicity.Existing a kind of 8% boric acid cockroach-killing gel bait, take boric acid as effective ingredient, but allure is not strong, and trapping effect is unsatisfactory.
Summary of the invention
The deficiency that the present invention exists for solving above-mentioned prior art, proposed a kind of boric acid cockroach-killing gel bait and preparation method thereof.Its scientific formulation is reasonable, and the preparation method is concisely convenient, and product has extremely strong allure to cockroach, and the roach that goes out is satisfactory for result.
The technical scheme that this bright technical solution problem is taked is, a kind of boric acid cockroach-killing gel bait, take boric acid as effective ingredient, take flour and/or corn flour as skeleton, take propolis and butter as bait, and the each component mass fraction is as follows: boric acid 9.5 ~ 11.5%, propolis 4 ~ 6%, butter 0.5 ~ 1.5%, flour and/or corn flour 57 ~ 68%, brown sugar 18 ~ 24%, and separately add suitable quantity of water.
As a kind of preferred, the each component mass fraction is as follows: boric acid 10%, and propolis 5%, butter 1%, flour 33%, corn flour 30%, brown sugar 21%, and separately add suitable quantity of water.
As a kind of preferred, the each component mass fraction is as follows: boric acid 10%, and propolis 5%, butter 1%, corn flour 63%, brown sugar 21%, and separately add suitable quantity of water.
A kind of preparation method of described boric acid cockroach-killing gel bait, comprise the steps:
(1) fill a prescription: in mass fraction, boric acid 9.5 ~ 11.5%, propolis 4 ~ 6%, butter 0.5 ~ 1.5%, flour and/or corn flour 57 ~ 68%, brown sugar 18 ~ 24%; Each component is by the formula weighing;
(2) mix: will drop into and stir cabin by the load weighted brown sugar of formula, boric acid, flour and/or corn flour, and close and stir the cabin lid, and open agitator, and stir, and form dry preparation;
(3) stir: will slowly add the stirring cabin by the load weighted propolis of formula while stirring, and add suitable quantity of water, and fully stir, and make propolis be attached to equably the dry preparation surface;
(4) figuration: add while stirring by the load weighted butter of formula, and add suitable quantity of water, fully stir, form the viscosity ointment preparation;
(5) standing: as to open and stir the cabin lid, make the standing 16-22 hour of preparation;
(6) moulding: i.e. packing, ointment preparation is sub-packed in the cassette holder by the flat bait box, build lid, and at the non-drying glue layer of cassette holder bottom adhesive band release liners.
In preparation process, the water yield added during stirring should become paste fully to stir rear product, and viscosity paste semi-solid state is standard, 9.5 ~ 10.5% of the gross mass that common the added water yield is boric acid, propolis, butter, flour, corn flour and brown sugar.
Product physical and chemical performance of the present invention is stable, and cockroach is had to extremely strong allure, is a kind of viscosity paste stomach toxicity preparation.Butter and propolis have very strong allure, and the polysaccharide formed after fermentation of corn starch also has stronger allure; Viscosity paste (semi-solid state) meets the feeding habit of cockroach; Except boric acid, each component used is all edible grain and food, and boric acid is a kind of bacterial growth inhibitor, is commonly used for faintly acid disinfectant and preservative, so product is very safe to non-target biology.In addition as the glue bait, particularly bottom is provided with the non-drying glue layer with release liners, during use, release liners on the non-drying glue layer of bottom is torn, open the lid of bait box, then it is sticked on the wall of cockroach activity, the hidden place such as in kitchen cabinet between the downside of the furniture back side, electrical equipment, kitchen, being killed of cockroach food.Good killing effect is arranged, again sanitation and hygiene.
Take according to Zhejiang Center For Disease Control and Prevention and Jiangsu Prov. Disease Preventing and Controlling Center the evidence that Groton bug is tested worm kind, product of the present invention has good drug effect, in Table 1 and table 2.
Table 1 Laboratory efficacy result of the test
| Test mechanism | LT 50 | Lethality |
| Zhejiang Center For Disease Control and Prevention | 1.65 d | 100% |
| Jiangsu Prov. Disease Preventing and Controlling Center | 0.96d | 97.80% |
Table 2 simulated field test of pesticide effectiveness result
| Test mechanism | The 24h lethality | The 48h lethality | The 72h lethality |
| Zhejiang Center For Disease Control and Prevention | 100% | 100% | 100% |
| Jiangsu Prov. Disease Preventing and Controlling Center | 84% | 96% | 99% |
The accompanying drawing explanation
Fig. 1 is preparation method's process flow diagram of the present invention.
Embodiment
Embodiment 1: boric acid cockroach-killing gel bait formula 1: in mass fraction, and boric acid 10%, propolis 5%, butter 1%, flour 33%, corn flour 30%, brown sugar 21%; And separately add approximately 10% the water of the gross mass of boric acid, propolis, butter, flour, corn flour and brown sugar.
Embodiment 2: boric acid cockroach-killing gel bait formula 2: in mass fraction, and boric acid 10.2%, propolis 5%, butter 1%, corn flour 63%, brown sugar 21%; And separately add approximately 10% the water of the gross mass of boric acid, propolis, butter, corn flour and brown sugar.
Embodiment 3: boric acid cockroach-killing gel bait formula 3: in mass fraction, and boric acid 9.8%, propolis 4%, butter 1.2%, flour 40%, corn flour 21%, brown sugar 24%; And separately add approximately 9.8% the water of the gross mass of boric acid, propolis, butter, flour, corn flour and brown sugar.
Embodiment 4: boric acid cockroach-killing gel bait formula 4: in mass fraction, and boric acid 9.5%, propolis 6%, butter 0.5%, flour 20%, corn flour 42%, brown sugar 22%; And separately add approximately 9.5% the water of the gross mass of boric acid, propolis, butter, flour, corn flour and brown sugar.
Embodiment 5: boric acid cockroach-killing gel bait formula 5: in mass fraction, and boric acid 10.5%, propolis 4.5%, butter 1%, corn flour 64%, brown sugar 20%; And separately add approximately 10.5% the water of the gross mass of boric acid, propolis, butter, corn flour and brown sugar.
Embodiment 6: boric acid cockroach-killing gel bait formula 6: in mass fraction, and boric acid 11%, propolis 6%, butter 1%, flour 28%, corn flour 36%, brown sugar 18%; And separately add approximately 10% the water of the gross mass of boric acid, propolis, butter, flour, corn flour and brown sugar.
Embodiment 7: boric acid cockroach-killing gel bait formula 7: in mass fraction, and boric acid 11.5%, propolis 4%, butter 1.5%, flour 18%, corn flour 41%, brown sugar 24%; And separately add approximately 9.5% the water of the gross mass of boric acid, propolis, butter, flour, corn flour and brown sugar.
Embodiment 8: boric acid cockroach-killing gel bait formula 8: in mass fraction, and boric acid 10.2%, propolis 4.8%, butter 1%, flour 30%, corn flour 32%, brown sugar 22%; And separately add approximately 9.6% the water of the gross mass of boric acid, propolis, butter, flour, corn flour and brown sugar.
Embodiment 9: the preparation method 1 of boric acid cockroach-killing gel bait:
(1) fill a prescription: according to the described formula of embodiment 1, in mass fraction, take boric acid 10%, propolis 5%, butter 1%, flour 33%, corn flour 30% and brown sugar 21%;
(2) mix: will drop into and stir cabin by the load weighted flour of formula, corn flour, brown sugar and boric acid, and close and stir the cabin lid, and open agitator, and stir, and form dry preparation;
(3) stir: will slowly add the stirring cabin by the load weighted propolis of formula while stirring, and add 8% water of the gross mass of boric acid, propolis, butter, flour, corn flour and brown sugar, and fully stir, and make propolis be attached to equably the dry preparation surface;
(4) figuration: add while stirring by the load weighted butter of formula, and add 2% water of the gross mass of boric acid, propolis, butter, flour, corn flour and brown sugar, fully stir, form the viscosity ointment preparation;
(5) standing: as to open and stir the cabin lid, make preparation standing over night (approximately 20 hours);
(6) moulding: ointment preparation is sub-packed in the cassette holder by the flat bait box, builds lid, and at the non-drying glue layer of cassette holder bottom adhesive band release liners.
Embodiment 10: the preparation method 2 of boric acid cockroach-killing gel bait:
(1) fill a prescription: according to the described formula of embodiment 2, in mass fraction, take boric acid 10%, propolis 5%, butter 1%, corn flour 63% and brown sugar 21%.
(2) mix: will drop into and stir cabin by the load weighted corn flour of formula, brown sugar and boric acid, and close and stir the cabin lid, and open agitator, and stir, and form dry preparation;
(3) stir: will slowly add the stirring cabin by the load weighted propolis of formula while stirring, and add 8.5% water of the gross mass of boric acid, propolis, butter, corn flour and brown sugar, and fully stir, and make propolis be attached to equably the dry preparation surface;
(4) figuration: add while stirring by the load weighted butter of formula, and add 1.5% water of the gross mass of boric acid, propolis, butter, corn flour and brown sugar, fully stir, form the viscosity ointment preparation;
(5) standing: as to open and stir the cabin lid, make preparation standing over night (approximately 18 hours);
(6) moulding: ointment preparation is sub-packed in the cassette holder by the flat bait box, builds lid, and at the non-drying glue layer of cassette holder bottom adhesive band release liners.
Claims (4)
1. a boric acid cockroach-killing gel bait, take boric acid as effective ingredient, take flour and/or corn flour as skeleton, it is characterized in that, take propolis and butter as bait, and the each component mass fraction is as follows: boric acid 9.5 ~ 11.5%, propolis 4 ~ 6%, butter 0.5 ~ 1.5%, flour and/or corn flour 57 ~ 68%, brown sugar 18 ~ 24%, and separately add suitable quantity of water.
2. boric acid cockroach-killing gel bait according to claim 1, is characterized in that, the each component mass fraction is as follows: boric acid 10%, and propolis 5%, butter 1%, flour 33%, corn flour 30%, brown sugar 21%, and separately add suitable quantity of water.
3. boric acid cockroach-killing gel bait according to claim 1, is characterized in that, the each component mass fraction is as follows: boric acid 10%, and propolis 5%, butter 1%, corn flour 63%, brown sugar 21%, and separately add suitable quantity of water.
4. the preparation method of a boric acid cockroach-killing gel bait according to claim 1, is characterized in that, comprises the steps:
(1) fill a prescription: in mass fraction, boric acid 9.5 ~ 11.5%, propolis 4 ~ 6%, butter 0.5 ~ 1.5%, flour and/or corn flour 57 ~ 68%, brown sugar 18 ~ 24%; Each component is by the formula weighing;
(2) mix: will drop into and stir cabin by the load weighted brown sugar of formula, boric acid, flour and/or corn flour, and close and stir the cabin lid, and open agitator, and stir, and form dry preparation;
(3) stir: will slowly add the stirring cabin by the load weighted propolis of formula while stirring, and add suitable quantity of water, and fully stir, and make propolis be attached to equably the dry preparation surface;
(4) figuration: add while stirring by the load weighted butter of formula, and add suitable quantity of water, fully stir, form the viscosity ointment preparation;
(5) standing: as to open and stir the cabin lid, make the standing 16-22 hour of preparation;
(6) moulding: ointment preparation is sub-packed in the cassette holder by the flat bait box, builds lid, and at the non-drying glue layer of cassette holder bottom adhesive band release liners.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201210525557.8A CN103027076B (en) | 2012-12-10 | 2012-12-10 | 10% boric acid cockroach gel and preparation method thereof |
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| CN201210525557.8A CN103027076B (en) | 2012-12-10 | 2012-12-10 | 10% boric acid cockroach gel and preparation method thereof |
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| CN103315000A (en) * | 2013-06-19 | 2013-09-25 | 海宁市祝场卫生用品厂 | Preparation method of cockroach killer |
| CN103734186B (en) * | 2013-12-23 | 2015-11-04 | 广西科技大学 | A kind of cockroach killer |
| CN105340976B (en) * | 2015-12-15 | 2018-07-27 | 成都嘉洁事生物科技有限公司 | A kind of cockroach attractant and preparation method thereof and cockroach killing chemicals obtained |
| CN107467090A (en) * | 2017-08-29 | 2017-12-15 | 广西贵港市恒桥米业有限公司 | A kind of ivory scented rice insect attractant and preparation method thereof |
| CN111296478A (en) * | 2018-12-10 | 2020-06-19 | 江苏功成生物科技有限公司 | Boric acid-containing insecticidal composition and application thereof |
| CN111226971A (en) * | 2020-03-03 | 2020-06-05 | 中山榄菊日化实业有限公司 | Combined cockroach killing bait and preparation method and use method thereof |
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| CN1475120A (en) * | 2003-06-30 | 2004-02-18 | 华南农业大学 | Preventing and controlling agent for cockroach |
| US20090214462A1 (en) * | 2004-01-12 | 2009-08-27 | Sondlin Technology Corp. | Cockcroach jelly bait |
| WO2007010095A2 (en) * | 2006-10-18 | 2007-01-25 | Oy Finnpesticides Ltd | Bait composition for cockroaches and ants |
| CN100998345B (en) * | 2007-01-10 | 2010-05-26 | 沈宏良 | Glue bait for trapping and killing cockroach and its preparing method |
| CN101422173A (en) * | 2007-10-29 | 2009-05-06 | 沈阳恒生清洗服务有限公司 | Gel bait capable of trapping and killing cockroach |
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