CN102002455B - Method for simultaneously producing mulberry anthocyanin and mulberry wine with mulberry juice - Google Patents
Method for simultaneously producing mulberry anthocyanin and mulberry wine with mulberry juice Download PDFInfo
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- CN102002455B CN102002455B CN201010545716A CN201010545716A CN102002455B CN 102002455 B CN102002455 B CN 102002455B CN 201010545716 A CN201010545716 A CN 201010545716A CN 201010545716 A CN201010545716 A CN 201010545716A CN 102002455 B CN102002455 B CN 102002455B
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Abstract
The invention discloses a method for simultaneously producing mulberry anthocyanin and mulberry wine by using mulberry juice as a raw material. The method comprises the following steps of: enabling mulberry juice to flow by a chromatography column which is filled with macroporous absorption resin capable of adsorbing mulberry anthocyanin, wherein the flowing juice adsorbed with mulberry anthocyanin can be used for producing mulberry wine through fermentation; eluting the mulberry anthocyanin adsorbed in the chromatography column with acidic ethanol; and concentrating and drying the eluted mulberry anthocyanin ethanol solution to obtain a mulberry anthocyanin product. By adopting the method provided by the invention, the mulberry anthocyanin product with a certain health function can be obtained, and the mulberry wine product is purple and has favorable luster and light transmission.
Description
Technical field
The present invention relates to a kind of is the method that raw material is produced sorosis cyanidin(e) and mulberry wine simultaneously with the Fructus Mori juice.
Background technology
China's planting mulberry and breeding silkworm are with a long history, and Morus alba Resource Development is very abundant.Mulberry fruit is the fruit of mulberry tree, and mulberry fruit just is employed as fruit and Chinese medicinal materials since ancient times, is confirmed as one of the agricultural-food of " be food be again medicine " at present by health ministry.The traditional Chinese medical science thinks that mulberry fruit is distinguished the flavor of sweet cold in nature, have promote the production of body fluid to quench thirst, liver-kidney tonifying, nourishing YIN and supplementing blood, the effect such as calm the nerves that makes eye bright, edible for a long time mulberry fruit can be promoted longevity.Modern medicine study shows that mulberry fruit has raise immunity, promotes the growth of hematopoietic cell, prevents effects such as human body artery hardens, enhances metabolism.
Sorosis is very short annual collection period, has only one month usually, normally adopts the form preservation raw material of sorosis Normal juice or juice concentrate to be used further to further processing.Sorosis Normal juice is produced has advantages such as technology is simple, facility investment is few, the fragrance maintenance is good, takies the more shortcoming of wrapping material and place but also there is raw material to store.It is little that concentrated Fructus Mori juice has a volume without spissated sorosis Normal juice relatively; Convenient transportation, the characteristics that packing cost is few; Simultaneously because concentrated Fructus Mori juice soluble solid content is higher; Be not easy putrid and deterioratedly, be particularly suitable for needing the international trade of long-distance transport, at present general large-scale outlet fruit juice corporate boss to want product form be soluble solid content 60% above juice concentrate.
Sorosis Normal juice and juice concentrate also can be processed into mulberry wine except that being processed into nectar; Drinks is one type of important consumer's goods of China; Along with going deep into of scientific research; The meliority that fruit wine had further is familiar with, and consumption is increasing, and the production of development fruit wine is the important directions of the current drinks industry of China.It is purplish red to contain abundant glucose, organic acid, mineral substance, VITAMINs, color and luster in the Fructus Mori juice, is fit to very much ferment wine brewing.Utilize the mulberry wine of Fructus Mori juice fermentative prodn not only to keep the most nutritive ingredients in the sorosis; Also have deep and remote strongly fragrant, the characteristics such as the wine body is plentiful, mellow, sour and sweet palatability, taste are continuous, unique style of lovely luster, the dense fragrance of aroma; Can be rated as the good merchantable brand in the fruit wine, utilize Fructus Mori juice fermentative prodn Mublerry wine to turn waste into wealth, significantly reduce the pollution of sorosis environment; Improve the overall economic efficiency in mulberry field greatly, this stability and development for silkworm and mulberry production has positive social effect.
Be rich in cyanidin(e) in sorosis Normal juice and the juice concentrate, cyanidin(e) belongs to natural red colouring matter, and food dye is very important foodstuff additive; Give food with pleasing color and luster; Give people enjoyment, play an important role to increasing appetite of people, but also be the basis of differentiating and estimate food quality with U.S.A.Red pigment is to use one of pigment the most widely.Sorosis cyanidin(e) also is one of edible natural pigment of health ministry approval use, code 08.129.It is reported that simultaneously sorosis cyanidin(e) has anti-oxidant significantly, anticancer, antiinflammation, liver and cardiovascular is had the certain protection effect.
The technology that present mulberry wine fermentative prodn generally adopts is to add yeast again after the sorosis Normal juice interpolation sucrose adjustment pol to carry out zymamsis; Adopt the mulberry wine of this technical matters fermentation owing to added more sucrose; Broken the saccharic acid balance in the Fructus Mori juice; Cause fruit wine to occur potato spirit easily, biogenic amine content is higher, easy the higher authorities' phenomenon.The technical matters of fermenting after also having some reports that sorosis Normal juice is concentrated adopts this technology, and the fruit wine mouthfeel of fermentation is better, is difficult for the higher authorities, and the color is too dark but exist, and lost the due clear of fruit wine, glossiness characteristics.
Summary of the invention
The object of the present invention is to provide a kind of method of producing sorosis cyanidin(e) and mulberry wine simultaneously with Fructus Mori juice, features simple and practical process not only can make coloury mulberry wine, and can make sorosis cyanidin(e) simultaneously.
The present invention realizes through following technical measures: a kind of method of producing sorosis cyanidin(e) and mulberry wine with Fructus Mori juice simultaneously; The Fructus Mori juice feedstream is crossed the chromatography column that the macroporous adsorbent resin that can adsorb sorosis cyanidin(e) is housed, and the effusive fruit juice that has adsorbed part sorosis cyanidin(e) is used for the fermentative prodn mulberry wine; Absorption sorosis cyanidin(e) adopts acidic ethanol that its wash-out is come out in the chromatography column, the sorosis cyanidin(e) ethanolic soln of wash-out through concentrating with drying after obtain sorosis cyanidin(e) product.
Through the amount and the flow velocity of control chromatography column resin, above-mentioned effusive Fructus Mori juice soluble solid content is between 10 ~ 30%, and anthocyanidin content is between 100 ~ 800mg/L.Make the wine and women-sensual pursuits that makes better, it is purplish red to reach color and luster, and printing opacity.
The sorosis cyanidin(e) product that adopts this method both can obtain having certain health care functions, the mulberry wine product colour is purplish red simultaneously, has good light transmittance, features simple and practical process, the development and use of further expanding sorosis.
Embodiment
Following specific embodiments of the invention describes in further detail.Following examples are used to explain the present invention, but are not used for limiting scope of the present invention.
Embodiment one
Sorosis juice concentrate with 65% is a raw material, gets 5kg sorosis juice concentrate, adds the 8kg pure water; Be diluted to soluble solid content 25%, anthocyanidin content 2930mg/L crosses diameter 8cm with the velocity flow of flow velocity 100L/hr; The chromatography column that the 4kgX-5 macroporous adsorbent resin is housed of height 1.2m when effusive Fructus Mori juice soluble solid content reaches 20%, begins to collect effluent; Collect 12.5kg, the Fructus Mori juice soluble solid content of collecting 24.5%, anthocyanidin content 650mg/L.
After stopping to collect, adopt the technology wash-out that often has to come out the sorosis cyanidin(e) that adsorbs in the chromatography column.Earlier with 20kg pure water rinsing chromatography column, the compositions such as saccharic acid of remnants on the post are rinsed out, wash post with 75% the ethanol of 0.5%HCl again; Be washed till colourless basically; Obtain 20L sorosis cyanidin(e) ethanolic soln, carry out thin film concentration, obtain the lotion of soluble solid content 65% after; Carry out lyophilize, obtain sorosis cyanidin(e) 25g at last.
The above-mentioned 12.5kg Fructus Mori juice of collecting is adopted common process fermentation system wine, add 4g Angel wine active dry yeast, 20 ℃ of fermentations 15 days; Do not descend to soluble solid content; Placed again 1 month, and, obtained mulberry wine after the ultrafiltration can through diatomite filtration.
Embodiment two
Sorosis juice concentrate with 65% is a raw material, gets 2.5kg sorosis juice concentrate, adds the 8kg pure water; Be diluted to soluble solid content 17.1%, anthocyanidin content 1813mg/L crosses diameter 8cm with the velocity flow of flow velocity 100L/hr; The chromatography column that the 4kgX-5 macroporous adsorbent resin is housed of height 1.2m begins to collect effluent when having flowed out when soluble solid content reaches 14%, behind the collection 10kg; Stop to collect; The Fructus Mori juice soluble solid content 16.7% that collect this moment, anthocyanidin content 184mg/L obtains sorosis cyanidin(e) 25g at last.
After stopping to collect,, compositions such as saccharic acid remaining on the post are rinsed out with 20kg pure water rinsing chromatography column; Wash post with 75% the ethanol of 0.5%HCl again, be washed till colourlessly basically, obtain 20L sorosis cyanidin(e) ethanolic soln; Carry out thin film concentration; After obtaining the solution of soluble solid content 10%, carry out spraying drying, obtain 12g sorosis cyanidin(e) at last.
With the 10kg Fructus Mori juice of collecting, add 800g sucrose, add 4g Angel wine active dry yeast again, 20 ℃ of fermentations 15 days, do not descend to soluble solid content, placed again 1 month, through diatomite filtration, obtain mulberry wine after the ultrafiltration can.
Embodiment three
Sorosis Normal juice with 25kg soluble solid 10.5% is raw material; Adopting thin film concentration to be concentrated into the 10kg soluble solid content is 26.2%, and anthocyanidin content is 3050mg/L, crosses diameter 8cm with the velocity flow of flow velocity 100L/hr; The chromatography column that the 4kgX-5 macroporous adsorbent resin is housed of height 1.2m; Begin to collect effluent when soluble solid content reaches 22% when having flowed out, behind the collection 9.6kg, stop to collect; The Fructus Mori juice soluble solid content 25.2% that collect this moment, anthocyanidin content 690mg/L.
After stopping to collect,, compositions such as saccharic acid remaining on the post are rinsed out with 20kg pure water rinsing chromatography column; Wash post with 75% the ethanol of 0.5%HCl again, be washed till colourlessly basically, obtain 20L sorosis cyanidin(e) ethanolic soln; Carry out thin film concentration; After obtaining the lotion of soluble solid content 65%, carry out vacuum microwave drying, obtain sorosis cyanidin(e) 20g at last.
With the 9.6kg Fructus Mori juice of collecting, add 4g Angel wine active dry yeast, 20 ℃ of fermentations 15 days, do not descend to soluble solid content, placed again 1 month, through diatomite filtration, obtain mulberry wine after the ultrafiltration can.
Claims (1)
1. method of producing sorosis cyanidin(e) and mulberry wine with Fructus Mori juice simultaneously; It is characterized in that: the Fructus Mori juice feedstream is crossed the chromatography column that the macroporous adsorbent resin that can adsorb sorosis cyanidin(e) is housed; The effusive fruit juice that has adsorbed part sorosis cyanidin(e) is used for the fermentative prodn mulberry wine; Said effusive Fructus Mori juice soluble solid content is between 10～30%, and anthocyanidin content is between 100～800mg/L; Absorption sorosis cyanidin(e) adopts acidic ethanol that its wash-out is come out in the chromatography column, the sorosis cyanidin(e) ethanolic soln of wash-out through concentrating with drying after obtain sorosis cyanidin(e); Described Fructus Mori juice raw material is: sorosis Normal juice is concentrated to soluble solid content 10～30% or the sorosis juice concentrate is diluted to soluble solid content 10～30%.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201010545716A CN102002455B (en) | 2010-11-16 | 2010-11-16 | Method for simultaneously producing mulberry anthocyanin and mulberry wine with mulberry juice |
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| CN201010545716A CN102002455B (en) | 2010-11-16 | 2010-11-16 | Method for simultaneously producing mulberry anthocyanin and mulberry wine with mulberry juice |
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| CN102002455A CN102002455A (en) | 2011-04-06 |
| CN102002455B true CN102002455B (en) | 2012-09-12 |
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103981067B (en) * | 2014-06-05 | 2016-04-27 | 济南国力生物科技有限公司 | A kind of complete processing of mulberry fruit |
| CN113234561B (en) * | 2021-06-21 | 2022-05-13 | 海南大学 | Fermentation method of mulberry sweet fermented fruit wine |
| CN113652324A (en) * | 2021-08-12 | 2021-11-16 | 攀枝花四喜农业发展有限责任公司 | Method for producing mulberry sweet wine without adding exogenous sugar and acid |
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2010
- 2010-11-16 CN CN201010545716A patent/CN102002455B/en active Active
Non-Patent Citations (4)
| Title |
|---|
| 刘学铭等.《D101A大孔吸附树脂吸附和分离桑椹红色素的研究》.《食品与发酵工业》.2002,第28卷(第1期),第19-22页. * |
| 季更生等.《桑椹红色素的研究现状与进展》.《安徽农业科学》.2007,第35卷(第28期),第8777-8778,8790页. * |
| 曹竑.《天然食品添加剂制取》.《食品添加剂》.2004,第413-414页. * |
| 陈美红等.《NKA大孔树脂分离纯化桑椹红色素的研究》.《食品科技》.2007,(第10期),第178-182页. * |
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| CN102002455A (en) | 2011-04-06 |
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