CN102994225A - Grease decoloring method - Google Patents

Grease decoloring method Download PDF

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Publication number
CN102994225A
CN102994225A CN2012104866517A CN201210486651A CN102994225A CN 102994225 A CN102994225 A CN 102994225A CN 2012104866517 A CN2012104866517 A CN 2012104866517A CN 201210486651 A CN201210486651 A CN 201210486651A CN 102994225 A CN102994225 A CN 102994225A
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holding tank
generating surface
light constituent
temperature
condenser
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CN2012104866517A
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CN102994225B (en
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陈汉卿
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Abstract

The invention discloses a grease decoloring method, belonging to the technical field of refining grease and used for solving the problems in grease decoloring that high temperature time is long, the product yield is low, and auxiliaries are in need and sewage is discharged. The grease decoloring method comprises the steps: increasing temperature of raw material oil to 150-170 DEG C through a heat exchanger, then sending the raw material oil into a molecular still, and evenly distributing on an evaporative surface with temperature of 190-245 DEG C through a distributor, wherein the vacuum degree ranges from 5Pa to 40 Pa; cooling light component pigment to 35-42 DEG C through a built-in condenser, wherein the cooled light component pigment flows in a light component collection tank and heavy components directly enter a heavy component collection tank; increasing the temperature of the heavy components to 230-260 DEG C through the heat exchanger, sending the heavy components to the molecular still, evenly distributing the material on the evaporative surface with temperature of 300-320 DEG C through the distributor under the vacuum degree of 0.1-5Pa, cooling light components to 35-42 DEG C through the built-in condenser, wherein the cooled light components flow in a decolored oil collection tank and the heavy components directly enter the heavy component collection tank. The grease decoloring method can be widely applied to the edible, cosmetic and fine chemical engineering fields.

Description

The decoloring method of grease
Technical field
The present invention relates to a kind of decoloring method, specifically the decoloring method of grease.
Background technology
The lustre index of grease is one of characteristic index of estimating its quality, and is in particular for the grease of edible, makeup and field of fine chemical purposes, just more strict to the requirement of its color and luster.Under the identical prerequisite of other indexs, the grease that color and luster is more shallow, more welcome.At present, the decoloring method of grease mainly contains following several: absorption method, chemical method and chromatography.Absorption method is discoloring agent by sorbing materials such as carclazyte, diatomite, attapulgite, gacs mainly, under 105~120 ℃ of high temperature, vacuum 266Pa condition, mixes approximately after 20 minutes, through namely getting bleached oil behind the filter filtration discoloring agent with grease.This method is the decoloring method that generally adopt in present oil and fat refining field, but for some darker grease of rear color and luster that comes unstuck, the decolorizing effect of this method is unsatisfactory, and can cause the loss of neutral oil in the decolorization, yield is reduced, and simultaneously recycling or the harmless processing of useless discoloring agent also increased burden for producer.Chemical method is that the material of the strong oxidizing properties such as employing benzoyl peroxide, hydrogen peroxide is auxiliary agent, pigment oxidation is reached the purpose of decolouring, is mainly used at present the decolouring of industrial grease.Grease after the main drawback of this method is to decolour is easy to inverse after pyroprocessing, directly affect its normal use, and in addition, this method can only be confined to the decolouring purposes of commercial grease, forbids to use for fields such as edible, makeup.The chromatography decolouring is widely used in laboratory scale grease-decolor at present, it separates according to the pigment principle different from grease retention time in chromatography column, the filling effect of pillar is most important to decolorizing effect, and main drawback is that the dress post to chromatography column requires height, treatment capacity is too little, cost is high, the cycle is long, be difficult to industrial applications.
Summary of the invention
The present invention overcomes the deficiency of above-mentioned technology, the decolouring that utilizes physical method to realize grease is provided, and the high-temperature time of whole process is extremely short, and product color surpasses the standard of GB primary oil, the product yield is high, does not add the decoloring method of the grease of any auxiliary agent, non-wastewater discharge.
In order to solve the problem of above-mentioned technology, the present invention is achieved by the following technical solutions: stock oil is warmed up to 150~170 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 190~245 ℃, vacuum tightness is at 5~40Pa, the light constituent pigment cools to 35~42 ℃ through built-in condenser, flow into the light constituent holding tank, recombinating to divide directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 230~260 ℃, enter molecular still, in generating surface, the temperature of generating surface is at 300~320 ℃ through the distributor uniform distribution for material, vacuum tightness is at 0.1~5Pa, light constituent cools to 35~42 ℃ through built-in condenser, flows into the bleached oil holding tank, recombinates to divide directly entering a restructuring minute holding tank.
Compared with prior art, beneficial effect advantage of the present invention is: utilize physical method to realize the decolouring of grease, the high-temperature time of whole process is extremely short, and product color surpasses the standard of GB primary oil, and the product yield is high, does not add any auxiliary agent, non-wastewater discharge.
Embodiment
Below in conjunction with embodiment the present invention is described in further detail:
Embodiment 1
The Oleum Gossypii semen that comes unstuck is warmed up to 150 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 190 ℃, vacuum tightness is at 5Pa, and the light constituent pigment cools to 35 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 230 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 300 ℃, and vacuum tightness is at 1Pa, and light constituent cools to 36 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 2
The Semen Maydis oil that comes unstuck is warmed up to 155 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 200 ℃, vacuum tightness is at 15Pa, and the light constituent pigment cools to 37 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 235 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 305 ℃, and vacuum tightness is at 2Pa, and light constituent cools to 38 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 3
The soybean oil of coming unstuck is warmed up to 160 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 215 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 240 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 310 ℃, and vacuum tightness is at 5Pa, and light constituent cools to 40 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 4
The peanut oil that comes unstuck is warmed up to 170 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 245 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 250 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 315 ℃, and vacuum tightness is at 4Pa, and light constituent cools to 42 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 5
The sesame oil that comes unstuck is warmed up to 165 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 230 ℃, vacuum tightness is at 35Pa, and the light constituent pigment cools to 39 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 250 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 306 ℃, and vacuum tightness is at 2.5Pa, and light constituent cools to 35 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 6
The sunflower seed oil that comes unstuck is warmed up to 159 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 220 ℃, vacuum tightness is at 30Pa, and the light constituent pigment cools to 35 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 230 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 320 ℃, and vacuum tightness is at 3.1Pa, and light constituent cools to 35 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 7
The plam oil that comes unstuck is warmed up to 150 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 190 ℃, vacuum tightness is at 5Pa, and the light constituent pigment cools to 35 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 230 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 300 ℃, and vacuum tightness is at 1Pa, and light constituent cools to 36 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 8
The rapeseed oil that comes unstuck is warmed up to 155 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 200 ℃, vacuum tightness is at 15Pa, and the light constituent pigment cools to 37 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 260 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 315 ℃, and vacuum tightness is at 2Pa, and light constituent cools to 38 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 9
The raisin seed oil that comes unstuck is warmed up to 160 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 215 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 240 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 310 ℃, and vacuum tightness is at 5Pa, and light constituent cools to 40 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 10
The walnut oil that comes unstuck is warmed up to 170 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 245 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 250 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 310 ℃, and vacuum tightness is at 4Pa, and light constituent cools to 42 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 11
The camellia seed oil that comes unstuck is warmed up to 165 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 230 ℃, vacuum tightness is at 35Pa, and the light constituent pigment cools to 39 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 238 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 306 ℃, and vacuum tightness is at 2.5Pa, and light constituent cools to 35 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 12
The safflower oil of coming unstuck is warmed up to 159 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 220 ℃, vacuum tightness is at 30Pa, and the light constituent pigment cools to 35 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 230 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 304 ℃, and vacuum tightness is at 3.1Pa, and light constituent cools to 35 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 13
The Castor oil that comes unstuck is warmed up to 160 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 215 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 240 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 310 ℃, and vacuum tightness is at 5Pa, and light constituent cools to 40 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 14
The Rice pollard oil that comes unstuck is warmed up to 170 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 245 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 260 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 320 ℃, and vacuum tightness is at 4Pa, and light constituent cools to 42 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 15
The wheatgerm oil that comes unstuck is warmed up to 165 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 230 ℃, vacuum tightness is at 35Pa, and the light constituent pigment cools to 39 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 238 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 306 ℃, and vacuum tightness is at 2.5Pa, and light constituent cools to 35 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 16
The Canola Oil that comes unstuck is warmed up to 159 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 220 ℃, vacuum tightness is at 30Pa, and the light constituent pigment cools to 35 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 230 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 304 ℃, and vacuum tightness is at 3.1Pa, and light constituent cools to 35 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 17
The Oleum Cocois that comes unstuck is warmed up to 150 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 190 ℃, vacuum tightness is at 5Pa, and the light constituent pigment cools to 35 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 230 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 300 ℃, and vacuum tightness is at 1Pa, and light constituent cools to 36 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 18
Little algae oil that comes unstuck is warmed up to 155 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 200 ℃, vacuum tightness is at 15Pa, and the light constituent pigment cools to 37 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 235 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 305 ℃, and vacuum tightness is at 2Pa, and light constituent cools to 38 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 19
The microbial oil that comes unstuck is warmed up to 160 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 215 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 240 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 310 ℃, and vacuum tightness is at 5Pa, and light constituent cools to 40 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 20
The lard oil that comes unstuck is warmed up to 170 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 225 ℃, vacuum tightness is at 20Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 250 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 300 ℃, and vacuum tightness is at 4Pa, and light constituent cools to 42 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 21
The tomato seed oil that comes unstuck is warmed up to 150 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 190 ℃, vacuum tightness is at 5Pa, and the light constituent pigment cools to 35 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 230 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 300 ℃, and vacuum tightness is at 1Pa, and light constituent cools to 36 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 22
The peony seed oil that comes unstuck is warmed up to 155 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 200 ℃, vacuum tightness is at 15Pa, and the light constituent pigment cools to 37 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 235 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 305 ℃, and vacuum tightness is at 2Pa, and light constituent cools to 38 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 23
The linseed oil that comes unstuck is warmed up to 160 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 215 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 240 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 310 ℃, and vacuum tightness is at 5Pa, and light constituent cools to 40 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 24
The rubber seed oil that comes unstuck is warmed up to 170 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 245 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 250 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 310 ℃, and vacuum tightness is at 4Pa, and light constituent cools to 42 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 25
The macadamia nut oil that comes unstuck is warmed up to 165 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 230 ℃, vacuum tightness is at 35Pa, and the light constituent pigment cools to 39 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 238 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 306 ℃, and vacuum tightness is at 2.5Pa, and light constituent cools to 35 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 26
The degummed oil tea-seed oil is warmed up to 159 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 220 ℃, vacuum tightness is at 30Pa, and the light constituent pigment cools to 35 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 230 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 304 ℃, and vacuum tightness is at 3.1Pa, and light constituent cools to 35 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 27
The butter that come unstuck are warmed up to 150 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 190 ℃, vacuum tightness is at 5Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 230 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 300 ℃, and vacuum tightness is at 1Pa, and light constituent cools to 42 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 28
The sheep oil that comes unstuck is warmed up to 155 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 200 ℃, vacuum tightness is at 15Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 235 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 305 ℃, and vacuum tightness is at 2Pa, and light constituent cools to 42 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 29
The fish oil that comes unstuck is warmed up to 150 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 190 ℃, vacuum tightness is at 5Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 230 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 300 ℃, and vacuum tightness is at 1Pa, and light constituent cools to 42 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank
Embodiment 30
The chicken fat that comes unstuck is warmed up to 155 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 200 ℃, vacuum tightness is at 15Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 235 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 305 ℃, and vacuum tightness is at 2Pa, and light constituent cools to 42 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 31
The duck oil that comes unstuck is warmed up to 155 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 200 ℃, vacuum tightness is at 15Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 235 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 305 ℃, and vacuum tightness is at 2Pa, and light constituent cools to 42 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 32
The Fructus Zanthoxyli oil that comes unstuck is warmed up to 150 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 190 ℃, vacuum tightness is at 5Pa, and the light constituent pigment cools to 35 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 230 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 300 ℃, and vacuum tightness is at 1Pa, and light constituent cools to 36 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 33
The Oleum Verniciae fordii that comes unstuck is warmed up to 155 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 200 ℃, vacuum tightness is at 15Pa, and the light constituent pigment cools to 37 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 235 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 305 ℃, and vacuum tightness is at 2Pa, and light constituent cools to 38 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 34
Degummed flax seeds oil is warmed up to 160 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 215 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 240 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 310 ℃, and vacuum tightness is at 5Pa, and light constituent cools to 40 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 35
The hempseed oil that comes unstuck is warmed up to 170 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 245 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 250 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 310 ℃, and vacuum tightness is at 4Pa, and light constituent cools to 42 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 36
The tallowseed oil that comes unstuck is warmed up to 155 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 200 ℃, vacuum tightness is at 15Pa, and the light constituent pigment cools to 37 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 235 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 305 ℃, and vacuum tightness is at 2Pa, and light constituent cools to 38 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 37
The Walnut oil. that comes unstuck is warmed up to 160 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 215 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 240 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 310 ℃, and vacuum tightness is at 5Pa, and light constituent cools to 40 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 38
The shinyleaf yellowhorn oil that comes unstuck is warmed up to 170 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 245 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 250 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 310 ℃, and vacuum tightness is at 4Pa, and light constituent cools to 42 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 39
The samara oil that comes unstuck is warmed up to 170 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 245 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 250 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 310 ℃, and vacuum tightness is at 4Pa, and light constituent cools to 42 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 40
The barbadosnut seed oil that comes unstuck is warmed up to 155 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 200 ℃, vacuum tightness is at 15Pa, and the light constituent pigment cools to 37 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 235 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 305 ℃, and vacuum tightness is at 2Pa, and light constituent cools to 38 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 41
The carclazyte oil that comes unstuck is warmed up to 160 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 215 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 240 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 310 ℃, and vacuum tightness is at 5Pa, and light constituent cools to 40 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 42
The changing food waste oil that comes unstuck is warmed up to 170 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 245 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 250 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 310 ℃, and vacuum tightness is at 4Pa, and light constituent cools to 42 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 43
The palm-kernel oil that comes unstuck is warmed up to 160 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 215 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 240 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 310 ℃, and vacuum tightness is at 5Pa, and light constituent cools to 40 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 44
The Malus spectabilis oil that comes unstuck is warmed up to 170 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 245 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 250 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 310 ℃, and vacuum tightness is at 4Pa, and light constituent cools to 42 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 45
The seed of Radix Dauci Sativae oil that comes unstuck is warmed up to 165 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 230 ℃, vacuum tightness is at 35Pa, and the light constituent pigment cools to 39 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 238 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 306 ℃, and vacuum tightness is at 2.5Pa, and light constituent cools to 35 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 46
The Prunus amygdalus oil that comes unstuck is warmed up to 159 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 220 ℃, vacuum tightness is at 30Pa, and the light constituent pigment cools to 35 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 230 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 304 ℃, and vacuum tightness is at 3.1Pa, and light constituent cools to 35 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 47
The lacquer tree seed oil that comes unstuck is warmed up to 160 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 215 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 240 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 310 ℃, and vacuum tightness is at 5Pa, and light constituent cools to 40 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 48
The Oil of Xanthium Sibiricum Seed that comes unstuck is warmed up to 170 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 245 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 250 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 310 ℃, and vacuum tightness is at 4Pa, and light constituent cools to 42 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 49
The camphor tree seed oil that comes unstuck is warmed up to 165 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 230 ℃, vacuum tightness is at 35Pa, and the light constituent pigment cools to 39 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 238 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 306 ℃, and vacuum tightness is at 2.5Pa, and light constituent cools to 35 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 50
The Oleum Tiglii that comes unstuck is warmed up to 159 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 220 ℃, vacuum tightness is at 30Pa, and the light constituent pigment cools to 35 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 230 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 304 ℃, and vacuum tightness is at 3.1Pa, and light constituent cools to 35 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 51
The fennel seed oil that comes unstuck is warmed up to 160 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 215 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 240 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 310 ℃, and vacuum tightness is at 5Pa, and light constituent cools to 40 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 52
The pumpkin-seed oil that comes unstuck is warmed up to 170 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 245 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 250 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 310 ℃, and vacuum tightness is at 4Pa, and light constituent cools to 42 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 53
The tobacco-seed oil that comes unstuck is warmed up to 160 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 215 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 240 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 310 ℃, and vacuum tightness is at 5Pa, and light constituent cools to 40 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 54
The China tree seed oil that comes unstuck is warmed up to 170 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 245 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 250 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 310 ℃, and vacuum tightness is at 4Pa, and light constituent cools to 42 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 55
The dog bone seeds of trees oil that comes unstuck is warmed up to 165 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 230 ℃, vacuum tightness is at 35Pa, and the light constituent pigment cools to 39 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 238 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 306 ℃, and vacuum tightness is at 2.5Pa, and light constituent cools to 35 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 56
The fragrant fruit oil that comes unstuck is warmed up to 170 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 245 ℃, vacuum tightness is at 40Pa, and the light constituent pigment cools to 42 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 250 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 310 ℃, and vacuum tightness is at 4Pa, and light constituent cools to 42 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.
Embodiment 57
The whale oil that comes unstuck is warmed up to 165 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 230 ℃, vacuum tightness is at 35Pa, and the light constituent pigment cools to 39 ℃ through built-in condenser, flows into the light constituent holding tank, recombinate to divide and directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 238 ℃, enters molecular still, material through the distributor uniform distribution in generating surface, the temperature of generating surface is at 306 ℃, and vacuum tightness is at 2.5Pa, and light constituent cools to 35 ℃ through built-in condenser, flow into the bleached oil holding tank, recombinating to divide directly entering a restructuring minute holding tank.

Claims (1)

1. the decoloring method of a grease, it is characterized in that: stock oil is warmed up to 150~170 ℃ through interchanger, then enter molecular still, through the distributor uniform distribution in generating surface, the temperature of generating surface is at 190~245 ℃, vacuum tightness is at 5~40Pa, the light constituent pigment cools to 35~42 ℃ through built-in condenser, flow into the light constituent holding tank, recombinating to divide directly entering a restructuring minute holding tank, then, restructuring lease making interchanger is warming up to 230~260 ℃, enter molecular still, in generating surface, the temperature of generating surface is at 300~320 ℃ through the distributor uniform distribution for material, vacuum tightness is at 0.1~5Pa, light constituent cools to 35~42 ℃ through built-in condenser, flows into the bleached oil holding tank, recombinates to divide directly entering a restructuring minute holding tank.
CN201210486651.7A 2012-11-27 2012-11-27 Grease decoloring method Active CN102994225B (en)

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CN103805337A (en) * 2014-01-10 2014-05-21 陈汉卿 Rice bran oil refining method
CN103805338A (en) * 2014-01-10 2014-05-21 陈汉卿 Short-path distillation production method and short-path distiller for increasing unsaturated fatty acid content of vegetable oil

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Publication number Priority date Publication date Assignee Title
CN103740462A (en) * 2014-01-10 2014-04-23 陈汉卿 Oil refining method
CN103805337A (en) * 2014-01-10 2014-05-21 陈汉卿 Rice bran oil refining method
CN103805338A (en) * 2014-01-10 2014-05-21 陈汉卿 Short-path distillation production method and short-path distiller for increasing unsaturated fatty acid content of vegetable oil
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