CN102993937A - Nanoscale wall surface permeation curing material and preparation method thereof - Google Patents
Nanoscale wall surface permeation curing material and preparation method thereof Download PDFInfo
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- CN102993937A CN102993937A CN2012105595476A CN201210559547A CN102993937A CN 102993937 A CN102993937 A CN 102993937A CN 2012105595476 A CN2012105595476 A CN 2012105595476A CN 201210559547 A CN201210559547 A CN 201210559547A CN 102993937 A CN102993937 A CN 102993937A
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Abstract
The invention relates to a nanoscale wall surface permeation curing material and a preparation method thereof. The nanoscale wall surface permeation curing material comprises the following components in percentage by weight: 60-80% of waterborne emulsion, 10-30% of deionized water, 0.5-0.8% of dispersing agent, 0.1-0.2% of AMP-95 aid, 3.5-4% of film forming agent, 0.05-0.1% of antifoaming agent, 0.1-0.15% of bactericide, 0.8-1.5% of thickening agent and 0.1-0.2% of curing agent. Through the invention, by adopting the nanoscale wall surface permeation curing material provided by the invention as an interior and exterior wall permeation curing material, when applying putty and leveling, the curing material can be directly applied before applying emulsion paint without scraping putty, mixing the putty with glue and then performing blade coating of the putty powder and applying the emulsion paint, thereby solving the problem of putty leveling, saving the putty powder and glue and saving processes and labor.
Description
Technical field
The present invention relates to a kind of material of construction, be specifically related to a kind of interior outer surface of wall infiltration solidification material and preparation method thereof.
Background technology
In the interior exterior wall brushing process of tradition, in the time of Puttying, can be because levelling to be polished to the metope of having scraped putty, the shedding phenomenon can appear in putty, at this time just putty powder and glue need to be mixed, again blade coating is one time, and carries out levelling, is coated with emulsion paint again, be a kind of very large waste for putty powder and glue like this, and wasted artificial and time; After interior exterior wall has been grown duration of service, need renovation, also above-mentioned problem can occur.
Exist high infiltration interfacial agents to solve the problems referred to above in the prior art, but time of drying is long, water tolerance, alkali resistance, abrasion resistance technical indicator all have much room for improvement.
Summary of the invention
In order to solve problems of the prior art, the present invention aims to provide a kind of again blade coating of putty powder and glue that need not to use, and permeablely enters metope and small particle is glued together, and reaches interior outer surface of wall infiltration solidification material of not shedding effect and preparation method thereof.
Technical scheme of the present invention is:
Nano level metope infiltration solidification material, component and weight percent are water-based emulsion 60-80%, deionized water 10-30%, dispersion agent 0.5-0.8%, AMP-95 auxiliary agent 0.1-0.2%, membrane-forming agent 3.5-4%, defoamer 0.05-0.1%, sterilant 0.1-0.15%, thickening material 0.8-1.5%, solidifying agent 0.1-0.2%.
Described water-based emulsion is at least a of aqueous polyurethane, waterborne polyester solution.
Described dispersion agent is at least a of fatty acid, aliphatic amide type or ester class.
Described membrane-forming agent is at least a of divinyl ethylene glycol monobutyl ether, vinyl ethylene glycol butyl ether.
Described defoamer is organo-siloxane, polyethers, silicon, ether grafting, contains at least a of amine, imines or amides.
Described sterilant is at least a of halogen, oxidants, surfactant-based, heterocyclic gas or pure series bactericidal agent.
Described thickening material is at least a of methylcellulose gum, carboxymethyl cellulose, Natvosol, Vltra tears, polyurethanes thickening material, wilkinite, attapulgite or pure aluminium silicate.
Described solidifying agent is at least a of aliphatic amide, aliphatic cyclic amine, aromatic amine, acid anhydrides, tertiary amine or polyamide resin solidifying agent.
A kind of nano level metope infiltration solidification material preparation method for preparing the steps include:
1) with measuring apparatus with proportionally accurate measurement of material;
2) under stirring, the 600-800rpm rotating speed will stir 5-10min in deionized water, the thickening material input mixing and blending machine;
3) rotating speed is transferred to the 900-1000rpm rotating speed, in mixing and blending machine, drop into the AMP-95 auxiliary agent, stir 5-10min;
4) after 1-8min AMP-95 auxiliary agent is uniformly dispersed, rotating speed is transferred to 1500-1700rpm, input dispersion agent, defoamer stir 5-10min in mixing and blending machine;
5) rotating speed is transferred to 1000-1500rpm, in mixing and blending machine, drop into membrane-forming agent, sterilant, in mixing and blending machine, stir 5-10min;
6) rotating speed is transferred to 800-1000rpm, in mixing and blending machine, drop into water-based emulsion and solidifying agent, in mixing and blending machine, stir 5-30min and get product.
The invention has the beneficial effects as follows:
Nano level metope infiltration solidification material of the present invention is as interior exterior wall infiltration solidification material, in the Puttying levelling, do not need putty is wiped off, and glue mixes, again blade coating putty powder again, then be coated with emulsion paint, but can directly be coated with solidify material, and then can be coated with emulsion paint, the invention solves the problem of putty levelling, save the use of putty powder and glue, also saved operation and artificial;
Nano level metope infiltration solidification excellent material performance of the present invention, 1 hour time of drying, abrasion resistance can reach 800 times without unusual in 60 hours in alkaline resistance test without unusual in 100 hours in water tolerance test, and performance is better than the height infiltration interfacial agents of prior art.
Embodiment
The present invention is described in more detail below in conjunction with embodiment.
Embodiment 1:
1) be waterborne polyester emulsion 80% with material according to weight percent with measuring apparatus, deionized water 14.3%, fatty acid dispersion agent 0.5%, AMP-95 auxiliary agent 0.1%, membrane-forming agent divinyl ethylene glycol monobutyl ether 4%, defoamer organo-siloxane 0.1%, oxidants sterilant 0.1%, polyurethanes thickening material 0.8%, 0.1% accurate measurement of solidifying agent aliphatic amide;
2) under stirring, the 600rpm rotating speed will stir 5min in deionized water, the thickening material input mixing and blending machine;
3) rotating speed is transferred to the 900rpm rotating speed, in mixing and blending machine, drop into the AMP-95 auxiliary agent, stir 5min;
4) after 1min AMP-95 auxiliary agent is uniformly dispersed, rotating speed is transferred to 1500rpm, input dispersion agent, defoamer stir 5min in mixing and blending machine;
5) rotating speed is transferred to 1000rpm, in mixing and blending machine, drop into membrane-forming agent, sterilant, in mixing and blending machine, stir 5min;
6) rotating speed is transferred to 800rpm, in mixing and blending machine, drop into water-based emulsion and solidifying agent, in mixing and blending machine, stir 5min and get product.
Embodiment 2:
1) be aqueous polyurethane 64% with material according to weight percent with measuring apparatus, deionized water 30%, aliphatic amide type dispersion agent 0.5%, AMP-95 auxiliary agent 0.1%, membrane-forming agent vinyl ethylene glycol butyl ether 3.5%, defoamer polyethers 0.1%, heterocyclic gaseous disinfectant 0.1%, Natvosol thickening material 1.5%, 0.2% accurate measurement of solidifying agent acid anhydrides;
2) under stirring, the 800rpm rotating speed will stir 10min in deionized water, the thickening material input mixing and blending machine;
3) rotating speed is transferred to the 1000rpm rotating speed, in mixing and blending machine, drop into the AMP-95 auxiliary agent, stir 10min;
4) after 8min AMP-95 auxiliary agent is uniformly dispersed, rotating speed is transferred to 1700rpm, input dispersion agent, defoamer stir 10min in mixing and blending machine;
5) rotating speed is transferred to 1500rpm, in mixing and blending machine, drop into membrane-forming agent, sterilant, in mixing and blending machine, stir 10min;
6) rotating speed is transferred to 1000rpm, in mixing and blending machine, drop into water-based emulsion and solidifying agent, in mixing and blending machine, stir 30min and get product.
Embodiment 3:
1) be aqueous polyurethane emulsion 70% with material according to weight percent with measuring apparatus, deionized water 24.5%, ester class dispersion agent 0.5%, AMP-95 auxiliary agent 0.2%, membrane-forming agent divinyl ethylene glycol monobutyl ether 3.5%, amides defoamer 0.1%, halogen sterilant 0.1%, thickening material Vltra tears 1%, 0.1% accurate measurement of solidifying agent polyamide resin;
2) under stirring, the 700rpm rotating speed will stir 8min in deionized water, the thickening material input mixing and blending machine;
3) rotating speed is transferred to the 950rpm rotating speed, in mixing and blending machine, drop into the AMP-95 auxiliary agent, stir 8min;
4) after 5min AMP-95 auxiliary agent is uniformly dispersed, rotating speed is transferred to 1600rpm, input dispersion agent, defoamer stir 8min in mixing and blending machine;
5) rotating speed is transferred to 1200rpm, in mixing and blending machine, drop into membrane-forming agent, sterilant, in mixing and blending machine, stir 8min;
6) rotating speed is transferred to 900rpm, in mixing and blending machine, drop into water-based emulsion and solidifying agent, in mixing and blending machine, stir 20min and get product.
Following table is the technical indicator contrast table of nano level metope infiltration solidification material of the present invention and prior art medium to high permeable interfacial agents:
Claims (9)
1. nano level metope infiltration solidification material, component and weight percent are water-based emulsion 60-80%, deionized water 10-30%, dispersion agent 0.5-0.8%, AMP-95 auxiliary agent 0.1-0.2%, membrane-forming agent 3.5-4%, defoamer 0.05-0.1%, sterilant 0.1-0.15%, thickening material 0.8-1.5%, solidifying agent 0.1-0.2%.
2. nano level metope infiltration solidification material as claimed in claim 1 is characterized in that, described water-based emulsion is at least a of aqueous polyurethane, waterborne polyester solution.
3. nano level metope infiltration solidification material as claimed in claim 1 is characterized in that, described dispersion agent is at least a of fatty acid, aliphatic amide type or ester class.
4. nano level metope infiltration solidification material as claimed in claim 1 is characterized in that, described membrane-forming agent is at least a of divinyl ethylene glycol monobutyl ether, vinyl ethylene glycol butyl ether.
5. nano level metope infiltration solidification material as claimed in claim 1 is characterized in that, described defoamer is organo-siloxane, polyethers, silicon, ether grafting, contains at least a of amine, imines or amides.
6. nano level metope infiltration solidification material as claimed in claim 1 is characterized in that, described sterilant is at least a of halogen, oxidants, surfactant-based, heterocyclic gas or pure series bactericidal agent.
7. nano level metope infiltration solidification material as claimed in claim 1, it is characterized in that described thickening material is at least a of methylcellulose gum, carboxymethyl cellulose, Natvosol, Vltra tears, polyurethanes thickening material, wilkinite, attapulgite or pure aluminium silicate.
8. nano level metope infiltration solidification material as claimed in claim 1 is characterized in that, described solidifying agent is at least a of aliphatic amide, aliphatic cyclic amine, aromatic amine, acid anhydrides, tertiary amine or polyamide resin solidifying agent.
9. one kind prepares such as the described nano level metope of claim 1-8 infiltration solidification material preparation method, the steps include:
1) with measuring apparatus with proportionally accurate measurement of material;
2) under stirring, the 600-800rpm rotating speed will stir 5-10min in deionized water, the thickening material input mixing and blending machine;
3) rotating speed is transferred to the 900-1000rpm rotating speed, in mixing and blending machine, drop into the AMP-95 auxiliary agent, stir 5-10min;
4) after 1-8min AMP-95 auxiliary agent is uniformly dispersed, rotating speed is transferred to 1500-1700rpm, input dispersion agent, defoamer stir 5-10min in mixing and blending machine;
5) rotating speed is transferred to 1000-1500rpm, in mixing and blending machine, drop into membrane-forming agent, sterilant, in mixing and blending machine, stir 5-10min;
6) rotating speed is transferred to 800-1000rpm, in mixing and blending machine, drop into water-based emulsion and solidifying agent, in mixing and blending machine, stir 5-30min and get product.
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| Application Number | Priority Date | Filing Date | Title |
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| CN2012105595476A CN102993937A (en) | 2012-12-21 | 2012-12-21 | Nanoscale wall surface permeation curing material and preparation method thereof |
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| CN2012105595476A CN102993937A (en) | 2012-12-21 | 2012-12-21 | Nanoscale wall surface permeation curing material and preparation method thereof |
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| CN102993937A true CN102993937A (en) | 2013-03-27 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105754443A (en) * | 2016-02-14 | 2016-07-13 | 佛山市恒学科技服务有限公司 | Efficient wallpaper base film |
| CN106947302A (en) * | 2017-04-06 | 2017-07-14 | 卢文书 | A kind of net taste interfacial agents of net aldehyde and preparation method thereof |
| CN108034893A (en) * | 2017-12-26 | 2018-05-15 | 苏州贝尔纳德铁路设备有限公司 | A kind of preparation method of railway equipment stainless steel clad plate |
| CN109880512A (en) * | 2019-02-18 | 2019-06-14 | 南京信息工程大学 | Silicane-modified polyurethane water-repellent paint and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1397618A (en) * | 2002-07-04 | 2003-02-19 | 许凤和 | Environment protection type water polyester paint for wood products and its preparing process |
| CN102443345A (en) * | 2011-10-27 | 2012-05-09 | 北京东方雨虹防水技术股份有限公司 | Aqueous polyurethane wall paint and preparation method thereof |
| CN102504685A (en) * | 2011-11-18 | 2012-06-20 | 肇庆千江高新材料科技有限公司 | Acid rain-resistant antifouling aqueous nanometer polyurethane exterior wall finish |
-
2012
- 2012-12-21 CN CN2012105595476A patent/CN102993937A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1397618A (en) * | 2002-07-04 | 2003-02-19 | 许凤和 | Environment protection type water polyester paint for wood products and its preparing process |
| CN102443345A (en) * | 2011-10-27 | 2012-05-09 | 北京东方雨虹防水技术股份有限公司 | Aqueous polyurethane wall paint and preparation method thereof |
| CN102504685A (en) * | 2011-11-18 | 2012-06-20 | 肇庆千江高新材料科技有限公司 | Acid rain-resistant antifouling aqueous nanometer polyurethane exterior wall finish |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105754443A (en) * | 2016-02-14 | 2016-07-13 | 佛山市恒学科技服务有限公司 | Efficient wallpaper base film |
| CN106947302A (en) * | 2017-04-06 | 2017-07-14 | 卢文书 | A kind of net taste interfacial agents of net aldehyde and preparation method thereof |
| CN108034893A (en) * | 2017-12-26 | 2018-05-15 | 苏州贝尔纳德铁路设备有限公司 | A kind of preparation method of railway equipment stainless steel clad plate |
| CN109880512A (en) * | 2019-02-18 | 2019-06-14 | 南京信息工程大学 | Silicane-modified polyurethane water-repellent paint and preparation method thereof |
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Application publication date: 20130327 |