CN103015160A - Method for producing bacteriostatic sole, lining or insole by using bacteriostatic agent - Google Patents
Method for producing bacteriostatic sole, lining or insole by using bacteriostatic agent Download PDFInfo
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- CN103015160A CN103015160A CN201210551269XA CN201210551269A CN103015160A CN 103015160 A CN103015160 A CN 103015160A CN 201210551269X A CN201210551269X A CN 201210551269XA CN 201210551269 A CN201210551269 A CN 201210551269A CN 103015160 A CN103015160 A CN 103015160A
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Abstract
The invention discloses a method for producing a bacteriostatic sole, lining or insole by using bacteriostatic agent. The method comprises the following steps: (1) the bacteriostatic agent is prepared to bacteriostatic agent water solution, and is selected from siberian solomonseal rhizome extract, scutellaria baicalensis extract, forsythia suspensa extract, honeySuchle flowers extract, coptis chinensis extract, radix isatidis extract and pepper extract or a mixture of several thereof; (2) the bacteriostatic agent water solution permeates into the sole, lining or insole; (3) the irradiation grafting is implemented; and (4) the moisture is dried to obtain the bacteriostatic sole, lining or insole. The method adopts the bacteriostatic agent which is harmless to people; the raw materials are cheap, easy to get, and easy to be degraded; and the environmental pollution from heavy metals and substances toxic for the people is avoided. The grafting process of the bacteriostatic agent adopts the mode of grafting after radiating electronic beams or plasma bodies in the sole, lining or the insole, so that the processing method is easy and feasible, no chemical pollution is generated, and energy conservation and environmental friendliness are achieved.
Description
Technical field
The present invention relates to antibacterial textiles, refer to that particularly a kind of bacteriostatic agent that utilizes makes antibacterial sole, footwear inside or the method for shoe-pad.
Background technology
China is that footwear are already made big country, also is the consumption big country of article of footwear.Yet in China, just have a people to suffer from pedopathy in per two people, adult's morbidity ratio is especially up to 75%, and the pedopathy above 60% is fungal infection, wherein the incidence of disease of tinea pedis (being commonly called as beriberi) is 45.2%, and the beriberi incidence of disease of southern china some areas can reach 50 ~ 60%.
China's beriberi incidence of disease is high, and main cause is that the shoes internal environment is conducive to microbial growth, and therefore, people require that generally footwear are carried out antibacterial and deodouring and process.
The bacteriostatic agent kind is a lot, substantially can be divided into following a few class: 1, organic heavy metal compound, as: beta-hydroxy quinolinone, 3,5-dimethylphenyl tin acetic acid esters, phenyl two hot mercury, tributyl lead acetate and alkanoic acid zinc etc.; 2, some dyestuffs or auxiliary agent, as: triphenylmethane dye, TMM-THPC etc.; 3, the antibiotic such as some organic titaniums, organo-aluminium, organic zirconate and tetracycline share; 4, aromatic series halogen compounds class, as: alpha-bromo-cinnamaldehyde, 2,4,4 '-three chloro-, 2 ' dihydroxy diphenyl ether, 5-chloro-2-(2,4-dichlorophenoxy) phenol etc.; 5, organosilicon quaternary ammonium salt compounds.Although above-mentioned bacteriostatic agent can make textiles have antimicrobial performance,, the bacteriostatic agent that has is simultaneously harmful.
Therefore, selecting the cheap bacteriostatic agent to health is an important selection in the antibacterial field of shoemaking.
Summary of the invention
The present invention is directed to the deficiencies in the prior art, provide a kind of utilize bacteriostatic agent make antibacterial sole, footwear inside, the method for shoe-pad.
The present invention utilizes bacteriostatic agent to make antibacterial sole, footwear inside or the method for shoe-pad, may further comprise the steps:
1) bacteriostatic agent is mixed with the bacteriostatic agent aqueous solution; Described bacteriostatic agent is selected from one or more the mixture in Rhizoma Polygonati extract, Baical Skullcap root P.E, forsythia suspense extraction, Honegsukle flower P.E, coptis extract, isatis root extract, the pepper extract;
2), make the bacteriostatic agent aqueous solution be penetrated into sole, footwear inside or in the shoe-pad inside with bacteriostatic agent aqueous solution soaking sole, footwear or shoe-pad, according to the sole of per kilogram, footwear inside or shoe-pad add 10 ~ 30 gram bacteriostatic agents;
3) to the sole that adopts bacteriostatic agent to process, footwear inside or shoe-pad carry out irradiation grafting;
4) at the bottom of the shoe drying, footwear inside or the moisture in the shoe-pad, namely get antibacterial sole, footwear inside or shoe-pad.
In the step 1) of the present invention, described Rhizoma Polygonati extract, Baical Skullcap root P.E, forsythia suspense extraction, Honegsukle flower P.E, coptis extract, isatis root extract, pepper extract are the powder by dry gained after extracting.
In the step 3) of the present invention, adopt sole that bacteriostatic agent processed, footwear inside or shoe-pad passes through electron beam or plasma radiation grafting, the energy of the generation of the accelerator that irradiation is used is 5 ~ 10Mev, and radiation dose rate is 80 ~ 100Gy.
Used Rhizoma Polygonati extract, Baical Skullcap root P.E, forsythia suspense extraction, Honegsukle flower P.E, coptis extract, isatis root extract, the pepper extract of the present invention is the natural plants bacteriostatic agent, the product that can buy for market.
Studies show that: the Rhizoma Polygonati extract aqueous solution of 1:320 concentration has inhibitory action to typhoid bacillus, staphylococcus aureus, acid-fast bacilli, and the 2% Rhizoma Polygonati extract aqueous solution has in various degree inhibitory action to common pathomycete in sabouraud culture medium.
Root of large-flowered skullcap decocting liquid, test tube slant method are tested 4% control of the concentration dog denticle born of the same parents bacterium and trichophyton, 8% control of the concentration oidium schoenleinii, the mutation of 10% control of the concentration oidium schoenleinii Mongolia, 15% control of the concentration homocentricity trichophyta and rust trichophyta.Root of large-flowered skullcap water logging agent 1:3 concentration is in vitro to trichophyton, Trichophyton concentricum, and oidium schoenleinii, Microsporon audouini, wool sample microspore tinea bacterium, epidermophyton rubrum, K, W, family name Epidermophyton, star nocardia etc. have in various degree bacteriostasis.
The capsule of weeping forsythia all has inhibitory action to multiple Grain-positive and negative bacteria. and its concentrated decoction suppresses typhoid bacillus, paratyphosum Bacterium, Escherichia coli, shigella dysenteriae, corynebacterium diphtheriae and comma bacillus, staphylococcus, streptococcus etc. external.There is report to point out that forsythol is the antibiotic active ingredient of the capsule of weeping forsythia. forsythol Mlc to staphylococcus aureus in test tube is 1:5120; Be 1:1280 to shigella dysenteriae; Be 1:640 to corynebacterium diphtheriae and paratyphoid (first) bacillus.Capsule of weeping forsythia water logging agent (1:5) has some inhibitory action to star-shaped nocardia in vitro.
Honeysuckle all has certain inhibitory action to various pathogens such as staphylococcus aureus, hemolytic streptococcus, Escherichia coli, shigella dysenteriae, comma bacillus, typhoid bacillus, paratyphosum Bacterium etc.Honeysuckle is to Salmonella, particularly the inhibitory action of typhoid bacillus and hemolytic streptococcus is like surpassing the capsule of weeping forsythia, inhibition to shigella dysenteriae, staphylococcus aureus is then seemingly better with the capsule of weeping forsythia. and the two unites use, there is no synergy in vitro, with the compound that the coptis, the root of large-flowered skullcap form, In Vitro Bacteriostasis is strong during than the alone capsule of weeping forsythia.
The coptis all has certain inhibitory action to staphylococcus aureus, hemolytic streptococcus, pneumococcus, diplococcus meningitidis, shigella dysenteriae, bacillus anthracis etc.
Radix Isatidis has effect to various bacteria.The isatis root extract infusion has inhibitory action to hay bacillus, staphylococcus aureus, sarcine, Escherichia coli, typhoid bacillus, paratyphoid A bacillus, dysentery (will Hayes, Fu Shi) bacillus, bacillus enteritidis etc.
Chinese prickly ash has inhibitory action to corynebacterium diphtheriae, Diplococcus pneumopniae, staphylococcus aureus and some dermatophyte.
Beneficial effect of the present invention is: the present invention adopts the bacteriostatic agent harmless to the people, and raw material is cheap and easy to get, and raw material easily is degraded, and avoids heavy metal and to the pollution of the poisonous material of people to environment.Bacteriostatic agent grafting process adopts electron beam or plasma radiation sole, footwear inside or the mode of shoe-pad and then grafting, and processing method is simple, does not have chemical contamination, energy-conserving and environment-protective.
The specific embodiment
The present invention is described in further detail below in conjunction with specific embodiment.
Embodiment 1
1) Rhizoma Polygonati extract is mixed with the Rhizoma Polygonati extract aqueous solution, used Rhizoma Polygonati extract is the powder by dry gained after extracting;
2) with Rhizoma Polygonati extract aqueous solution soaking sole, the Rhizoma Polygonati extract aqueous solution is penetrated in the sole, according to the sole adding 20 gram Rhizoma Polygonati extracts of per kilogram;
3) sole that adopts Rhizoma Polygonati extract to process is carried out the electron beam irradiation grafting, the energy of the generation of the accelerator that irradiation is used is 5Mev, and radiation dose rate is 100Gy
4) moisture at the bottom of the shoe drying namely gets antibacterial sole.
Made sole has inhibitory action in various degree to staphylococcus aureus, common pathomycete after testing.
Embodiment 2
1) Baical Skullcap root P.E is mixed with the Baical Skullcap root P.E aqueous solution, used Baical Skullcap root P.E is the powder by dry gained after extracting;
2) with Baical Skullcap root P.E aqueous solution soaking footwear inside, make the Baical Skullcap root P.E aqueous solution be penetrated into footwear inside in, add 15 gram Baical Skullcap root P.Es inside according to the footwear of per kilogram;
3) footwear that adopt Baical Skullcap root P.E to process are carried out the electron beam irradiation grafting inside, the energy of the generation of the accelerator that irradiation is used is 6Mev, and radiation dose rate is 80Gy;
4) moisture of shoe drying in inside namely gets antibacterial footwear inside.
Made footwear have inhibitory action in various degree to staphylococcus aureus, common pathomycete inside after testing.
Embodiment 3
1) forsythia suspense extraction is mixed with the forsythia suspense extraction aqueous solution, used forsythia suspense extraction is the powder by dry gained after extracting;
2) with forsythia suspense extraction aqueous solution soaking shoe-pad, the forsythia suspense extraction aqueous solution is penetrated in the shoe-pad, according to the shoe-pad adding 24 gram forsythia suspense extractions of per kilogram;
3) shoe-pad that adopts forsythia suspense extraction to process is carried out the electron beam irradiation grafting, the energy of the generation of the accelerator that irradiation is used is 7Mev, and radiation dose rate is 95Gy;
4) moisture in the drying shoe-pads namely gets antibacterial shoe-pad.
Made shoe-pad has inhibitory action in various degree to staphylococcus aureus, common pathomycete after testing.
Embodiment 4
1) Honegsukle flower P.E is mixed with the Honegsukle flower P.E aqueous solution, used Honegsukle flower P.E is the powder by dry gained after extracting;
2) with Honegsukle flower P.E aqueous solution soaking sole, the Honegsukle flower P.E aqueous solution is penetrated in the sole, according to the sole adding 25 gram Honegsukle flower P.Es of per kilogram;
3) sole that adopts Honegsukle flower P.E to process is carried out the electron beam irradiation grafting, the energy of the generation of the accelerator that irradiation is used is 8Mev, and radiation dose rate is 90Gy;
4) moisture at the bottom of the shoe drying namely gets antibacterial sole.
Made sole has inhibitory action in various degree to staphylococcus aureus, common pathomycete after testing.
Embodiment 5
1) coptis extract is mixed with the coptis extract aqueous solution, used coptis extract is the powder by dry gained after extracting;
2) with coptis extract aqueous solution soaking shoe-pad, the coptis extract aqueous solution is penetrated in the shoe-pad, according to the shoe-pad adding 30 gram coptis extracts of per kilogram;
3) carry out the electron beam irradiation grafting to adopting coptis extract to process shoe-pad, the energy of the generation of the accelerator that irradiation is used is 9Mev, and radiation dose rate is 85Gy;
4) moisture in the drying shoe-pads namely gets antibacterial shoe-pad.
Made shoe-pad has inhibitory action in various degree to staphylococcus aureus, common pathomycete after testing.
Embodiment 6
1) isatis root extract is mixed with the isatis root extract aqueous solution, used isatis root extract is the powder by dry gained after extracting;
2) with isatis root extract aqueous solution soaking footwear inside, make the isatis root extract aqueous solution be penetrated into footwear inside in, add 22 gram isatis root extracts inside according to the footwear of per kilogram;
3) footwear that adopt isatis root extract to process are carried out the electron beam irradiation grafting inside, the energy of the generation of the accelerator that irradiation is used is 10Mev, and radiation dose rate is 80Gy;
4) moisture of shoe drying in inside namely gets antibacterial footwear inside.
Made footwear have inhibitory action in various degree to staphylococcus aureus, common pathomycete inside after testing.
Embodiment 7
1) pepper extract is mixed with the pepper extract aqueous solution, used pepper extract is the powder by dry gained after extracting;
2) with pepper extract aqueous solution soaking footwear inside, make the pepper extract aqueous solution be penetrated into footwear inside in, add 18 gram pepper extracts inside according to the footwear of per kilogram;
3) footwear that adopt pepper extract to process are carried out the electron beam irradiation grafting inside, the energy of the generation of the accelerator that irradiation is used is 10Mev, and radiation dose rate is 80Gy;
4) moisture of shoe drying in inside namely gets antibacterial footwear inside.
Made footwear have in various degree inhibitory action to staphylococcus aureus, dermatophyte inside after testing.
Embodiment 8
1) bacteriostatic agent is mixed with the bacteriostatic agent aqueous solution, used bacteriostatic agent is the mixture of Honegsukle flower P.E and forsythia suspense extraction, and used Honegsukle flower P.E and forsythia suspense extraction are by extracting the powder of rear dry gained;
2) with bacteriostatic agent aqueous solution soaking shoe-pad, the bacteriostatic agent aqueous solution is penetrated in the shoe-pad, according to the shoe-pad adding 10 gram bacteriostatic agents of per kilogram;
3) shoe-pad that adopts bacteriostatic agent to process is carried out the electron beam irradiation grafting, the energy of the generation of the accelerator that irradiation is used is 7Mev, and radiation dose rate is 85Gy;
4) moisture in the drying shoe-pads namely gets antibacterial shoe-pad.
Made shoe-pad has inhibitory action in various degree to staphylococcus aureus, common pathomycete after testing.
Embodiment 9
1) bacteriostatic agent is mixed with the bacteriostatic agent aqueous solution, used bacteriostatic agent is the mixture of Honegsukle flower P.E, coptis extract and Baical Skullcap root P.E, and used Honegsukle flower P.E, coptis extract and Baical Skullcap root P.E are by extracting the powder of rear dry gained;
2) with bacteriostatic agent aqueous solution soaking shoe-pad, the bacteriostatic agent aqueous solution is penetrated in the shoe-pad, according to the shoe-pad adding 12 gram bacteriostatic agents of per kilogram;
3) shoe-pad that adopts bacteriostatic agent to process is carried out the electron beam irradiation grafting, the energy of the generation of the accelerator that irradiation is used is 7Mev, and radiation dose rate is 85Gy;
4) moisture in the drying shoe-pads namely gets antibacterial shoe-pad.
Made shoe-pad has inhibitory action in various degree to staphylococcus aureus, common pathomycete after testing.
Claims (3)
1. one kind is utilized bacteriostatic agent to make antibacterial sole, footwear inside or the method for shoe-pad, it is characterized in that, may further comprise the steps:
1) bacteriostatic agent is mixed with the bacteriostatic agent aqueous solution; Described bacteriostatic agent is selected from one or more the mixture in Rhizoma Polygonati extract, Baical Skullcap root P.E, forsythia suspense extraction, Honegsukle flower P.E, coptis extract, isatis root extract, the pepper extract;
2), make the bacteriostatic agent aqueous solution be penetrated into sole, footwear inside or in the shoe-pad inside with bacteriostatic agent aqueous solution soaking sole, footwear or shoe-pad, according to the sole of per kilogram, footwear inside or shoe-pad add 10 ~ 30 gram bacteriostatic agents;
3) to the sole that adopts bacteriostatic agent to process, footwear inside or shoe-pad carry out irradiation grafting;
4) at the bottom of the shoe drying, footwear inside or the moisture in the shoe-pad, namely get antibacterial sole, footwear inside or shoe-pad.
2. the bacteriostatic agent that utilizes according to claim 1 is made antibacterial sole, footwear inside or the method for shoe-pad, it is characterized in that: in the step 1), described Rhizoma Polygonati extract, Baical Skullcap root P.E, forsythia suspense extraction, Honegsukle flower P.E, coptis extract, isatis root extract, pepper extract are the powder by dry gained after extracting.
3. the bacteriostatic agent that utilizes according to claim 1 is made antibacterial sole, footwear inside or the method for shoe-pad, it is characterized in that: in the step 3), adopt sole that bacteriostatic agent processed, footwear inside or shoe-pad pass through electron beam or plasma radiation grafting, the energy of the generation of the accelerator that irradiation is used is 5 ~ 10Mev, and radiation dose rate is 80 ~ 100Gy.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210551269.XA CN103015160B (en) | 2012-12-18 | 2012-12-18 | Method for producing bacteriostatic sole, lining or insole by using bacteriostatic agent |
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| CN201210551269.XA CN103015160B (en) | 2012-12-18 | 2012-12-18 | Method for producing bacteriostatic sole, lining or insole by using bacteriostatic agent |
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| CN103015160B CN103015160B (en) | 2015-06-03 |
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Cited By (4)
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| CN104358104A (en) * | 2014-11-07 | 2015-02-18 | 江南大学 | Method for preparing antimicrobial textiles by using electronic radiation technology |
| CN107335286A (en) * | 2017-08-08 | 2017-11-10 | 成都漆彩之星环保科技有限公司 | A kind of composite air filter cotton |
| CN108823126A (en) * | 2018-04-12 | 2018-11-16 | 黄山学院 | A kind of rhizoma polygonati endophyte and its application |
| CN110760085A (en) * | 2019-10-15 | 2020-02-07 | 湖州健塑塑业科技有限公司 | Self-purification pipeline and preparation method and application thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104358104A (en) * | 2014-11-07 | 2015-02-18 | 江南大学 | Method for preparing antimicrobial textiles by using electronic radiation technology |
| CN104358104B (en) * | 2014-11-07 | 2016-06-15 | 江南大学 | A kind of method utilizing electron radiation technology to prepare antibacterial fabric |
| CN107335286A (en) * | 2017-08-08 | 2017-11-10 | 成都漆彩之星环保科技有限公司 | A kind of composite air filter cotton |
| CN108823126A (en) * | 2018-04-12 | 2018-11-16 | 黄山学院 | A kind of rhizoma polygonati endophyte and its application |
| CN110760085A (en) * | 2019-10-15 | 2020-02-07 | 湖州健塑塑业科技有限公司 | Self-purification pipeline and preparation method and application thereof |
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| CN103015160B (en) | 2015-06-03 |
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