CN103013291A - Epoxy resin coating adhesive for roasting and curing metal zipper and preparation method thereof - Google Patents
Epoxy resin coating adhesive for roasting and curing metal zipper and preparation method thereof Download PDFInfo
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- CN103013291A CN103013291A CN2012105037709A CN201210503770A CN103013291A CN 103013291 A CN103013291 A CN 103013291A CN 2012105037709 A CN2012105037709 A CN 2012105037709A CN 201210503770 A CN201210503770 A CN 201210503770A CN 103013291 A CN103013291 A CN 103013291A
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Abstract
The invention relates to epoxy resin coating adhesive for roasting and curing a metal zipper and a preparation method thereof. The epoxy resin coating adhesive comprises a component A, a component B and a component C, wherein the component A is a film-forming substance; the component B is curing agent; the component C is mixed solvent. In terms of mass, the A component comprises the following materials in percentage by weight: 63-75% of epoxy resin, 25-37% of solvent; the B component comprises the following materials in percentage by weight: 38-50% of hardening agent, 30-42% of brightening agent, 10% of smoothing agent, 5% of catalyst and 5% of acid-proof antalkaline; the component C comprises the following materials in percentage by weight: 63-75% of dimethylbenzene, 10% of butyl ether, 10-22% of butanol and 5% of butyl ester. During a process of carrying out metal zipper coating, the using mass ratio of the coating adhesive is A:B:C of 1:1:1. The zipper coating has the characteristics such as good transparency, acid and alkali resistance, friction resistance, water resistance, ageing resistance, incapacity of discoloring and staining, and the like after being roasted at a low temperature, so that the quality and the level of the zipper are improved.
Description
Technical field
The present invention relates to the technical field of a kind of baking-curing epoxy resin glue and preparation method thereof, more specifically relate to epoxy resin glue and the production technique thereof of a kind of metal zip fastener protective coating special use.
Background technology
The plain metal slide fastener is generally directly finalized the design behind row's tooth and is become product, and this slide fastener is the oxidation of chain odontogeny and discoloration problem through wash water or after making moist, and greatly reduces the market competitiveness.The key that addresses these problems is application one deck high quality protective coating on the matallic surface layer of slide fastener.Metal zip fastener on the existing domestic market of close examination, also some has been coated with one deck protective coating in the metallic surface, but is limited to quality and the complete processing of coating adhesive, and its protection effect is still relatively poor.
Summary of the invention
The object of the present invention is to provide a kind of baking-curing metal zip fastener epoxy coating glue, after making the zipper metal external coating, transparency is good, salt spray resistance, acid and alkali-resistance, rub resistance, water-fast, ageing-resistant, nondiscoloration, sticking look, and the slide fastener class promotes, and the market competitiveness strengthens.
The technical problem that will solve required for the present invention can be achieved through the following technical solutions:
1. fill a prescription: be comprised of A, B, C three components, it is as shown in the table for each component composition:
Wherein: the Resins, epoxy in the A component is the E-33 bisphenol A epoxide resin; Solvent in the A component is ethylene glycol; Stiffening agent in the B component is the SU of Henan nation liquid sclerotherapy; Brightening agent in the B component is young eastern BL-20 baking vanish brightener; Smooth agent in the B component is young eastern OP-8050 (the COALAR)-general levelling deaeration of A/SL solvent-borne type smooth agent; Siccative in the B component is dibutyl tin laurate; Acid-proof antalkaline in the B component is Tutofusin tris.
2. proportioning:
By mass, proportioning is A: B: C=1: 1: 1.
3. the processing step of coating adhesive preparation is:
(1) preparation A component: with the on request ratio mixing of each component, temperature control is between 61 ℃-68 ℃, and low rate mixing 20min mixes, and the barrelling sealing is stand-by;
(2) preparation B component: with the on request ratio mixing of each component, temperature control is between 66 ℃-73 ℃, and low rate mixing 30min mixes, and the barrelling sealing is stand-by;
(3) preparation C component: with the on request ratio mixing of each component, temperature control is between 46 ℃-53 ℃, and low rate mixing 10min mixes, and the barrelling sealing is stand-by;
(4) preparation coating adhesive: when wish is implemented the metal zip fastener coating process, be A: B: C=1 with above-mentioned three kinds of barreled material by the quality proportioning: mix at 1: 1, use immediately after low rate mixing 2min mixes.
By the prepared baking-curing metal zip fastener epoxy coating glue of the present invention, that a kind of cost is reasonable, viscosity is low, the transparency is good, the oily mater of applicable baking-curing, the zipper metal external coating, coating has behind low-temperature bake that transparency is good, salt spray resistance, acid and alkali-resistance, rub resistance, water-fast, ageing-resistant, nondiscoloration, characteristics such as sticking look, slide fastener quality and class promote, and the market competitiveness strengthens.
Embodiment
1, the preparation of three components, take each preparation 100kg as example:
(1) preparation of A component: take by weighing Resins, epoxy 70kg, solvent 30kg and mix, temperature control is about 65 ℃, and low rate mixing 20min mixes, and the barrelling sealing is stand-by;
(2) preparation of B component: take by weighing stiffening agent 45kg, brightening agent 35kg, smooth agent 10kg, siccative 5kg, acid-proof antalkaline 5kg mixing, temperature control is about 70 ℃, and low rate mixing 30min mixes, and the barrelling sealing is stand-by;
(3) preparation of C component: take by weighing dimethylbenzene 70kg, butyl ether 10kg, butanols 15kg, butyl ester 5kg mixing, temperature control is about 50 ℃, and low rate mixing 10min mixes, and the barrelling sealing is stand-by;
Wherein: the Resins, epoxy in the A component is the E-33 bisphenol A epoxide resin; Solvent in the A component is ethylene glycol; Stiffening agent in the B component is the SU of Henan nation liquid sclerotherapy; Brightening agent in the B component is young eastern BL-20 baking vanish brightener; Smooth agent in the B component is young eastern OP-8050 (the COALAR)-general levelling deaeration of A/SL solvent-borne type smooth agent; Siccative in the B component is dibutyl tin laurate; Acid-proof antalkaline in the B component is Tutofusin tris.
2, the preparation of coating adhesive, take preparation 30kg as example: when wish is implemented coating process, take by weighing A, B, each 10kg of C component mixes, low rate mixing 2min uses after evenly immediately.
Claims (9)
1. a baking-curing metal zip fastener epoxy coating glue is comprised of A, B, C three components, and the functional quality proportioning is A: B: C=1: 1: 1, by mass, the A component consist of Resins, epoxy 63-75% and solvent 25-37%; The B component consist of stiffening agent 38-50%, brightening agent 30-42%, smooth agent 10%, siccative 5% and acid-proof antalkaline 5%; The C component consist of dimethylbenzene 63-75%, butyl ether 10%, butanols 10-22% and butyl ester 5%.
2. baking-curing metal zip fastener epoxy coating glue according to claim 1, it is characterized in that: the Resins, epoxy in the A component is the E-33 bisphenol A epoxide resin.
3. baking-curing metal zip fastener epoxy coating glue according to claim 1, it is characterized in that: the solvent in the A component is ethylene glycol.
4. baking-curing metal zip fastener epoxy coating glue according to claim 1, it is characterized in that: the stiffening agent in the B component is the SU of Henan nation liquid sclerotherapy.
5. baking-curing metal zip fastener epoxy coating glue according to claim 1, it is characterized in that: the brightening agent in the B component is young eastern BL-20 baking vanish brightener.
6. baking-curing metal zip fastener epoxy coating glue according to claim 1, it is characterized in that: the smooth agent in the B component is young eastern OP-8050 (the COALAR)-general levelling deaeration of A/SL solvent-borne type smooth agent.
7. baking-curing metal zip fastener epoxy coating glue according to claim 1, it is characterized in that: the siccative in the B component is dibutyl tin laurate.
8. baking-curing metal zip fastener epoxy coating glue according to claim 1, it is characterized in that: the acid-proof antalkaline in the B component is Tutofusin tris.
9. baking-curing metal zip fastener according to claim 1 is with the preparation method of epoxy coating glue, and its processing step is as follows:
(1) preparation A component: with the on request ratio mixing of each component, temperature control is between 61 ℃-68 ℃, and low rate mixing 20min mixes, and the barrelling sealing is stand-by;
(2) preparation B component: with the on request ratio mixing of each component, temperature control is between 66 ℃-73 ℃, and low rate mixing 30min mixes, and the barrelling sealing is stand-by;
(3) preparation C component: with the on request ratio mixing of each component, temperature control is between 46 ℃-53 ℃, and low rate mixing 10min mixes, and the barrelling sealing is stand-by;
(4) preparation coating adhesive: when wish is implemented the metal zip fastener coating process, be A: B: C=1 with above-mentioned three kinds of barreled material by the quality proportioning: mix at 1: 1, low rate mixing 2min mixes rear use.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210503770.9A CN103013291B (en) | 2012-12-02 | 2012-12-02 | Epoxy resin coating adhesive for roasting and curing metal zipper and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210503770.9A CN103013291B (en) | 2012-12-02 | 2012-12-02 | Epoxy resin coating adhesive for roasting and curing metal zipper and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103013291A true CN103013291A (en) | 2013-04-03 |
| CN103013291B CN103013291B (en) | 2015-02-25 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201210503770.9A Expired - Fee Related CN103013291B (en) | 2012-12-02 | 2012-12-02 | Epoxy resin coating adhesive for roasting and curing metal zipper and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105949953A (en) * | 2016-06-12 | 2016-09-21 | 蚌埠市禹会区贵宾装饰材料商行 | Wear-resisting baked varnish for photo frame |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102010572A (en) * | 2010-11-16 | 2011-04-13 | 宏昌电子材料股份有限公司 | Environment-friendly epoxy resin composition as well as preparation method and application thereof |
| CN102153952A (en) * | 2010-12-12 | 2011-08-17 | 广东辉丰科技股份有限公司 | Composite coating for surface of zipper pull head and baking finish process |
-
2012
- 2012-12-02 CN CN201210503770.9A patent/CN103013291B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102010572A (en) * | 2010-11-16 | 2011-04-13 | 宏昌电子材料股份有限公司 | Environment-friendly epoxy resin composition as well as preparation method and application thereof |
| CN102153952A (en) * | 2010-12-12 | 2011-08-17 | 广东辉丰科技股份有限公司 | Composite coating for surface of zipper pull head and baking finish process |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105949953A (en) * | 2016-06-12 | 2016-09-21 | 蚌埠市禹会区贵宾装饰材料商行 | Wear-resisting baked varnish for photo frame |
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| Publication number | Publication date |
|---|---|
| CN103013291B (en) | 2015-02-25 |
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Granted publication date: 20150225 Termination date: 20181202 |