CN102994332B - Making method of spirulina wine - Google Patents
Making method of spirulina wine Download PDFInfo
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- CN102994332B CN102994332B CN2012103016712A CN201210301671A CN102994332B CN 102994332 B CN102994332 B CN 102994332B CN 2012103016712 A CN2012103016712 A CN 2012103016712A CN 201210301671 A CN201210301671 A CN 201210301671A CN 102994332 B CN102994332 B CN 102994332B
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Images
Abstract
The invention provides a making technology of spirulina wine. The traditional spirulina wine is formed by directly soaking spirulina into grain wine, and is turbid in color, poor in mouth feel and low in phycocyanin content. The making method comprises the steps of: extracting spirulina twice by using alcohol and water, and extracting chlorophyll, beta-carotene and phycocyanin from spirulina to the greatest extent. Through determination, 76 percent of phycocyanin, 61 percent of gamma-linolenic acid and 67 percent of beta-carotene in spirulina powder can be extracted into the wine. Compared with the traditional direct soaking technology, the making technology has the advantage that the effective utilization rate of phycocyanin is increased to 76 percent from 19 percent. Experiment results indicate that the spirulina wine made by adopting the making technology provided by the invention has the advantages of good mouth feel, clear color, high phycocyanin content, simpleness in process and long quality guarantee period, and can be blended into drinking wines with different colors and tastes, different alcoholic strengths and different active ingredients.
Description
Technical field
The invention belongs to the health promoting wine field, relate in particular to a kind of spirulina wine making method.
Background technology
Spirulina is to be acknowledged as abundant, the most balanced a kind of basic foodstuff of nutrition, and the nutrient contg of 1 gram spirulina equals the summation of 1 kilogram of all kinds of vegetable nutrient composition.Spirulina integrates the various nutrient elements of needed by human, and β-carotene wherein is the precursor of vitamin A, is the nutritive element that body weight for humans is wanted, and has the body immunity of raising and anticancer effect.Vitamin B12 can help protein and nucleic acid to carry out metabolism, enhancing development.Can also promote erythrocytic generation, the prevention anaemia.Algae blue pigment contributes to the multiple important enzyme of synthetic and balance the body metabolism.Anticancer growth and strengthening immunity are played an important role, and are a kind of rare natural pigments.Gamma-linolenic acid is called as the unsaturated fatty acids of needed by human, has the metabolism that reduces serum cholesterol, accelerates alcohol and transforms, improves the physiological action such as allergic dermatitis.Traditional spirulina wine is that spirulina directly is immersed in grain wine, color and luster muddiness not only, and mouthfeel is poor, and Phycocyanins, C-content is low.And my method is, with the second alcohol and water, spirulina is carried out to twice extraction, to greatest extent the chlorophyll in spirulina, β-carotene and Phycocyanins, C-are extracted.After measured, 76% Phycocyanins, C-in the algae powder, 61% gamma-linolenic acid, 67% β-carotene can be extracted in wine.With traditional direct immersion, compare, the effective rate of utilization of Phycocyanins, C-brings up to 76% from 19%.
The patent CN1144096A obtained the authorization at present, disclose a kind of manufacture method of spirulina wine, but so lengthy and tedious complexity of method, cost is higher, and practicality is not high.
In a word, the spirulina wine that uses new technology to produce has the advantages such as mouthfeel is good, color and luster is limpid, Phycocyanins, C-content is high, technical process is simple.
Summary of the invention
In order to overcome the deficiency of current technology, the invention provides a kind of spirulina wine production method, concrete technical scheme is as follows:
A kind of spirulina wine making method is characterized in that this spirulina wine making step is as follows:
The first step
Get spirulina dry algae powder 1.5g and be dissolved in 200ml distilled water, fully stir and shake up 60min, with the silk cover filtering of mesh bore 80-100 μ m, after removing sediment, by the centrifugal 5min of whizzer for supernatant liquor, rotating speed 3500r/min, get the standing 24h of supernatant liquor, get supernatant liquor standby as A liquid;
Second step
Get spirulina dry algae powder 2g and be dissolved in the ethanol of 200ml95%, fully stir, shake up 45min, with the silk cover filtering of mesh bore 60-80 μ m, after removing sediment, get supernatant liquor, with the centrifugal 4min of whizzer, rotating speed 4000r/min, get the standing 36h of supernatant liquor, gets supernatant liquor standby as B liquid.
The 3rd step
Get wine base or former wine 200ml, add A liquid 25ml, fully stir or shake up 15min, add again B liquid 20ml, fully shake up 30min, a small amount of flocks is now arranged, with the silk cover filtering of mesh bore 50-60 μ m, remove flocks, get the centrifugal 4min of supernatant liquor, rotating speed 4500r/min, get the standing 96h of supernatant liquor, get supernatant liquor, bottling completes.
A kind of spirulina wine making method is characterized in that this spirulina wine making step is as follows:
The first step
Getting spirulina dry algae powder 2.5g is dissolved in 280ml distilled water, fully stir and shake up 60min, silk cover filtering with mesh bore 80-100 μ m, after removing sediment, by the centrifugal 5min of whizzer for supernatant liquor, rotating speed 3500r/min, get the standing 24h of supernatant liquor, get supernatant liquor standby as A liquid, extract Phycocyanins, C-, supernatant liquor is sky blue;
Second step
Getting spirulina dry algae powder 4g is dissolved in the ethanol of 400ml95%, fully stir, shake up 45min, with the silk cover filtering of mesh bore 60-80 μ m, after removing sediment, get supernatant liquor, with the centrifugal 4min of whizzer, rotating speed 4000r/min, get the standing 36h of supernatant liquor, gets supernatant liquor standby as B liquid, extract the Alcohol soluble compositions such as β-carotene, chlorophyll a, leaf vitamin B12, gamma-linolenic acid, supernatant liquor is grass green;
The 3rd step
Get wine base or former wine 200ml, add A liquid 25ml, fully stir or shake up 15min, add again B liquid 20ml, fully shake up 30min, a small amount of flocks is now arranged, with the silk cover filtering of mesh bore 50-60 μ m, remove flocks, get the centrifugal 4min of supernatant liquor, rotating speed 4500r/min, get the standing 96h of supernatant liquor, get supernatant liquor, bottling completes.
A kind of spirulina wine making method is characterized in that this spirulina wine making step is as follows:
The first step
Get spirulina dry algae powder 25g, supplementary component is dissolved in 2500ml distilled water, fully stir and shake up 60min, silk cover filtering with mesh bore 80-100 μ m, after removing sediment, by the centrifugal 5min of whizzer for supernatant liquor, rotating speed 3500r/min, get the standing 24h of supernatant liquor, gets supernatant liquor standby as A liquid; Described supplementary component is:
Second step
Getting spirulina dry algae powder 40g is dissolved in the ethanol of 4000ml95%, fully stir, shake up 45min, with the silk cover filtering of mesh bore 60-80 μ m, after removing sediment, get supernatant liquor, with the centrifugal 4min of whizzer, rotating speed 4000r/min, get the standing 36h of supernatant liquor, gets supernatant liquor standby as B liquid, extract the Alcohol soluble compositions such as β-carotene, chlorophyll a, leaf vitamin B12, gamma-linolenic acid, supernatant liquor is grass green.
The 3rd step
Get wine base or former wine 2000ml, add A liquid 250ml, fully stir or shake up 15min, add again B liquid 200ml, fully shake up 30min, a small amount of flocks is now arranged, with the silk cover filtering of mesh bore 50-60 μ m, remove flocks, get the centrifugal 4min of supernatant liquor, rotating speed 4500r/min, get the standing 96h of supernatant liquor, get supernatant liquor, bottling completes.
A kind of spirulina wine making method is characterized in that this spirulina wine making step is as follows:
The first step
Get spirulina dry algae powder 25g, supplementary component is dissolved in 2500ml distilled water, fully stir and shake up 60min, silk cover filtering with mesh bore 80-100 μ m, after removing sediment, by the centrifugal 5min of whizzer for supernatant liquor, rotating speed 3500r/min, get the standing 24h of supernatant liquor, gets supernatant liquor standby as A liquid; Described supplementary component is:
Second step
Getting spirulina dry algae powder 4g is dissolved in the ethanol of 400ml95%, fully stir, shake up 45min, with the silk cover filtering of mesh bore 60-80 μ m, after removing sediment, get supernatant liquor, with the centrifugal 4min of whizzer, rotating speed 4000r/min, get the standing 36h of supernatant liquor, gets supernatant liquor standby as B liquid, extract the Alcohol soluble compositions such as β-carotene, chlorophyll a, leaf vitamin B12, gamma-linolenic acid, supernatant liquor is grass green.
The 3rd step
Get wine base or former wine 200ml, add A liquid 25ml, fully stir or shake up 15min, add again B liquid 20ml, fully shake up 30min, a small amount of flocks is now arranged, with the silk cover filtering of mesh bore 50-60 μ m, remove flocks, get the centrifugal 4min of supernatant liquor, rotating speed 4500r/min, get the standing 96h of supernatant liquor, get supernatant liquor, bottling completes.
Beneficial effect:
Experimental result shows, uses the spirulina wine of new technology production to have the advantages such as mouthfeel is good, color and luster is limpid, Phycocyanins, C-content is high, technical process is simple.
The accompanying drawing explanation
The preparation flow figure that Fig. 1 is A liquid
The preparation flow figure that Fig. 2 is B liquid
Fig. 3 is spirulina wine fabrication processing figure
Embodiment
A kind of spirulina wine making method is characterized in that this spirulina wine making step is as follows:
The first step
Get spirulina dry algae powder 1.5g and be dissolved in 200ml distilled water, fully stir and shake up 60min, with the silk cover filtering of mesh bore 80-100 μ m, after removing sediment, by the centrifugal 5min of whizzer for supernatant liquor, rotating speed 3500r/min, get the standing 24h of supernatant liquor, get supernatant liquor standby as A liquid;
Second step
Get spirulina dry algae powder 2g and be dissolved in the ethanol of 200ml95%, fully stir, shake up 45min, with the silk cover filtering of mesh bore 60-80 μ m, after removing sediment, get supernatant liquor, with the centrifugal 4min of whizzer, rotating speed 4000r/min, get the standing 36h of supernatant liquor, gets supernatant liquor standby as B liquid.
The 3rd step
Get wine base or former wine 200ml, add A liquid 25ml, fully stir or shake up 15min, add again B liquid 20ml, fully shake up 30min, a small amount of flocks is now arranged, with the silk cover filtering of mesh bore 50-60 μ m, remove flocks, get the centrifugal 4min of supernatant liquor, rotating speed 4500r/min, get the standing 96h of supernatant liquor, get supernatant liquor, bottling completes.
A kind of spirulina wine making method is characterized in that this spirulina wine making step is as follows:
The first step
Getting spirulina dry algae powder 2.5g is dissolved in 280ml distilled water, fully stir and shake up 60min, silk cover filtering with mesh bore 80-100 μ m, after removing sediment, by the centrifugal 5min of whizzer for supernatant liquor, rotating speed 3500r/min, get the standing 24h of supernatant liquor, get supernatant liquor standby as A liquid, extract Phycocyanins, C-, supernatant liquor is sky blue;
Second step
Getting spirulina dry algae powder 4g is dissolved in the ethanol of 400ml95%, fully stir, shake up 45min, with the silk cover filtering of mesh bore 60-80 μ m, after removing sediment, get supernatant liquor, with the centrifugal 4min of whizzer, rotating speed 4000r/min, get the standing 36h of supernatant liquor, gets supernatant liquor standby as B liquid, extract the Alcohol soluble compositions such as β-carotene, chlorophyll a, leaf vitamin B12, gamma-linolenic acid, supernatant liquor is grass green;
The 3rd step
Get wine base or former wine 200ml, add A liquid 25ml, fully stir or shake up 15min, add again B liquid 20ml, fully shake up 30min, a small amount of flocks is now arranged, with the silk cover filtering of mesh bore 50-60 μ m, remove flocks, get the centrifugal 4min of supernatant liquor, rotating speed 4500r/min, get the standing 96h of supernatant liquor, get supernatant liquor, bottling completes.
A kind of spirulina wine making method is characterized in that this spirulina wine making step is as follows:
The first step
Get spirulina dry algae powder 25g, supplementary component is dissolved in 2500ml distilled water, fully stir and shake up 60min, silk cover filtering with mesh bore 80-100 μ m, after removing sediment, by the centrifugal 5min of whizzer for supernatant liquor, rotating speed 3500r/min, get the standing 24h of supernatant liquor, gets supernatant liquor standby as A liquid; Described supplementary component is:
Second step
Getting spirulina dry algae powder 40g is dissolved in the ethanol of 4000ml95%, fully stir, shake up 45min, with the silk cover filtering of mesh bore 60-80 μ m, after removing sediment, get supernatant liquor, with the centrifugal 4min of whizzer, rotating speed 4000r/min, get the standing 36h of supernatant liquor, gets supernatant liquor standby as B liquid, extract the Alcohol soluble compositions such as β-carotene, chlorophyll a, leaf vitamin B12, gamma-linolenic acid, supernatant liquor is grass green.
The 3rd step
Get wine base or former wine 2000ml, add A liquid 250ml, fully stir or shake up 15min, add again B liquid 200ml, fully shake up 30min, a small amount of flocks is now arranged, with the silk cover filtering of mesh bore 50-60 μ m, remove flocks, get the centrifugal 4min of supernatant liquor, rotating speed 4500r/min, get the standing 96h of supernatant liquor, get supernatant liquor, bottling completes.
A kind of spirulina wine making method is characterized in that this spirulina wine making step is as follows:
The first step
Get spirulina dry algae powder 25g, supplementary component is dissolved in 2500ml distilled water, fully stir and shake up 60min, silk cover filtering with mesh bore 80-100 μ m, after removing sediment, by the centrifugal 5min of whizzer for supernatant liquor, rotating speed 3500r/min, get the standing 24h of supernatant liquor, gets supernatant liquor standby as A liquid; Described supplementary component is:
Second step
Getting spirulina dry algae powder 4g is dissolved in the ethanol of 400ml95%, fully stir, shake up 45min, with the silk cover filtering of mesh bore 60-80 μ m, after removing sediment, get supernatant liquor, with the centrifugal 4min of whizzer, rotating speed 4000r/min, get the standing 36h of supernatant liquor, gets supernatant liquor standby as B liquid, extract the Alcohol soluble compositions such as β-carotene, chlorophyll a, leaf vitamin B12, gamma-linolenic acid, supernatant liquor is grass green.
The 3rd step
Get wine base or former wine 200ml, add A liquid 25ml, fully stir or shake up 15min, add again B liquid 20ml, fully shake up 30min, a small amount of flocks is now arranged, with the silk cover filtering of mesh bore 50-60 μ m, remove flocks, get the centrifugal 4min of supernatant liquor, rotating speed 4500r/min, get the standing 96h of supernatant liquor, get supernatant liquor, bottling completes.
Precaution
1) in second step, ethanol used should be the ethanol of the fermentative production such as grain, i.e. grain wine, but not industrial ethyl alcohol;
2) institute in steps, the first step particularly, all should not under high light (being no more than 8000lux) or direct sunlight and high temperature, (be no more than 35 ℃) carries out;
3) the first step should complete as far as possible in the short period of time, in order to avoid the Phycocyanins, C-sex change;
Should avoid direct sunlight when 4) finished wine is preserved.
Need explanation, the numerical range in specific embodiment to realize, more than end points and mid point can realize, the length limit is not carried out exhaustive at this.
Finally it should be noted that: above embodiment only, in order to technical scheme of the present invention to be described, is not intended to limit; Although with reference to previous embodiment, the present invention is had been described in detail, those of ordinary skill in the art is to be understood that: its technical scheme that still can put down in writing previous embodiment is modified, or part technical characterictic wherein is equal to replacement; And these modifications or replacement do not make the essence of appropriate technical solution break away from the spirit and scope of embodiment of the present invention technical scheme.
Claims (4)
1. a spirulina wine making method is characterized in that this spirulina wine making step is as follows:
The first step
Get spirulina dry algae powder 1.5g and be dissolved in 200ml distilled water, fully stir and shake up 60min, with the silk cover filtering of mesh bore 80-100 μ m, after removing sediment, by the centrifugal 5min of whizzer for supernatant liquor, rotating speed 3500r/min, get the standing 24h of supernatant liquor, get supernatant liquor standby as A liquid;
Second step
Get spirulina dry algae powder 2g and be dissolved in the ethanol of 200m195%, fully stir, shake up 45min, with the silk cover filtering of mesh bore 60-80 μ m, after removing sediment, get supernatant liquor, with the centrifugal 4min of whizzer, rotating speed 4000r/min, get the standing 36h of supernatant liquor, gets supernatant liquor standby as B liquid;
The 3rd step
Get wine base or former wine 200ml, add A liquid 25ml, fully stir or shake up 15min, add again B liquid 20ml, fully shake up 30min, a small amount of flocks is now arranged, with the silk cover filtering of mesh bore 50-60 μ m, remove flocks, get the centrifugal 4min of supernatant liquor, rotating speed 4500r/min, get the standing 96h of supernatant liquor, get supernatant liquor, bottling completes.
2. a spirulina wine making method is characterized in that this spirulina wine making step is as follows:
The first step
Getting spirulina dry algae powder 2.5g is dissolved in 280ml distilled water, fully stir and shake up 60min, silk cover filtering with mesh bore 80-100 μ m, after removing sediment, by the centrifugal 5min of whizzer for supernatant liquor, rotating speed 3500r/min, get the standing 24h of supernatant liquor, get supernatant liquor standby as A liquid, extract Phycocyanins, C-, supernatant liquor is sky blue;
Second step
Getting spirulina dry algae powder 4g is dissolved in the ethanol of 400m195%, fully stir, shake up 45min, with the silk cover filtering of mesh bore 60-80 μ m, after removing sediment, get supernatant liquor, with the centrifugal 4min of whizzer, rotating speed 4000r/min, get the standing 36h of supernatant liquor, gets supernatant liquor standby as B liquid, extract the Alcohol soluble compositions such as β-carotene, chlorophyll a, leaf vitamin B12, gamma-linolenic acid, supernatant liquor is grass green;
The 3rd step
Get wine base or former wine 200mi, add A liquid 25ml, fully stir or shake up 15min, add again B liquid 20ml, fully shake up 30min, a small amount of flocks is now arranged, with the silk cover filtering of mesh bore 50-60 μ m, remove flocks, get the centrifugal 4min of supernatant liquor, rotating speed 4500r/min, get the standing 96h of supernatant liquor, get supernatant liquor, bottling completes.
3. spirulina wine making method as claimed in claim 2 is characterized in that this spirulina wine making step is as follows:
The first step
Get spirulina dry algae powder 25g, supplementary component is dissolved in 2500ml distilled water, fully stir and shake up 60min, silk cover filtering with mesh bore 80-100 μ m, after removing sediment, by the centrifugal 5min of whizzer for supernatant liquor, rotating speed 3500r/min, get the standing 24h of supernatant liquor, gets supernatant liquor standby as A liquid; Described supplementary component is:
Second step
Getting spirulina dry algae powder 40g is dissolved in the ethanol of 4000m195%, fully stir, shake up 45min, with the silk cover filtering of mesh bore 60-80 μ m, after removing sediment, get supernatant liquor, with the centrifugal 4min of whizzer, rotating speed 4000r/min, get the standing 36h of supernatant liquor, gets supernatant liquor standby as B liquid, extract the Alcohol soluble compositions such as β-carotene, chlorophyll a, leaf vitamin B12, gamma-linolenic acid, supernatant liquor is grass green;
The 3rd step
Get wine base or former wine 2000ml, add A liquid 250ml, fully stir or shake up 15min, add again B liquid 200ml, fully shake up 30min, a small amount of flocks is now arranged, with the silk cover filtering of mesh bore 50-60 μ m, remove flocks, get the centrifugal 4min of supernatant liquor, rotating speed 4500r/min, get the standing 96h of supernatant liquor, get supernatant liquor, bottling completes.
4. a kind of spirulina wine making method as claimed in claim 2 is characterized in that this spirulina wine making step is as follows:
The first step
Get spirulina dry algae powder 25g, supplementary component is dissolved in 2500ml distilled water, fully stir and shake up 60min, silk cover filtering with mesh bore 80-100 μ m, after removing sediment, by the centrifugal 5min of whizzer for supernatant liquor, rotating speed 3500r/min, get the standing 24h of supernatant liquor, gets supernatant liquor standby as A liquid; Described supplementary component is:
Second step
Getting spirulina dry algae powder 4g is dissolved in the ethanol of 400m195%, fully stir, shake up 45min, with the silk cover filtering of mesh bore 60-80 μ m, after removing sediment, get supernatant liquor, with the centrifugal 4min of whizzer, rotating speed 4000r/min, get the standing 36h of supernatant liquor, gets supernatant liquor standby as B liquid, extract the Alcohol soluble compositions such as β-carotene, chlorophyll a, leaf vitamin B12, gamma-linolenic acid, supernatant liquor is grass green;
The 3rd step
Get wine base or former wine 200ml, add A liquid 25ml, fully stir or shake up 15min, add again B liquid 20ml, fully shake up 30min, a small amount of flocks is now arranged, with the silk cover filtering of mesh bore 50-60 μ m, remove flocks, get the centrifugal 4min of supernatant liquor, rotating speed 4500r/min, get the standing 96h of supernatant liquor, get supernatant liquor, bottling completes.
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| CN103805487B (en) * | 2014-03-04 | 2016-04-06 | 临沂大学 | A kind of making method of marine alga wine |
| CN104263603B (en) * | 2014-10-20 | 2017-01-18 | 临沂大学 | Wine with arctium lappa and dunaliella salina and preparation technology thereof |
| CN106119000A (en) * | 2016-08-28 | 2016-11-16 | 北海生巴达生物科技有限公司 | A kind of chlorella rice wine and brewing method |
| CN108060046A (en) * | 2016-11-09 | 2018-05-22 | 山东群英医学研究有限公司 | A kind of auxiliary reducing hyperglycaemia, the health liquor of hyperlipidemia |
| CN107475047A (en) * | 2017-10-22 | 2017-12-15 | 北京与果酒业有限公司 | A kind of phycocyanin assembled alcoholic drinks and preparation method thereof |
| CN111909811A (en) * | 2020-07-27 | 2020-11-10 | 深圳市太空微藻生物科技有限公司 | Preparation method and product of algae-flavor liquor |
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