CN102994225B - Grease decoloring method - Google Patents

Grease decoloring method Download PDF

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Publication number
CN102994225B
CN102994225B CN201210486651.7A CN201210486651A CN102994225B CN 102994225 B CN102994225 B CN 102994225B CN 201210486651 A CN201210486651 A CN 201210486651A CN 102994225 B CN102994225 B CN 102994225B
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holding tank
generating surface
heavy constituent
constituent
temperature
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CN102994225A (en
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陈汉卿
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Abstract

The invention discloses a grease decoloring method, belonging to the technical field of refining grease and used for solving the problems in grease decoloring that high temperature time is long, the product yield is low, and auxiliaries are in need and sewage is discharged. The grease decoloring method comprises the steps: increasing temperature of raw material oil to 150-170 DEG C through a heat exchanger, then sending the raw material oil into a molecular still, and evenly distributing on an evaporative surface with temperature of 190-245 DEG C through a distributor, wherein the vacuum degree ranges from 5Pa to 40 Pa; cooling light component pigment to 35-42 DEG C through a built-in condenser, wherein the cooled light component pigment flows in a light component collection tank and heavy components directly enter a heavy component collection tank; increasing the temperature of the heavy components to 230-260 DEG C through the heat exchanger, sending the heavy components to the molecular still, evenly distributing the material on the evaporative surface with temperature of 300-320 DEG C through the distributor under the vacuum degree of 0.1-5Pa, cooling light components to 35-42 DEG C through the built-in condenser, wherein the cooled light components flow in a decolored oil collection tank and the heavy components directly enter the heavy component collection tank. The grease decoloring method can be widely applied to the edible, cosmetic and fine chemical engineering fields.

Description

The decoloring method of grease
Technical field
The present invention relates to a kind of decoloring method, specifically the decoloring method of grease.
Background technology
The lustre index of grease is one of characteristic index of evaluating its quality, in particular for the grease of edible, makeup and field of fine chemical purposes, just more strict to the requirement of its color and luster.Under the identical prerequisite of other indexs, the grease that color and luster is more shallow, more welcome.At present, the decoloring method of grease mainly contains several as follows: absorption method, chemical method and chromatography.Absorption method is mainly discoloring agent by sorbing materials such as carclazyte, diatomite, attapulgite, gacs, under 105~120 DEG C of high temperature, vacuum 266Pa condition, mixes after approximately 20 minutes with grease, after filter filters discoloring agent, obtains bleached oil.This method is the decoloring method that current oil and fat refining field generally adopts, but the darker grease of color and luster after coming unstuck for some, the decolorizing effect of this method is unsatisfactory, and in decolorization, can cause the loss of neutral oil, yield is reduced, and the recycling of useless discoloring agent or harmless processing are also for producer has increased burden simultaneously.Chemical method is that the material of the strong oxidizing properties such as employing benzoyl peroxide, hydrogen peroxide is auxiliary agent, pigment oxidation is reached to the object of decolouring, is mainly used at present the decolouring of industrial grease.The main drawback of this method is that the grease after decolouring is easy to inverse after pyroprocessing, directly affects it and normally uses, and in addition, this method can only be confined to the decolouring purposes of commercial grease, forbids to use for fields such as edible, makeup.Chromatography decolouring is widely used in laboratory scale grease-decolor at present, it carries out separation according to the pigment principle different from grease retention time in chromatography column, the filling effect of pillar is most important to decolorizing effect, main drawback be to the dress post of chromatography column require height, treatment capacity is too little, cost is high, the cycle is long, be difficult to industrial applications.
Summary of the invention
The present invention overcomes the deficiency of above-mentioned technology, the decolouring that utilizes physical method to realize grease is provided, and the high-temperature time of whole process is extremely short, and product color exceedes the standard of GB primary oil, product yield is high, does not add the decoloring method of the grease of any auxiliary agent, non-wastewater discharge.
In order to solve the problem of above-mentioned technology, the present invention is achieved by the following technical solutions: stock oil is warmed up to 150~170 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 190~245 DEG C, vacuum tightness is at 5~40Pa, light constituent pigment cools to 35~42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 230~260 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 300~320 DEG C, vacuum tightness is at 0.1~5Pa, light constituent cools to 35~42 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Compared with prior art, beneficial effect advantage of the present invention is: utilize physical method to realize the decolouring of grease, the high-temperature time of whole process is extremely short, and product color exceedes the standard of GB primary oil, and product yield is high, does not add any auxiliary agent, non-wastewater discharge.
Embodiment
Below in conjunction with embodiment, the present invention is described in further detail:
Embodiment 1
The Oleum Gossypii semen that comes unstuck is warmed up to 150 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 190 DEG C, vacuum tightness is at 5Pa, light constituent pigment cools to 35 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 230 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 300 DEG C, vacuum tightness is at 1Pa, light constituent cools to 36 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 2
The Semen Maydis oil that comes unstuck is warmed up to 155 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 200 DEG C, vacuum tightness is at 15Pa, light constituent pigment cools to 37 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 235 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 305 DEG C, vacuum tightness is at 2Pa, light constituent cools to 38 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 3
The soybean oil of coming unstuck is warmed up to 160 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 215 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 240 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 310 DEG C, vacuum tightness is at 5Pa, light constituent cools to 40 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 4
The peanut oil that comes unstuck is warmed up to 170 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 245 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 250 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 315 DEG C, vacuum tightness is at 4Pa, light constituent cools to 42 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 5
The sesame oil that comes unstuck is warmed up to 165 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 230 DEG C, vacuum tightness is at 35Pa, light constituent pigment cools to 39 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 250 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 306 DEG C, vacuum tightness is at 2.5Pa, light constituent cools to 35 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 6
The sunflower seed oil that comes unstuck is warmed up to 159 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 220 DEG C, vacuum tightness is at 30Pa, light constituent pigment cools to 35 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 230 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 320 DEG C, vacuum tightness is at 3.1Pa, light constituent cools to 35 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 7
The plam oil that comes unstuck is warmed up to 150 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 190 DEG C, vacuum tightness is at 5Pa, light constituent pigment cools to 35 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 230 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 300 DEG C, vacuum tightness is at 1Pa, light constituent cools to 36 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 8
The rapeseed oil that comes unstuck is warmed up to 155 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 200 DEG C, vacuum tightness is at 15Pa, light constituent pigment cools to 37 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 260 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 315 DEG C, vacuum tightness is at 2Pa, light constituent cools to 38 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 9
The raisin seed oil that comes unstuck is warmed up to 160 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 215 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 240 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 310 DEG C, vacuum tightness is at 5Pa, light constituent cools to 40 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 10
The walnut oil that comes unstuck is warmed up to 170 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 245 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 250 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 310 DEG C, vacuum tightness is at 4Pa, light constituent cools to 42 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 11
The camellia seed oil that comes unstuck is warmed up to 165 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 230 DEG C, vacuum tightness is at 35Pa, light constituent pigment cools to 39 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 238 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 306 DEG C, vacuum tightness is at 2.5Pa, light constituent cools to 35 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 12
The safflower oil of coming unstuck is warmed up to 159 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 220 DEG C, vacuum tightness is at 30Pa, light constituent pigment cools to 35 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 230 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 304 DEG C, vacuum tightness is at 3.1Pa, light constituent cools to 35 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 13
The Castor oil that comes unstuck is warmed up to 160 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 215 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 240 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 310 DEG C, vacuum tightness is at 5Pa, light constituent cools to 40 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 14
The Rice pollard oil that comes unstuck is warmed up to 170 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 245 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 260 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 320 DEG C, vacuum tightness is at 4Pa, light constituent cools to 42 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 15
The wheatgerm oil that comes unstuck is warmed up to 165 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 230 DEG C, vacuum tightness is at 35Pa, light constituent pigment cools to 39 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 238 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 306 DEG C, vacuum tightness is at 2.5Pa, light constituent cools to 35 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 16
The Canola Oil that comes unstuck is warmed up to 159 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 220 DEG C, vacuum tightness is at 30Pa, light constituent pigment cools to 35 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 230 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 304 DEG C, vacuum tightness is at 3.1Pa, light constituent cools to 35 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 17
The Oleum Cocois that comes unstuck is warmed up to 150 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 190 DEG C, vacuum tightness is at 5Pa, light constituent pigment cools to 35 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 230 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 300 DEG C, vacuum tightness is at 1Pa, light constituent cools to 36 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 18
Micro-algae oil that comes unstuck is warmed up to 155 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 200 DEG C, vacuum tightness is at 15Pa, light constituent pigment cools to 37 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 235 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 305 DEG C, vacuum tightness is at 2Pa, light constituent cools to 38 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 19
The microbial oil that comes unstuck is warmed up to 160 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 215 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 240 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 310 DEG C, vacuum tightness is at 5Pa, light constituent cools to 40 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 20
The lard oil that comes unstuck is warmed up to 170 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 225 DEG C, vacuum tightness is at 20Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 250 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 300 DEG C, vacuum tightness is at 4Pa, light constituent cools to 42 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 21
The tomato seed oil that comes unstuck is warmed up to 150 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 190 DEG C, vacuum tightness is at 5Pa, light constituent pigment cools to 35 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 230 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 300 DEG C, vacuum tightness is at 1Pa, light constituent cools to 36 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 22
The peony seed oil that comes unstuck is warmed up to 155 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 200 DEG C, vacuum tightness is at 15Pa, light constituent pigment cools to 37 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 235 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 305 DEG C, vacuum tightness is at 2Pa, light constituent cools to 38 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 23
The linseed oil that comes unstuck is warmed up to 160 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 215 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 240 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 310 DEG C, vacuum tightness is at 5Pa, light constituent cools to 40 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 24
The rubber seed oil that comes unstuck is warmed up to 170 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 245 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 250 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 310 DEG C, vacuum tightness is at 4Pa, light constituent cools to 42 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 25
The macadamia nut oil that comes unstuck is warmed up to 165 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 230 DEG C, vacuum tightness is at 35Pa, light constituent pigment cools to 39 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 238 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 306 DEG C, vacuum tightness is at 2.5Pa, light constituent cools to 35 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 26
Degummed oil tea-seed oil is warmed up to 159 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 220 DEG C, vacuum tightness is at 30Pa, light constituent pigment cools to 35 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 230 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 304 DEG C, vacuum tightness is at 3.1Pa, light constituent cools to 35 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 27
The butter that come unstuck are warmed up to 150 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 190 DEG C, vacuum tightness is at 5Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 230 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 300 DEG C, vacuum tightness is at 1Pa, light constituent cools to 42 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 28
The sheep oil that comes unstuck is warmed up to 155 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 200 DEG C, vacuum tightness is at 15Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 235 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 305 DEG C, vacuum tightness is at 2Pa, light constituent cools to 42 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 29
The fish oil that comes unstuck is warmed up to 150 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 190 DEG C, vacuum tightness is at 5Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 230 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 300 DEG C, vacuum tightness is at 1Pa, light constituent cools to 42 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank
Embodiment 30
The chicken fat that comes unstuck is warmed up to 155 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 200 DEG C, vacuum tightness is at 15Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 235 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 305 DEG C, vacuum tightness is at 2Pa, light constituent cools to 42 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 31
The duck oil that comes unstuck is warmed up to 155 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 200 DEG C, vacuum tightness is at 15Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 235 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 305 DEG C, vacuum tightness is at 2Pa, light constituent cools to 42 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 32
The Fructus Zanthoxyli oil that comes unstuck is warmed up to 150 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 190 DEG C, vacuum tightness is at 5Pa, light constituent pigment cools to 35 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 230 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 300 DEG C, vacuum tightness is at 1Pa, light constituent cools to 36 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 33
The Oleum Verniciae fordii that comes unstuck is warmed up to 155 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 200 DEG C, vacuum tightness is at 15Pa, light constituent pigment cools to 37 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 235 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 305 DEG C, vacuum tightness is at 2Pa, light constituent cools to 38 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 34
Degummed flax seeds oil is warmed up to 160 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 215 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 240 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 310 DEG C, vacuum tightness is at 5Pa, light constituent cools to 40 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 35
The hempseed oil that comes unstuck is warmed up to 170 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 245 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 250 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 310 DEG C, vacuum tightness is at 4Pa, light constituent cools to 42 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 36
The tallowseed oil that comes unstuck is warmed up to 155 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 200 DEG C, vacuum tightness is at 15Pa, light constituent pigment cools to 37 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 235 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 305 DEG C, vacuum tightness is at 2Pa, light constituent cools to 38 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 37
The Walnut oil. that comes unstuck is warmed up to 160 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 215 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 240 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 310 DEG C, vacuum tightness is at 5Pa, light constituent cools to 40 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 38
The shinyleaf yellowhorn oil that comes unstuck is warmed up to 170 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 245 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 250 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 310 DEG C, vacuum tightness is at 4Pa, light constituent cools to 42 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 39
The samara oil that comes unstuck is warmed up to 170 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 245 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 250 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 310 DEG C, vacuum tightness is at 4Pa, light constituent cools to 42 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 40
The barbadosnut seed oil that comes unstuck is warmed up to 155 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 200 DEG C, vacuum tightness is at 15Pa, light constituent pigment cools to 37 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 235 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 305 DEG C, vacuum tightness is at 2Pa, light constituent cools to 38 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 41
The carclazyte oil that comes unstuck is warmed up to 160 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 215 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 240 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 310 DEG C, vacuum tightness is at 5Pa, light constituent cools to 40 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 42
The changing food waste oil that comes unstuck is warmed up to 170 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 245 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 250 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 310 DEG C, vacuum tightness is at 4Pa, light constituent cools to 42 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 43
The palm-kernel oil that comes unstuck is warmed up to 160 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 215 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 240 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 310 DEG C, vacuum tightness is at 5Pa, light constituent cools to 40 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 44
The Malus spectabilis oil that comes unstuck is warmed up to 170 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 245 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 250 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 310 DEG C, vacuum tightness is at 4Pa, light constituent cools to 42 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 45
The seed of Radix Dauci Sativae oil that comes unstuck is warmed up to 165 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 230 DEG C, vacuum tightness is at 35Pa, light constituent pigment cools to 39 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 238 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 306 DEG C, vacuum tightness is at 2.5Pa, light constituent cools to 35 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 46
The Prunus amygdalus oil that comes unstuck is warmed up to 159 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 220 DEG C, vacuum tightness is at 30Pa, light constituent pigment cools to 35 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 230 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 304 DEG C, vacuum tightness is at 3.1Pa, light constituent cools to 35 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 47
The lacquer tree seed oil that comes unstuck is warmed up to 160 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 215 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 240 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 310 DEG C, vacuum tightness is at 5Pa, light constituent cools to 40 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 48
The Oil of Xanthium Sibiricum Seed that comes unstuck is warmed up to 170 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 245 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 250 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 310 DEG C, vacuum tightness is at 4Pa, light constituent cools to 42 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 49
The camphor tree seed oil that comes unstuck is warmed up to 165 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 230 DEG C, vacuum tightness is at 35Pa, light constituent pigment cools to 39 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 238 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 306 DEG C, vacuum tightness is at 2.5Pa, light constituent cools to 35 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 50
The Oleum Tiglii that comes unstuck is warmed up to 159 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 220 DEG C, vacuum tightness is at 30Pa, light constituent pigment cools to 35 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 230 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 304 DEG C, vacuum tightness is at 3.1Pa, light constituent cools to 35 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 51
The fennel seed oil that comes unstuck is warmed up to 160 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 215 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 240 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 310 DEG C, vacuum tightness is at 5Pa, light constituent cools to 40 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 52
The pumpkin-seed oil that comes unstuck is warmed up to 170 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 245 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 250 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 310 DEG C, vacuum tightness is at 4Pa, light constituent cools to 42 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 53
The tobacco-seed oil that comes unstuck is warmed up to 160 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 215 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 240 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 310 DEG C, vacuum tightness is at 5Pa, light constituent cools to 40 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 54
The China tree seed oil that comes unstuck is warmed up to 170 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 245 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 250 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 310 DEG C, vacuum tightness is at 4Pa, light constituent cools to 42 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 55
The dog bone seeds of trees oil that comes unstuck is warmed up to 165 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 230 DEG C, vacuum tightness is at 35Pa, light constituent pigment cools to 39 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 238 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 306 DEG C, vacuum tightness is at 2.5Pa, light constituent cools to 35 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 56
The fragrant fruit oil that comes unstuck is warmed up to 170 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 245 DEG C, vacuum tightness is at 40Pa, light constituent pigment cools to 42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 250 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 310 DEG C, vacuum tightness is at 4Pa, light constituent cools to 42 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
Embodiment 57
The whale oil that comes unstuck is warmed up to 165 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 230 DEG C, vacuum tightness is at 35Pa, light constituent pigment cools to 39 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 238 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 306 DEG C, vacuum tightness is at 2.5Pa, light constituent cools to 35 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.

Claims (1)

1. the decoloring method of a grease, it is characterized in that: the stock oil that comes unstuck is warmed up to 150~170 DEG C through interchanger, then enter molecular still, through distributor uniform distribution in generating surface, the temperature of generating surface is at 190~245 DEG C, vacuum tightness is at 5~40Pa, light constituent pigment cools to 35~42 DEG C through built-in condenser, flow into light constituent holding tank, heavy constituent directly enters heavy constituent holding tank, then, heavy constituent is warming up to 230~260 DEG C through interchanger, enter molecular still, material through distributor uniform distribution in generating surface, the temperature of generating surface is at 300~320 DEG C, vacuum tightness is at 0.1~5Pa, light constituent cools to 35~42 DEG C through built-in condenser, flow into bleached oil holding tank, heavy constituent directly enters heavy constituent holding tank.
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